O-007C Safety_ CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I_II_3

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10/24/23, 3:45 AM O-007C Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652150 1/7 O-007C Safety Due No due date Points 10 Questions 10 Available Sep 5 at 12a.m. - Dec 6 at 11:59p.m. Time Limit 30 Minutes Allowed Attempts Unlimited Instructions Attempt History Attempt Time Score KEPT Attempt 3 3 minutes 10 out of 10 LATEST Attempt 3 3 minutes 10 out of 10 Attempt 2 3 minutes 9 out of 10 Attempt 1 3 minutes 8 out of 10 Correct answers are hidden. Score for this attempt: 10 out of 10 Submitted Oct 24 at 3:44a.m. This attempt took 3 minutes. Provide the correct answer to each of the following safety questions. You answer correctly to 80% of the questions of this quiz in order to perform the experiment in the organic laboratory. Take the Quiz Again 1 / 1 pts Question 1 Indicate the correct order in which the following items should be assembled to construct a reflux apparatus. The construction should be from the bench top upwards.
10/24/23, 3:45 AM O-007C Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652150 2/7 a, c, e, b, d d, b, e, c, a b, d, e, c, a a, c, e, d, b 1 / 1 pts Question 2 You want to set up a reaction (or recrystallization) where the temperature will be controlled by the boiling point of your solvent or mixture of solvents, and you do not need to regulate or monitor the temperature. Which type of heat source would be the most adequate to use? Oil bath Thermowell Microwave reactor Heating mantle Heat gun 1 / 1 pts Question 3
10/24/23, 3:45 AM O-007C Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652150 3/7 This piece of equipment should always be part of the apparatus set-up whenever a reaction is being heated. Its main purpose is facilitate the quick removal of the heat source away from the round bottom flask. It is particularly important if the reaction is overheated or any material is being unsafely projected outside the reaction pot. Water pump Lab jack Stir plate Ice-water bath Condenser 1 / 1 pts Question 4 You want to set up a reaction where you are required to maintain the temperature within a small temperature range. Which type of heat source should you use? Microwave reactor Oil bath Heat gun Heating mantle Thermowell 1 / 1 pts Question 5
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10/24/23, 3:45 AM O-007C Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652150 4/7 When you perform any reaction, all the reagents should be adequately mixed to maximize the collisions between the reactants. Which of the following would be the most appropriate way of guaranteeing this is true of your reaction taking place inside a round bottom flask (RBF)? Swirl the contents of the flask vigoruosly before you finally clamp the RBF in place The reactants will effectively mix on their own without an external mechanical aid Before charging the RBF with the reagents, place a magnetic stir bar inside the RBF Periodically stir the reaction manually using a glass stir rod. 1 / 1 pts Question 6 What specific fault in the glassware should you look for before you decide to use a round bottom flask for rotary evaporation? Any marker stains Any star crack in the flask Residual label adhesive Dirt or water stains
10/24/23, 3:45 AM O-007C Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652150 5/7 1 / 1 pts Question 7 One of the most common procedures in organic synthesis is the removal of solvent at reduced pressure using a rotary evaporator. Correctly match the steps to the order in which they should be done to safely perform the rotary evaporation in the lab. e.g. Step 1. Connect the round bottom flask to the rotovap trap and hold it in place. Step 2... Sep 6. Look at the condenser and look for the point where no more solvent is dripping. Setp 7... Step 11. Disconnect the RBF from the rotary evaporator. Step 2. Connect the vaccum tu Step 3. Move the red lever to a Step 4. Start the rotation. Step 5. Lower the RBF into the Step 7. Remove the RBF from Step 8. Stop the rotation. Step 9.
10/24/23, 3:45 AM O-007C Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652150 6/7 Move the red lever to a Step 10. Hold your RBF with you 1 / 1 pts Question 8 To ensure a quantitative transfer from the flask containing your sample to the round bottom flask you use for the rotary evaporation, you can rinse the flask that originally contained your sample with small portions of the solvent to wash any sample left behind. True False 1 / 1 pts Question 9 A molybdate stain is used as a secondary visualization method during TLC analysis. The solution should not be kept in the fumehood and should not be in contact with your skin because it is... flamable. corrosive. a lacrimator. a biological hazard. caustic.
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10/24/23, 3:45 AM O-007C Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652150 7/7 1 / 1 pts Question 10 After you use the TLC plates, where should you dispose of them? Take it home as a souvenir. The solid waste containter in the waste fumehood. In the trash can at the end of the bench. In waste bucket labeled "TLC waste" Quiz Score: 10 out of 10

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