O-007C Safety_ CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I_II

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10/24/23, 3:38 AM O-007C Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652150 1/6 O-007C Safety Due No due date Points 10 Questions 10 Available Sep 5 at 12a.m. - Dec 6 at 11:59p.m. Time Limit 30 Minutes Allowed Attempts Unlimited Instructions Attempt History Attempt Time Score LATEST Attempt 1 3 minutes 8 out of 10 Correct answers are hidden. Score for this attempt: 8 out of 10 Submitted Oct 24 at 3:37a.m. This attempt took 3 minutes. Provide the correct answer to each of the following safety questions. You answer correctly to 80% of the questions of this quiz in order to perform the experiment in the organic laboratory. Take the Quiz Again 1 / 1 pts Question 1 This piece of equipment should always be part of the apparatus set-up whenever a reaction is being heated. Its main purpose is facilitate the quick removal of the heat source away from the round bottom flask. It is particularly important if the reaction is overheated or any material is being unsafely projected outside the reaction pot. Lab jack Water pump
10/24/23, 3:38 AM O-007C Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652150 2/6 Ice-water bath Stir plate Condenser 0 / 1 pts Question 2 Incorrect Incorrect You want to set up a reaction (or recrystallization) where the temperature will be controlled by the boiling point of your solvent or mixture of solvents, and you do not need to regulate or monitor the temperature. Which type of heat source would be the most adequate to use? Oil bath Thermowell Heat gun Microwave reactor Heating mantle 1 / 1 pts Question 3 When assembling a reflux condenser, the tubing should be connected such that the water flows against gravity.
10/24/23, 3:38 AM O-007C Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652150 3/6 True False Yes! This is correct. Make sure you keep the water flow against gravity. 0 / 1 pts Question 4 Incorrect Incorrect You want to set up a reaction where you are required to maintain the temperature within a small temperature range. Which type of heat source should you use? Oil bath Thermowell Microwave reactor Heat gun Heating mantle
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10/24/23, 3:38 AM O-007C Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652150 4/6 1 / 1 pts Question 5 What would you use to monitor the temperature of your oil bath when the procedure calls for a careful control of the reaction temperature? The palm of your hand to feel the heat irradiated from the bath The lab instructor's thermic vision Digital thermometer Mercury thermometer 1 / 1 pts Question 6 What specific fault in the glassware should you look for before you decide to use a round bottom flask for rotary evaporation? Any marker stains Dirt or water stains Any star crack in the flask Residual label adhesive 1 / 1 pts Question 7 What is the maximum volume of solution that can be concentrated in a 100 mL round bottom flask (RBF) on the rotary evaporator?
10/24/23, 3:38 AM O-007C Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652150 5/6 25 mL Any volume, it does not make a difference. 100 mL 10 mL at a time. 50 mL 1 / 1 pts Question 8 To ensure a quantitative transfer from the flask containing your sample to the round bottom flask you use for the rotary evaporation, you can rinse the flask that originally contained your sample with small portions of the solvent to wash any sample left behind. True False 1 / 1 pts Question 9 A molybdate stain is used as a secondary visualization method during TLC analysis. The solution should not be kept in the fumehood and should not be in contact with your skin because it is... caustic. a lacrimator. flamable. a biological hazard.
10/24/23, 3:38 AM O-007C Safety: CHEM 3XX ALL LABS 2023W1 Chemistry Integrated Laboratory I/II https://canvas.ubc.ca/courses/122851/quizzes/652150 6/6 corrosive. 1 / 1 pts Question 10 After you use the TLC plates, where should you dispose of them? In the trash can at the end of the bench. The solid waste containter in the waste fumehood. In waste bucket labeled "TLC waste" Take it home as a souvenir. Quiz Score: 8 out of 10
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