O-0005 Safety_ CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I_II_3

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10/22/23, 11:55 PM O-0005 Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652167 1/9 O-0005 Safety Due No due date Points 14 Questions 14 Available Sep 5 at 12a.m. - Dec 6 at 11:59p.m. Time Limit 30 Minutes Allowed Attempts Unlimited Instructions Attempt History Attempt Time Score KEPT Attempt 3 5 minutes 14 out of 14 LATEST Attempt 3 5 minutes 14 out of 14 Attempt 2 6 minutes 13.38 out of 14 Attempt 1 9 minutes 8 out of 14 Correct answers are hidden. Score for this attempt: 14 out of 14 Submitted Oct 22 at 11:55p.m. This attempt took 5 minutes. Provide the correct answer to each of the following safety questions. You answer correctly to 80% of the questions of this quiz in order to perform the experiment in the organic laboratory. Take the Quiz Again 1 / 1 pts Question 1 You want to start your reaction, but you realize that the stirplate is not working. What is the fits thing you should do? Call your TA and ask them to solve the problem.
10/22/23, 11:55 PM O-0005 Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652167 2/9 Call the laboratory technicial and ask them to check all the plates in the lab. Call the lab director and ask them to look into the problem. Call 911 Check if it is plugged into the wall socket. 1 / 1 pts Question 2 When assembling a reflux condenser, the tubing should be connected such that the water flows against gravity. True False
10/22/23, 11:55 PM O-0005 Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652167 3/9 Yes! This is correct. Make sure you keep the water flow against gravity. 1 / 1 pts Question 3 What would you use to monitor the temperature of your oil bath when the procedure calls for a careful control of the reaction temperature? The palm of your hand to feel the heat irradiated from the bath The lab instructor's thermic vision Digital thermometer Mercury thermometer 1 / 1 pts Question 4 How many clamps are necessary to safely hold a reflux apparatus in place? 2 4 1 3
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10/22/23, 11:55 PM O-0005 Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652167 4/9 1 / 1 pts Question 5 You want to set up a reaction where you are required to maintain the temperature within a small temperature range. Which type of heat source should you use? Oil bath Microwave reactor Heat gun Heating mantle Thermowell 1 / 1 pts Question 6 What type of glassware/piece of equipment would you use to add a solid reactant to a round bottom flask to prevent the solid to contaminate the walls of the glass joint? Hirsch funnel Büchner funnel Plastic solids' funnel Glass funnel 1 / 1 pts Question 7
10/22/23, 11:55 PM O-0005 Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652167 5/9 Where should you dispose of the drying agent (Na SO or MgSO ) once you have finished the extraction/drying process? 2 4 4 In the non-halogenated waste in the waste fumehood. The solid waste containter in the waste fumehood. In the trash can at the end of the bench. In the halogenated waste in the waste fumehood. 1 / 1 pts Question 8 Where should you dispose of the discarded aqueous layers collected after any separation or extraction? Halogenated waste in fumehood area Non-halogenated waste in fumehood area Down the drain with lots of cold running water. Solid waste in fumehood area 1 / 1 pts Question 9 If you spill 100 mL DCM on your bench, the best course of action is: To use paper towels to absorb as much as possible and leave it in the fume hood to dry
10/22/23, 11:55 PM O-0005 Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652167 6/9 No action is necessary, it will evaporate quickly on its own To call 911 and evacuate the lab as DCM is extremely dangerous To move away all heat sources as DCM is flammable and then let it evaporate 1 / 1 pts Question 10 A student forgot to add 3M HCl at the end of the reaction. What problem can this lead to? Some product will remain deprotonated and stay in the aqueous layer Unreacted sodium borohydride can reduce the nitro group Aldol reaction can occur under basic conditions Some borohydride will not be quenched and can be extracted into DCM 1 / 1 pts Question 11 A student added too much 3M HCl to their reaction mixture at the end of the reaction. What problem can this lead to? The amino group can get protonated, rendering the product water-soluble Too much hydrogen will be generated from unreacted borohydride, which is a safety issue
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10/22/23, 11:55 PM O-0005 Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652167 7/9 The product will decompose under strong acidic conditions The nitro group can be reduced under acidic conditions 1 / 1 pts Question 12 What is the maximum volume of solution that can be concentrated in a 100 mL round bottom flask (RBF) on the rotary evaporator? 50 mL 25 mL 100 mL Any volume, it does not make a difference. 10 mL at a time. 1 / 1 pts Question 13 One of the most common procedures in organic synthesis is the removal of solvent at reduced pressure using a rotary evaporator. Correctly match the steps to the order in which they should be done to safely perform the rotary evaporation in the lab. e.g. Step 1. Connect the round bottom flask to the rotovap trap and hold it in place. Step 2... Sep 6. Look at the condenser and look for the point where no more solvent is dripping.
10/22/23, 11:55 PM O-0005 Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652167 8/9 Setp 7... Step 11. Disconnect the RBF from the rotary evaporator. Step 2. Connect the vaccum tu Step 3. Move the red lever to a Step 4. Start the rotation. Step 5. Lower the RBF into the Step 7. Remove the RBF from Step 8. Stop the rotation. Step 9. Move the red lever to a Step 10. Hold your RBF with you 1 / 1 pts Question 14 What specific fault in the glassware should you look for before you decide to use a round bottom flask for rotary evaporation? Any star crack in the flask Residual label adhesive
10/22/23, 11:55 PM O-0005 Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652167 9/9 Dirt or water stains Any marker stains Quiz Score: 14 out of 14
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