100 80 60 4000 20 Wown 2114 3295 IR Spectrum (oud) 40 proton decoupled 2H 10 3C NMR Spectrum (100 MHz, CDC, solution) 3000 ¹H NMR Spectrum (400 MHz, CDC, solution) 25 55 200 I 9 182 80 1 8 2000 M-83 120 V (cm) 2H L 160 expansion 1600 C₂H₂N 160 200 240 280 m/e DEPT CH, CH, CH 1 20 1 7 1H 1200 6 120 Mass Spectrum 2H 800 1.5 5 solvent L L 80 1 exchanges with DO 4 2H 3 No significant UV absorption above 220 m 40 2 113 08 (ppm) 1 TMS 1 L 0 ō (ppm) IR: List bands and possible/probable structural units responsible Band (cm³) Possible stretches/functional groups MS: Molecular Formula 13C NMR: 1 2 3 4 5 6 Chem. Shift (8) Type of C (sp), sp², carbonyl, etc.) ¹H NMR: 1 IHD(DU)= Chem. Shift (8) Multiplicity (singlet, doublet, etc.) 2 3 4 5 6 If you need more space, add any additional signal info here: (Show calculation) # of attached H's #of identical C's in signal Probable Type of H (methyl, aromatic, etc.) #of identical H's in signal

100 80 60 4000 20 Wown 2114 3295 IR Spectrum (oud) 40 proton decoupled 2H 10 3C NMR Spectrum (100 MHz, CDC, solution) 3000 ¹H NMR Spectrum (400 MHz, CDC, solution) 25 55 200 I 9 182 80 1 8 2000 M-83 120 V (cm) 2H L 160 expansion 1600 C₂H₂N 160 200 240 280 m/e DEPT CH, CH, CH 1 20 1 7 1H 1200 6 120 Mass Spectrum 2H 800 1.5 5 solvent L L 80 1 exchanges with DO 4 2H 3 No significant UV absorption above 220 m 40 2 113 08 (ppm) 1 TMS 1 L 0 ō (ppm) IR: List bands and possible/probable structural units responsible Band (cm³) Possible stretches/functional groups MS: Molecular Formula 13C NMR: 1 2 3 4 5 6 Chem. Shift (8) Type of C (sp), sp², carbonyl, etc.) ¹H NMR: 1 IHD(DU)= Chem. Shift (8) Multiplicity (singlet, doublet, etc.) 2 3 4 5 6 If you need more space, add any additional signal info here: (Show calculation) # of attached H's #of identical C's in signal Probable Type of H (methyl, aromatic, etc.) #of identical H's in signal

Chemistry

10th Edition

ISBN:9781305957404

Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Chapter1: Chemical Foundations

Section: Chapter Questions

Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...

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