7.) From the following sets of data, please propose a reasonable structure for the unknown organic compound. This molecule is entirely composed of C, H, and N only. Please show all of your work and feel free to write on the spectra any clues as to the structure. 4000 3000 2000 1000 5DO uavENI HBERI.. Infrared spectrum of unknown. KBr salt plate sample. 100 MS-NU-6396 80 60 40 20 10 20 30 40 50 60 70 80 90 100 110 m/z Mass spectrum of unknown. Molecular ion 83.1 Relative Intensity

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Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
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Chapter1: Chemical Foundations
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Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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7.) From the following sets of data, please propose a reasonable structure for the unknown organic
compound. This molecule is entirely composed of C, H, and N only. Please show all of your work and
feel free to write on the spectra any clues as to the structure.
4000
3000
2000
1000
S DO
Infrared spectrum of unknown. KBr salt plate sample.
100
MS-NU-6396
80
60
40
20 -
10
20
30
40
50
60
70
80
90
100
110
m/z
Mass spectrum of unknown. Molecular ion = 83.1
Relative Intensity
Transcribed Image Text:7.) From the following sets of data, please propose a reasonable structure for the unknown organic compound. This molecule is entirely composed of C, H, and N only. Please show all of your work and feel free to write on the spectra any clues as to the structure. 4000 3000 2000 1000 S DO Infrared spectrum of unknown. KBr salt plate sample. 100 MS-NU-6396 80 60 40 20 - 10 20 30 40 50 60 70 80 90 100 110 m/z Mass spectrum of unknown. Molecular ion = 83.1 Relative Intensity
10
8
7
6.
2
1
ppm
HPM-02-485
'H-NMR of unknown. Singlet at 1.44 ppm, integration = 9 protons.
ppm
Int.
Assign.
125.90
22
3
28.41
1000
28.12
116
1
200
180
160
140
120
100
80
60
40
20
CDS-00-185
ppm
13C-NMR spectrum of unknown (some overlap in signals, see label).
Transcribed Image Text:10 8 7 6. 2 1 ppm HPM-02-485 'H-NMR of unknown. Singlet at 1.44 ppm, integration = 9 protons. ppm Int. Assign. 125.90 22 3 28.41 1000 28.12 116 1 200 180 160 140 120 100 80 60 40 20 CDS-00-185 ppm 13C-NMR spectrum of unknown (some overlap in signals, see label).
Expert Solution
Step 1

IR spectra deals results from the interaction of infrared radiation with matter by absorption. IR spectra uses the IR radiation for the excitation of a molecule and thereby generate the IR spectrum as a function of frequency or wavelength of light. IR spectra has been used as a finger print to identify chemical compounds or functional groups.

Mass spectrum is the technique used in analytical chemistry for the separation of ions based on the mass to charge ratio which basically ionizes chemical species in the ionization chamber of a mass spectrometer. Fragmentation is the breaking up of unstable molecular ions which is usually formed in the ionization chamber of a mass spectrometer. These fragments will cause a pattern in the mass spectrum. 

Every nuclei will have spin and if an external magnetic field is applied, there will be an energy transfer which corresponds to radio frequencies. NMR shows different frequencies which corresponds to different kind of protons in an unknown organic compound.

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