Structure problem4StruktuurprobleemIR Spectrum(liquid film)168640003000200016001200800V (cm)100Mass Spectrum105807760M*14840120204080120160200240280m/e13C NMR Spectrum(50.0 MHz, CDCI, solution)DEPT CH CH,t CHexpansionproton decoupled135130 ppmsolvent20016012080400 (ppm)'H NMR Spectrum(200 MHz, CDCI, solution)expansionelle3.02.01.0ppmIntegralTMS1098764218 (ppm)% of base peak

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Structure problem 4 Struktuurprobleem IR Spectrum (iquid fim) 1686 4000 3000 2000 1600 1200 800 V (cm") 100- 105 Mass Spectrum 80 77 60 M* 148 40 120 20 40 80 120 160 200 240 280 m/e 13C NMR Spectrum (50.0 MHz. CDCI, solution) DEPT CH CH CHt expansion proton decoupled 135 130 ppm solvent 200 160 120 80 40 O 8 (ppm) 'H NMR Spectrum (200 MHz. CDCI, solution) expansion lle 2.0 1.0 ppm Integral TMS 10 9 7 6 4 2 1 8 (ppm) % of base peak

Structure problem 4 Struktuurprobleem IR Spectrum (iquid fim) 1686 4000 3000 2000 1600 1200 800 V (cm") 100- 105 Mass Spectrum 80 77 60 M* 148 40 120 20 40 80 120 160 200 240 280 m/e 13C NMR Spectrum (50.0 MHz. CDCI, solution) DEPT CH CH CHt expansion proton decoupled 135 130 ppm solvent 200 160 120 80 40 O 8 (ppm) 'H NMR Spectrum (200 MHz. CDCI, solution) expansion lle 2.0 1.0 ppm Integral TMS 10 9 7 6 4 2 1 8 (ppm) % of base peak

Principles of Instrumental Analysis

7th Edition

ISBN:9781305577213

Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch

Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch

Chapter19: Nuclear Magnetic Resonance Spectroscopy

Section: Chapter Questions

Problem 19.33QAP

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What is the IR and HNMRAndCNMR and mass