O-007C Safety_ CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I_II_2

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10/24/23, 3:42 AM O-007C Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652150 1/6 O-007C Safety Due No due date Points 10 Questions 10 Available Sep 5 at 12a.m. - Dec 6 at 11:59p.m. Time Limit 30 Minutes Allowed Attempts Unlimited Instructions Attempt History Attempt Time Score KEPT Attempt 2 3 minutes 9 out of 10 LATEST Attempt 2 3 minutes 9 out of 10 Attempt 1 3 minutes 8 out of 10 Correct answers are hidden. Score for this attempt: 9 out of 10 Submitted Oct 24 at 3:41a.m. This attempt took 3 minutes. Provide the correct answer to each of the following safety questions. You answer correctly to 80% of the questions of this quiz in order to perform the experiment in the organic laboratory. Take the Quiz Again 1 / 1 pts Question 1 The heating source (Thermowell, heating mantle, oil bath) must NEVER be directly plugged into the wall socket. It should be plugged into a power regulator, and the regulator in turn should be plugged into the wall socket. True False
10/24/23, 3:42 AM O-007C Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652150 2/6 1 / 1 pts Question 2 Match the laboratoy equipment or glassware with their correct name. a. Reflux condenser b. Stir plate c. Round bottom flask d. Lab jack e. Three prong clamp 1 / 1 pts Question 3 When you perform any reaction, all the reagents should be adequately mixed to maximize the collisions between the reactants. Which of the following would be the most appropriate way of guaranteeing this is true of your reaction taking place inside a round bottom flask (RBF)?
10/24/23, 3:42 AM O-007C Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652150 3/6 Periodically stir the reaction manually using a glass stir rod. The reactants will effectively mix on their own without an external mechanical aid Before charging the RBF with the reagents, place a magnetic stir bar inside the RBF Swirl the contents of the flask vigoruosly before you finally clamp the RBF in place 0 / 1 pts Question 4 Incorrect Incorrect You want to set up a reaction (or recrystallization) where the temperature will be controlled by the boiling point of your solvent or mixture of solvents, and you do not need to regulate or monitor the temperature. Which type of heat source would be the most adequate to use? Microwave reactor Thermowell Heating mantle Oil bath Heat gun 1 / 1 pts Question 5 How many clamps are necessary to safely hold a reflux apparatus in place?
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10/24/23, 3:42 AM O-007C Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652150 4/6 4 2 3 1 1 / 1 pts Question 6 In organic chemistry, rotary evaporation is used to remove organic solvents under reduced pressure. You can do so in one go or in several iterations. Between iterations, it does not matter if there's a little solvent left in the flask, it can be removed on the next iteration. Only when you are "rotovapping" your last batch you want to ensure no solvent (or only traces) are left. How would you ensure that all the solvent has been removed from your flask in the last instance of your rotary evaporation? After the solvent has stopped dripping on the condenser, wait 5 min. before you disconnect the flask from the rotovap. Add drying agent to the flast to ensure no water is present in the sample After the solvent has stopped dripping on the condenser, wait 50 min. before you disconnect the flask from the rotovap. Let the flask sit on the bench top for 30 min. so any solvent evaporates on its own 1 / 1 pts Question 7
10/24/23, 3:42 AM O-007C Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652150 5/6 What specific fault in the glassware should you look for before you decide to use a round bottom flask for rotary evaporation? Residual label adhesive Dirt or water stains Any star crack in the flask Any marker stains 1 / 1 pts Question 8 What is the maximum volume of solution that can be concentrated in a 100 mL round bottom flask (RBF) on the rotary evaporator? 100 mL 50 mL Any volume, it does not make a difference. 25 mL 10 mL at a time. 1 / 1 pts Question 9 A molybdate stain is used as a secondary visualization method during TLC analysis. The solution should not be kept in the fumehood and should not be in contact with your skin because it is... corrosive.
10/24/23, 3:42 AM O-007C Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652150 6/6 flamable. a biological hazard. a lacrimator. caustic. 1 / 1 pts Question 10 After you use the TLC plates, where should you dispose of them? In waste bucket labeled "TLC waste" The solid waste containter in the waste fumehood. In the trash can at the end of the bench. Take it home as a souvenir. Quiz Score: 9 out of 10
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