Introductory Chemistry: Concepts and Critical Thinking (8th Edition)
8th Edition
ISBN: 9780134421377
Author: Charles H Corwin
Publisher: PEARSON
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Chapter 11, Problem 27E
Interpretation Introduction
Interpretation:
The three examples of crystalline solids are to be stated.
Concept introduction:
The rigid, incompressible objects present in the surrounding are classified as solid. The rigidity and incompressibility of solids is due to tight packing of particles. The properties of solid are quite different from the properties of liquid and gas.
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Experiment:
Each team will be provided with 5g of a mixture of acetanilide and salicylic acid. You will divide it into three 1.5 g portions in separate 125 mL Erlenmeyer flasks savıng some for melting point analysis. Dissolve the mixture in each flask in ~60mL of DI water by heating to boiling on a hotplate. Take the flasks off the hotplate once you have a clear solution and let them stand on the bench top for 5 mins and then allow them to cool as described below.
Sample A-Let the first sample cool slowly to room temperature by letting it stand on your lab bench, with occasional stirring to promote crystallization.
Sample B-Cool the second sample 1n a tap-water bath to 10-15 °C
Sample C-Cool the third sample in an ice-bath to 0-2 °C
Results:
weight after recrystalization and melting point temp.
A=0.624g,102-115°
B=0.765g, 80-105°
C=1.135g, 77-108
What is the percent yield of A,B, and C.
Chapter 11 Solutions
Introductory Chemistry: Concepts and Critical Thinking (8th Edition)
Ch. 11 - Prob. 1CECh. 11 - Prob. 2CECh. 11 - Prob. 3CECh. 11 - Prob. 4CECh. 11 - Prob. 5CECh. 11 - Prob. 6CECh. 11 - Prob. 7CECh. 11 - Prob. 8CECh. 11 - Prob. 1KTCh. 11 - Prob. 2KT
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