O-0005 Safety_ CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I_II

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10/22/23, 11:43 PM O-0005 Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652167 1/8 O-0005 Safety Due No due date Points 14 Questions 14 Available Sep 5 at 12a.m. - Dec 6 at 11:59p.m. Time Limit 30 Minutes Allowed Attempts Unlimited Instructions Attempt History Attempt Time Score LATEST Attempt 1 9 minutes 8 out of 14 Correct answers are hidden. Score for this attempt: 8 out of 14 Submitted Oct 22 at 11:43p.m. This attempt took 9 minutes. Provide the correct answer to each of the following safety questions. You answer correctly to 80% of the questions of this quiz in order to perform the experiment in the organic laboratory. Take the Quiz Again 0 / 1 pts Question 1 Incorrect Incorrect You want to set up a reaction where you are required to maintain the temperature within a small temperature range. Which type of heat source should you use? Heat gun Heating mantle Microwave reactor
10/22/23, 11:43 PM O-0005 Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652167 2/8 Oil bath Thermowell 0 / 1 pts Question 2 Incorrect Incorrect When assembling a reflux condenser, the tubing should be connected such that the water flows against gravity. True False 1 / 1 pts Question 3 When you perform any reaction, all the reagents should be adequately mixed to maximize the collisions between the reactants. Which of the following would be the most appropriate way of guaranteeing this is true of your reaction taking place inside a round bottom flask (RBF)?
10/22/23, 11:43 PM O-0005 Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652167 3/8 Swirl the contents of the flask vigoruosly before you finally clamp the RBF in place Periodically stir the reaction manually using a glass stir rod. Before charging the RBF with the reagents, place a magnetic stir bar inside the RBF The reactants will effectively mix on their own without an external mechanical aid 1 / 1 pts Question 4 What would you use to monitor the temperature of your oil bath when the procedure calls for a careful control of the reaction temperature? The lab instructor's thermic vision Mercury thermometer The palm of your hand to feel the heat irradiated from the bath Digital thermometer 0 / 1 pts Question 5 Incorrect Incorrect How many clamps are necessary to safely hold a reflux apparatus in place? 4
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10/22/23, 11:43 PM O-0005 Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652167 4/8 3 2 1 0 / 1 pts Question 6 Incorrect Incorrect What type of glassware/piece of equipment would you use to add a solid reactant to a round bottom flask to prevent the solid to contaminate the walls of the glass joint? Glass funnel Hirsch funnel Plastic solids' funnel Büchner funnel 1 / 1 pts Question 7 Where should you dispose of the drying agent (Na SO or MgSO ) once you have finished the extraction/drying process? 2 4 4 In the non-halogenated waste in the waste fumehood. In the halogenated waste in the waste fumehood. The solid waste containter in the waste fumehood. In the trash can at the end of the bench.
10/22/23, 11:43 PM O-0005 Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652167 5/8 1 / 1 pts Question 8 Where should you dispose of the discarded aqueous layers collected after any separation or extraction? Non-halogenated waste in fumehood area Halogenated waste in fumehood area Down the drain with lots of cold running water. Solid waste in fumehood area 1 / 1 pts Question 9 If you spill 100 mL DCM on your bench, the best course of action is: To call 911 and evacuate the lab as DCM is extremely dangerous To move away all heat sources as DCM is flammable and then let it evaporate To use paper towels to absorb as much as possible and leave it in the fume hood to dry No action is necessary, it will evaporate quickly on its own 1 / 1 pts Question 10 A student forgot to add 3M HCl at the end of the reaction. What problem can this lead to?
10/22/23, 11:43 PM O-0005 Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652167 6/8 Aldol reaction can occur under basic conditions Some borohydride will not be quenched and can be extracted into DCM Unreacted sodium borohydride can reduce the nitro group Some product will remain deprotonated and stay in the aqueous layer 0 / 1 pts Question 11 Incorrect Incorrect A student added too much 3M HCl to their reaction mixture at the end of the reaction. What problem can this lead to? Too much hydrogen will be generated from unreacted borohydride, which is a safety issue The nitro group can be reduced under acidic conditions The product will decompose under strong acidic conditions The amino group can get protonated, rendering the product water-soluble 1 / 1 pts Question 12 To ensure a quantitative transfer from the flask containing your sample to the round bottom flask you use for the rotary evaporation, you can rinse the flask that originally contained your sample with small portions of the solvent to wash any sample left behind. True False
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10/22/23, 11:43 PM O-0005 Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652167 7/8 1 / 1 pts Question 13 What is the maximum volume of solution that can be concentrated in a 100 mL round bottom flask (RBF) on the rotary evaporator? 10 mL at a time. Any volume, it does not make a difference. 25 mL 100 mL 50 mL 0 / 1 pts Question 14 Incorrect Incorrect In organic chemistry, rotary evaporation is used to remove organic solvents under reduced pressure. You can do so in one go or in several iterations. Between iterations, it does not matter if there's a little solvent left in the flask, it can be removed on the next iteration. Only when you are "rotovapping" your last batch you want to ensure no solvent (or only traces) are left. How would you ensure that all the solvent has been removed from your flask in the last instance of your rotary evaporation? Add drying agent to the flast to ensure no water is present in the sample After the solvent has stopped dripping on the condenser, wait 5 min. before you disconnect the flask from the rotovap. Let the flask sit on the bench top for 30 min. so any solvent evaporates on its own
10/22/23, 11:43 PM O-0005 Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652167 8/8 After the solvent has stopped dripping on the condenser, wait 50 min. before you disconnect the flask from the rotovap. Quiz Score: 8 out of 14

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