Experimental Organic Chemistry: A Miniscale & Microscale Approach (Cengage Learning Laboratory Series for Organic Chemistry)
6th Edition
ISBN: 9781305080461
Author: John C. Gilbert, Stephen F. Martin
Publisher: Brooks Cole
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Question
Chapter 4.4, Problem 4E
Interpretation Introduction
Interpretation:Efficiency of packed fractional distillation column is more than that of unpacked column for separation of two closed boiling liquids should be determined.
Concept introduction:Fractional distillation is separation technique that separates various fractions of components in mixture. This process is based on vaporization of one or more fractions or parts of mixture. It is used to separate components of mixture that have difference in boiling points less than
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Chapter 4 Solutions
Experimental Organic Chemistry: A Miniscale & Microscale Approach (Cengage Learning Laboratory Series for Organic Chemistry)
Ch. 4.2 - Prob. 1ECh. 4.2 - Prob. 2ECh. 4.2 - Prob. 3ECh. 4.2 - Prob. 4ECh. 4.2 - Prob. 5ECh. 4.2 - Prob. 6ECh. 4.2 - Prob. 7ECh. 4.2 - Prob. 8ECh. 4.2 - Prob. 9ECh. 4.3 - Prob. 1E
Ch. 4.3 - Prob. 2ECh. 4.3 - Prob. 3ECh. 4.3 - Prob. 4ECh. 4.3 - Prob. 5ECh. 4.3 - Prob. 6ECh. 4.3 - Prob. 7ECh. 4.3 - Prob. 8ECh. 4.4 - Prob. 1ECh. 4.4 - Prob. 2ECh. 4.4 - Prob. 3ECh. 4.4 - Prob. 4ECh. 4.4 - Prob. 5ECh. 4.4 - Prob. 6ECh. 4.4 - Prob. 7ECh. 4.4 - Prob. 8ECh. 4.4 - Prob. 9ECh. 4.4 - Prob. 11ECh. 4.4 - Prob. 12ECh. 4.4 - Prob. 13ECh. 4.4 - Prob. 14ECh. 4.6 - Prob. 1ECh. 4.6 - Prob. 2ECh. 4.6 - Prob. 3ECh. 4.6 - Prob. 4ECh. 4.6 - Prob. 5ECh. 4.6 - Prob. 6ECh. 4.6 - Prob. 7ECh. 4.6 - Prob. 8ECh. 4.6 - Prob. 9E
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- What limitations are encountered in the apolication of sublimation as a general method of purification?arrow_forwardThe melting-point capillary of a white crystalline substance is left to cool. The same capillary shows a substantially higher melting point of 145°C. Repeated recrystallization produces sharp melting points of about 114°C. Explain the behavior of a cooled and remelted sample.arrow_forwardBriefly explain how slow cooling contributes to the formation of pure crystals during recrystallization.arrow_forward
- What specifically occurs when a liquid mixture is distilled? O ) Components of a solid mixture are separated by differences in melting points 2) Components of a solid mixture are separated by differences in boiling points 3) Components of a liquid mixture are separated by differences in boiling points 4) Components of a liquid mixture are separated by differences in melting pointsarrow_forwardWhen performing a recrystallization of an impure solid, why is it important to allow the heated solution to cool slowly? Group of answer choices For the molecules of the pure solid to arrange in organized crystal lattices. To encourage solubility. To avoid the need for ice. To trap particles in the crystal lattice.arrow_forwardHeating a solid until it passes directly from the solid phase into the gaseous phase. Separating a liquid from an insoluble solid sediment by carefully pouring the liquid from the solid without disturbing the solid. The process of vapor returning to the solid phase without a liquid phase in between. Heating a mixture to vaporize a volatile liquid component to make the remaining component dry. Separating a solid from a liquid using a porous material, such as paper, charcoal, or sand, as a filter. Using a solvent to selectively dissolve one or more components from a solid mixture. Answer Bank extraction filtration decantation deposition sublimation evaporationarrow_forward
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