O-0005 Safety_ CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I_II_2

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10/22/23, 11:50 PM O-0005 Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652167 1/9 O-0005 Safety Due No due date Points 14 Questions 14 Available Sep 5 at 12a.m. - Dec 6 at 11:59p.m. Time Limit 30 Minutes Allowed Attempts Unlimited Instructions Attempt History Attempt Time Score KEPT Attempt 2 6 minutes 13.38 out of 14 LATEST Attempt 2 6 minutes 13.38 out of 14 Attempt 1 9 minutes 8 out of 14 Correct answers are hidden. Score for this attempt: 13.38 out of 14 Submitted Oct 22 at 11:50p.m. This attempt took 6 minutes. Provide the correct answer to each of the following safety questions. You answer correctly to 80% of the questions of this quiz in order to perform the experiment in the organic laboratory. Take the Quiz Again 1 / 1 pts Question 1 You want to start your reaction, but you realize that the stirplate is not working. What is the fits thing you should do? Call the laboratory technicial and ask them to check all the plates in the lab. Call the lab director and ask them to look into the problem.
10/22/23, 11:50 PM O-0005 Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652167 2/9 Call 911 Call your TA and ask them to solve the problem. Check if it is plugged into the wall socket. 1 / 1 pts Question 2 The heating source (Thermowell, heating mantle, oil bath) must NEVER be directly plugged into the wall socket. It should be plugged into a power regulator, and the regulator in turn should be plugged into the wall socket. True False 1 / 1 pts Question 3 When assembling a reflux condenser, the tubing should be connected such that the water flows against gravity. True
10/22/23, 11:50 PM O-0005 Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652167 3/9 False Yes! This is correct. Make sure you keep the water flow against gravity. 1 / 1 pts Question 4 What would you use to monitor the temperature of your oil bath when the procedure calls for a careful control of the reaction temperature? The lab instructor's thermic vision Digital thermometer Mercury thermometer The palm of your hand to feel the heat irradiated from the bath 1 / 1 pts Question 5 Match the laboratoy equipment or glassware with their correct name. a. Reflux condenser
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10/22/23, 11:50 PM O-0005 Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652167 4/9 b. Stir plate c. Round bottom flask d. Lab jack e. Three prong clamp 1 / 1 pts Question 6 What type of glassware/piece of equipment would you use to add a solid reactant to a round bottom flask to prevent the solid to contaminate the walls of the glass joint? Büchner funnel Glass funnel Hirsch funnel Plastic solids' funnel 1 / 1 pts Question 7 Where should you dispose of the drying agent (Na SO or MgSO ) once you have finished the extraction/drying process? 2 4 4 In the halogenated waste in the waste fumehood. The solid waste containter in the waste fumehood.
10/22/23, 11:50 PM O-0005 Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652167 5/9 In the non-halogenated waste in the waste fumehood. In the trash can at the end of the bench. 1 / 1 pts Question 8 Where should you dispose of the discarded aqueous layers collected after any separation or extraction? Halogenated waste in fumehood area Non-halogenated waste in fumehood area Solid waste in fumehood area Down the drain with lots of cold running water. 1 / 1 pts Question 9 If you spill 100 mL DCM on your bench, the best course of action is: To call 911 and evacuate the lab as DCM is extremely dangerous No action is necessary, it will evaporate quickly on its own To use paper towels to absorb as much as possible and leave it in the fume hood to dry To move away all heat sources as DCM is flammable and then let it evaporate
10/22/23, 11:50 PM O-0005 Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652167 6/9 1 / 1 pts Question 10 A student forgot to add 3M HCl at the end of the reaction. What problem can this lead to? Unreacted sodium borohydride can reduce the nitro group Some product will remain deprotonated and stay in the aqueous layer Aldol reaction can occur under basic conditions Some borohydride will not be quenched and can be extracted into DCM 1 / 1 pts Question 11 A student added too much 3M HCl to their reaction mixture at the end of the reaction. What problem can this lead to? The amino group can get protonated, rendering the product water-soluble The product will decompose under strong acidic conditions The nitro group can be reduced under acidic conditions Too much hydrogen will be generated from unreacted borohydride, which is a safety issue 1 / 1 pts Question 12 What is the maximum volume of solution that can be concentrated in a 100 mL round bottom flask (RBF) on the rotary evaporator?
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10/22/23, 11:50 PM O-0005 Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652167 7/9 10 mL at a time. 50 mL 25 mL Any volume, it does not make a difference. 100 mL 0.38 / 1 pts Question 13 Partial Partial One of the most common procedures in organic synthesis is the removal of solvent at reduced pressure using a rotary evaporator. Correctly match the steps to the order in which they should be done to safely perform the rotary evaporation in the lab. e.g. Step 1. Connect the round bottom flask to the rotovap trap and hold it in place. Step 2... Sep 6. Look at the condenser and look for the point where no more solvent is dripping. Setp 7... Step 11. Disconnect the RBF from the rotary evaporator. Step 2. Connect the vaccum tub Step 3. Move the red lever to a Step 4. Start the rotation. Step 5.
10/22/23, 11:50 PM O-0005 Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652167 8/9 Lower the RBF into the w Step 7. Stop the rotation. Step 8. Move the red lever to a v Step 9. Hold your RBF with you Step 10. Remove the RBF from t 1 / 1 pts Question 14 In organic chemistry, rotary evaporation is used to remove organic solvents under reduced pressure. You can do so in one go or in several iterations. Between iterations, it does not matter if there's a little solvent left in the flask, it can be removed on the next iteration. Only when you are "rotovapping" your last batch you want to ensure no solvent (or only traces) are left. How would you ensure that all the solvent has been removed from your flask in the last instance of your rotary evaporation? Add drying agent to the flast to ensure no water is present in the sample After the solvent has stopped dripping on the condenser, wait 50 min. before you disconnect the flask from the rotovap. After the solvent has stopped dripping on the condenser, wait 5 min. before you disconnect the flask from the rotovap.
10/22/23, 11:50 PM O-0005 Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652167 9/9 Let the flask sit on the bench top for 30 min. so any solvent evaporates on its own Quiz Score: 13.38 out of 14
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