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IR Spectrum d) Wat 4000 100 80 60 41 43 40 10 3000 "C NMR Spectrum (150 MHz, CDC, skon) proton decoupled DEPT CH, CHICHT 200 H NMR Spectrum (100 M CDC, solution) L 9 2248 2000 M83 (15) 80 120 160 200 m/e ▬▬▬▬▬▬▬▬▬ 8 V (cm) 160 23 1600 I 7 22 120 1200 6 Mass Spectrum 240 21 20 expansion (ottosca) L 800 C₂H₂N Corgiv 280 solvent I 5 expansion 80 11 L 4 NE MORE expansion No significant UV absorption above 220 nm are 24226 as as as 10 3 40 2 0 1 8 (ppm) TMS 0 8 (ppm) ppm 20 22 -24 26 -28 116 -118 -120 H-C me-HSQC Spectrum (600 MHz, CDC, solution)-122 Black cross-peaks CH and CH Red cross-peaks CH T -124 TA 3.0 2.8 2.6 2.4 2.2 2.0 1.8 1.6 1.4 1.2 1.0 0.8 0.6 ppm. ppm 20 22 -24 26 28 -116 -118 -120 122 H-C HMBC Spectrum (600 MHz, CDC, solution) TT 124 3.0 2.8 2.6 2.4 2.2 2.0 1.8 1.6 1.4 1.2 1.0 0.8 0.6 ppm IR: List bands and possible/probable structural units responsible Band (cm) Possible stretches/functional groups MS: Molecular Formula DC NMR: 1 2 3 4 5 6 Chem. Shift (8) Type of C (sp), sp², carbonyl, etc.) ¹H NMR: Chem. Shift (8) Multiplicity (singlet, doublet, etc.) vicin IHD(DU)= (Show calculation) 1 2 3 4 5 6 If you need more space, add any additional signal info here: #of attached H's # of identical C's in signal Probable Type of H (methyl, aromatic, etc.) #of identical H's in signal

IR Spectrum d) Wat 4000 100 80 60 41 43 40 10 3000 "C NMR Spectrum (150 MHz, CDC, skon) proton decoupled DEPT CH, CHICHT 200 H NMR Spectrum (100 M CDC, solution) L 9 2248 2000 M83 (15) 80 120 160 200 m/e ▬▬▬▬▬▬▬▬▬ 8 V (cm) 160 23 1600 I 7 22 120 1200 6 Mass Spectrum 240 21 20 expansion (ottosca) L 800 C₂H₂N Corgiv 280 solvent I 5 expansion 80 11 L 4 NE MORE expansion No significant UV absorption above 220 nm are 24226 as as as 10 3 40 2 0 1 8 (ppm) TMS 0 8 (ppm) ppm 20 22 -24 26 -28 116 -118 -120 H-C me-HSQC Spectrum (600 MHz, CDC, solution)-122 Black cross-peaks CH and CH Red cross-peaks CH T -124 TA 3.0 2.8 2.6 2.4 2.2 2.0 1.8 1.6 1.4 1.2 1.0 0.8 0.6 ppm. ppm 20 22 -24 26 28 -116 -118 -120 122 H-C HMBC Spectrum (600 MHz, CDC, solution) TT 124 3.0 2.8 2.6 2.4 2.2 2.0 1.8 1.6 1.4 1.2 1.0 0.8 0.6 ppm IR: List bands and possible/probable structural units responsible Band (cm) Possible stretches/functional groups MS: Molecular Formula DC NMR: 1 2 3 4 5 6 Chem. Shift (8) Type of C (sp), sp², carbonyl, etc.) ¹H NMR: Chem. Shift (8) Multiplicity (singlet, doublet, etc.) vicin IHD(DU)= (Show calculation) 1 2 3 4 5 6 If you need more space, add any additional signal info here: #of attached H's # of identical C's in signal Probable Type of H (methyl, aromatic, etc.) #of identical H's in signal

Chemistry
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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4000 IR Spectrum quid film) 100 80 60 40 YI 2248 41 10 3000 43 40 proton decoupled "C NMR Spectrum (150 MHz CDC, solution) 68 DEPT CH, CH, 1 CHT 9 200 ¹H NMR Spectrum (600 MHz, CDC, solution) M83 (<1%) 80 120 2000 v (cm) 8 m/e 160 160 2.3 L 7 1600 2.2 200 ryper 1200 6 ▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬ 120 Mass Spectrum 240 21 2.0 expansions (not to scale) 800 I CsH₂N 280 5 expansion 80 4 270 255 256 255 expansion No significant UV absorption above 220 nm 27.0 245 250 255 1.0 3 40 L 2 0 8 (ppm) 1 1 TMS L 1 0 8 (ppm) 10 ¹H-¹C me-HSQC Spectrum (600 MHz, CDC, solution) Black cross-peaks CH and CH Red cross-peaks CH₂ ppm 20 ¹H-"C HMBC Spectrum (600 MHz, CDC), solution) -22 -24 -26 -28 116 118 120 122 124 3.0 2.8 2.6 2.4 2.2 2.0 1.8 1.6 1.4 1.2 1.0 0.8 0.6 ppm ppm 20 22 -24 26 28 -116 118 -120 122 -124 3.0 2.8 2.6 2.4 2.2 2.0 1.8 1.6 1.4 1.2 1.0 0.8 0.6 ppm IR: List bands and possible/probable structural units responsible Band (cm³) Possible stretches/functional groups MS: Molecular Formula 13C NMR: 1 2 3 4 5 6 Chem. Shift (8) Type of C (sp, sp², carbonyl, etc.) ¹H NMR: Chem. Shift (8) Multiplicity (singlet, doublet, etc.) IHD(DU)= 1 2 3 4 5 6 If you need more space, add any additional signal info here: (Show calculation) # of attached H's # of identical C's in signal Probable Type of H (methyl, aromatic, etc.) # of identical H's in signal
Transcribed Image Text:4000 IR Spectrum quid film) 100 80 60 40 YI 2248 41 10 3000 43 40 proton decoupled "C NMR Spectrum (150 MHz CDC, solution) 68 DEPT CH, CH, 1 CHT 9 200 ¹H NMR Spectrum (600 MHz, CDC, solution) M83 (<1%) 80 120 2000 v (cm) 8 m/e 160 160 2.3 L 7 1600 2.2 200 ryper 1200 6 ▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬▬ 120 Mass Spectrum 240 21 2.0 expansions (not to scale) 800 I CsH₂N 280 5 expansion 80 4 270 255 256 255 expansion No significant UV absorption above 220 nm 27.0 245 250 255 1.0 3 40 L 2 0 8 (ppm) 1 1 TMS L 1 0 8 (ppm) 10 ¹H-¹C me-HSQC Spectrum (600 MHz, CDC, solution) Black cross-peaks CH and CH Red cross-peaks CH₂ ppm 20 ¹H-"C HMBC Spectrum (600 MHz, CDC), solution) -22 -24 -26 -28 116 118 120 122 124 3.0 2.8 2.6 2.4 2.2 2.0 1.8 1.6 1.4 1.2 1.0 0.8 0.6 ppm ppm 20 22 -24 26 28 -116 118 -120 122 -124 3.0 2.8 2.6 2.4 2.2 2.0 1.8 1.6 1.4 1.2 1.0 0.8 0.6 ppm IR: List bands and possible/probable structural units responsible Band (cm³) Possible stretches/functional groups MS: Molecular Formula 13C NMR: 1 2 3 4 5 6 Chem. Shift (8) Type of C (sp, sp², carbonyl, etc.) ¹H NMR: Chem. Shift (8) Multiplicity (singlet, doublet, etc.) IHD(DU)= 1 2 3 4 5 6 If you need more space, add any additional signal info here: (Show calculation) # of attached H's # of identical C's in signal Probable Type of H (methyl, aromatic, etc.) # of identical H's in signal
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