2089 IR Spectrum (liquid film) LL 4000 100 80 of base peak 3000 63 60 405 20 40 13C NMR Spectrum (50.0 MHz CDCI, solution) proton coupled www proton decoupled 200 ¹H NMR Spectrum (200 MHz, CDCI, solution) 10 9 65 83 80 1 8 2000 V (cm¹) M** 98/100/102 120 160 m/e 160 my 689 1600 1200 200 120 800 Mass Spectrum C2H4Cl2 280 solvent 240 expansions 6.0 5.8 ppm J 7 6 5 1 J 80 2.2 2.0 ppm 4 Problem 13 No significant UV absorption above 220 nm 0 3 40 1 2 1 8 (ppm) TMS 1 119 0 8 (ppm)

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Problem 13
119
2089
IR Spectrum
(guid fim)
689
4000
3000
2000
1600
1200
800
V (cm')
100
Mass Spectrum
63
80
No significant UV
60
absorption above 220 nm
40
65
M
98/100/102
83
20
C2H4CI2
40
80
120
160
200
240
280
m/e
13C NMR Spectrum
(50.0 MHz. CDCI, solution)
proton coupled
solvent
proton decoupled
200
160
120
80
40
0 8 (ppm)
H NMR Spectrum
(200 MHz. CDCI, solution)
expansions
6.0
5.8 ppm
22 2.0 ppm
TMS
5 4
3
2
1
8 (ppm)
10
8.
6.
102
of base peak
Transcribed Image Text:Problem 13 119 2089 IR Spectrum (guid fim) 689 4000 3000 2000 1600 1200 800 V (cm') 100 Mass Spectrum 63 80 No significant UV 60 absorption above 220 nm 40 65 M 98/100/102 83 20 C2H4CI2 40 80 120 160 200 240 280 m/e 13C NMR Spectrum (50.0 MHz. CDCI, solution) proton coupled solvent proton decoupled 200 160 120 80 40 0 8 (ppm) H NMR Spectrum (200 MHz. CDCI, solution) expansions 6.0 5.8 ppm 22 2.0 ppm TMS 5 4 3 2 1 8 (ppm) 10 8. 6. 102 of base peak
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