Experimental Organic Chemistry: A Miniscale & Microscale Approach (Cengage Learning Laboratory Series for Organic Chemistry)
Experimental Organic Chemistry: A Miniscale & Microscale Approach (Cengage Learning Laboratory Series for Organic Chemistry)
6th Edition
ISBN: 9781305080461
Author: John C. Gilbert, Stephen F. Martin
Publisher: Brooks Cole
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Chapter 4.3, Problem 5E

a)

Interpretation Introduction

Interpretation: Effect on observed temperature if thermometer bulb is placed below condenser should be determined.

Concept introduction: Distillation is technique that is used to separate components of liquid mixture with help of selective boiling and condensation. This procedure either separates components partially or completely from mixture. It is one of physical process to separate mixtures and not by chemical reactions.

b)

Interpretation Introduction

Interpretation: Effect on observed temperature if thermometer bulb is placed above condenser should be determined.

Concept introduction: Distillation is technique that is used to separate components of liquid mixture with help of selective boiling and condensation. This procedure either separates components partially or completely from mixture. It is one of physical process to separate mixtures and not by chemical reactions.

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Transmitance 3. Which one of the following compounds corresponds to this IR spectrum? Point out the absorption band(s) that helped you decide. OH H3C OH H₂C CH3 H3C CH3 H3C INFRARED SPECTRUM 0.8- 0.6 0.4- 0.2 3000 2000 1000 Wavenumber (cm-1) 4. Consider this compound: H3C On the structure above, label the different types of H's as A, B, C, etc. In table form, list the labeled signals, and for each one state the number of hydrogens, their shifts, and the splitting you would observe for these hydrogens in the ¹H NMR spectrum. Label # of hydrogens splitting Shift (2)
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