Relative Intensity 60 20 Unknown #4 Elemental Analysis: 68.90% Carbon, 15.03% Hydrogen, 16.07% Nitrogen Mass Spec 0 10 20 30 13C NMR 50 m/z 03 Mass of Molecular lon= 87 m/z 70 90 100 200 120 160. 140 120 100 80 60 40 20 0 ppm 'H NMR IR 1 100 2 122 doubles ill 2 7 9 ppm HSP-47-343 три 4000 Chemical Formula: Proposed Structure: 2000 1500 1000 500 3000 2000- - HDI Calculation:

Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter9: Atomic Absorption And Atomic Fluorescence Spectrometry
Section: Chapter Questions
Problem 9.16QAP
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Relative Intensity
60
20
Unknown #4
Elemental Analysis:
68.90% Carbon, 15.03% Hydrogen, 16.07% Nitrogen
Mass Spec
0
10
20
30
13C NMR
50
m/z
03
Mass of
Molecular lon=
87 m/z
70
90
100
200
120 160.
140
120
100
80
60
40
20
0
ppm
'H NMR
IR
1
100
2
122
doubles
ill
2
7
9
ppm
HSP-47-343
три
4000
Chemical Formula:
Proposed Structure:
2000 1500 1000 500
3000 2000-
-
HDI Calculation:
Transcribed Image Text:Relative Intensity 60 20 Unknown #4 Elemental Analysis: 68.90% Carbon, 15.03% Hydrogen, 16.07% Nitrogen Mass Spec 0 10 20 30 13C NMR 50 m/z 03 Mass of Molecular lon= 87 m/z 70 90 100 200 120 160. 140 120 100 80 60 40 20 0 ppm 'H NMR IR 1 100 2 122 doubles ill 2 7 9 ppm HSP-47-343 три 4000 Chemical Formula: Proposed Structure: 2000 1500 1000 500 3000 2000- - HDI Calculation:
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