100 80 60 4000 20 Wown 2114 3295 IR Spectrum (oud) 40 proton decoupled 2H 10 3C NMR Spectrum (100 MHz, CDC, solution) 3000 ¹H NMR Spectrum (400 MHz, CDC, solution) 25 55 200 I 9 182 80 1 8 2000 M-83 120 V (cm) 2H L 160 expansion 1600 C₂H₂N 160 200 240 280 m/e DEPT CH, CH, CH 1 20 1 7 1H 1200 6 120 Mass Spectrum 2H 800 1.5 5 solvent L L 80 1 exchanges with DO 4 2H 3 No significant UV absorption above 220 m 40 2 113 08 (ppm) 1 TMS 1 L 0 ō (ppm) IR: List bands and possible/probable structural units responsible Band (cm³) Possible stretches/functional groups MS: Molecular Formula 13C NMR: 1 2 3 4 5 6 Chem. Shift (8) Type of C (sp), sp², carbonyl, etc.) ¹H NMR: 1 IHD(DU)= Chem. Shift (8) Multiplicity (singlet, doublet, etc.) 2 3 4 5 6 If you need more space, add any additional signal info here: (Show calculation) # of attached H's #of identical C's in signal Probable Type of H (methyl, aromatic, etc.) #of identical H's in signal

Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
icon
Related questions
Question
3296
IR Spectrum
(quid film)
.......
wwwddd
4000
100
80
60
40F 8
-28
20
40
proton decoupled
10
13C NMR Spectrum
(100 MHz, CDC, solution)
2H
-
3000
¹H NMR Spectrum
(400 MHz, CDC, solution)
55
200
2.5
9
80
82
2114
8
2000
M = 83
120
V (cm-¹)
2H
L
160
expansion
1600 1200
C₂H₂N
160 200 240 280
m/e
DEPT CH, I CH₂ 1 CH 1
2.0
I
7
1H
6
L
120
Mass Spectrum
2H
1.5
800
5
solvent
I
80
exchanges
with DO
4
2H
L
3
No significant UV
absorption above 220 nm
|||
L
40
2
113
08 (ppm)
1
1
TMS
0
8 (ppm)
IR: List bands and possible/probable structural units responsible
Band (cm³)
Possible stretches/functional groups
MS:
Molecular Formula
13C NMR:
1
2
3
4
5
6
¹H NMR:
1
Chem. Shift (8) Type of C (sp, sp2²,
carbonyl, etc.)
2
Chem. Shift (8) Multiplicity (singlet,
doublet, etc.)
IHD(DU)=
3
4
5
6
If you need more space, add any additional signal info here:
(Show calculation)
of attached c
# of attached H's
# of identical C's in
signal
Probable Type of H
(methyl, aromatic, etc.)
# of identical H's
in signal
Transcribed Image Text:3296 IR Spectrum (quid film) ....... wwwddd 4000 100 80 60 40F 8 -28 20 40 proton decoupled 10 13C NMR Spectrum (100 MHz, CDC, solution) 2H - 3000 ¹H NMR Spectrum (400 MHz, CDC, solution) 55 200 2.5 9 80 82 2114 8 2000 M = 83 120 V (cm-¹) 2H L 160 expansion 1600 1200 C₂H₂N 160 200 240 280 m/e DEPT CH, I CH₂ 1 CH 1 2.0 I 7 1H 6 L 120 Mass Spectrum 2H 1.5 800 5 solvent I 80 exchanges with DO 4 2H L 3 No significant UV absorption above 220 nm ||| L 40 2 113 08 (ppm) 1 1 TMS 0 8 (ppm) IR: List bands and possible/probable structural units responsible Band (cm³) Possible stretches/functional groups MS: Molecular Formula 13C NMR: 1 2 3 4 5 6 ¹H NMR: 1 Chem. Shift (8) Type of C (sp, sp2², carbonyl, etc.) 2 Chem. Shift (8) Multiplicity (singlet, doublet, etc.) IHD(DU)= 3 4 5 6 If you need more space, add any additional signal info here: (Show calculation) of attached c # of attached H's # of identical C's in signal Probable Type of H (methyl, aromatic, etc.) # of identical H's in signal
Expert Solution
steps

Step by step

Solved in 3 steps with 3 images

Blurred answer
Knowledge Booster
Electron Paramagnetic Resonance
Learn more about
Need a deep-dive on the concept behind this application? Look no further. Learn more about this topic, chemistry and related others by exploring similar questions and additional content below.
Similar questions
  • SEE MORE QUESTIONS
Recommended textbooks for you
Chemistry
Chemistry
Chemistry
ISBN:
9781305957404
Author:
Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:
Cengage Learning
Chemistry
Chemistry
Chemistry
ISBN:
9781259911156
Author:
Raymond Chang Dr., Jason Overby Professor
Publisher:
McGraw-Hill Education
Principles of Instrumental Analysis
Principles of Instrumental Analysis
Chemistry
ISBN:
9781305577213
Author:
Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:
Cengage Learning
Organic Chemistry
Organic Chemistry
Chemistry
ISBN:
9780078021558
Author:
Janice Gorzynski Smith Dr.
Publisher:
McGraw-Hill Education
Chemistry: Principles and Reactions
Chemistry: Principles and Reactions
Chemistry
ISBN:
9781305079373
Author:
William L. Masterton, Cecile N. Hurley
Publisher:
Cengage Learning
Elementary Principles of Chemical Processes, Bind…
Elementary Principles of Chemical Processes, Bind…
Chemistry
ISBN:
9781118431221
Author:
Richard M. Felder, Ronald W. Rousseau, Lisa G. Bullard
Publisher:
WILEY