Experimental Organic Chemistry: A Miniscale & Microscale Approach (Cengage Learning Laboratory Series for Organic Chemistry)
Experimental Organic Chemistry: A Miniscale & Microscale Approach (Cengage Learning Laboratory Series for Organic Chemistry)
6th Edition
ISBN: 9781305080461
Author: John C. Gilbert, Stephen F. Martin
Publisher: Brooks Cole
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Chapter 4.3, Problem 2E
Interpretation Introduction

Interpretation:Completely labeled apparatus that is required for simple distillation should be determined.

Concept introduction: Simple distillation is a separation technique that is used to separate a mixture of organic compounds with the difference in their boiling points more than 40 °C . In other words, this procedure is applied for the removal of nonvolatile impurities from volatile solvents. If one of the compounds in an organic mixture is volatile, its vapors will form first and are converted into liquid with help of condenser. This way all of volatile compound gets converted into liquid and therefore it is separated from nonvolatile component.

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Transmitance 3. Which one of the following compounds corresponds to this IR spectrum? Point out the absorption band(s) that helped you decide. OH H3C OH H₂C CH3 H3C CH3 H3C INFRARED SPECTRUM 0.8- 0.6 0.4- 0.2 3000 2000 1000 Wavenumber (cm-1) 4. Consider this compound: H3C On the structure above, label the different types of H's as A, B, C, etc. In table form, list the labeled signals, and for each one state the number of hydrogens, their shifts, and the splitting you would observe for these hydrogens in the ¹H NMR spectrum. Label # of hydrogens splitting Shift (2)
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