THANSHITTANCETST Relative Intensity LOD 5D Unknown #2 Elemental Analysis: 55.81% Carbon, 7.03% Hydrogen, 37.17% Oxygen Exchanges 100 MS-NW-4945 80- 60 40 40 20 0 10 20 30 40 40 4000 Mass Spec Mass of Molecular lon= 86 m/z 550 50 60 70 80 - 90 100 110 120 m/z IR 3000 2000 AVENUMBER 1500 1000 500 1H NMR with D₂O 5.32 ppm 5.25 ppm 6.07 ppm Chemical Formula: Proposed Structure: 12 15 13C NMR 6 PPM 200 180 160 140 120 100 CDS-03-015 ppm HDI Calculation: 88 80 60 60 40 40 2.90 ppm 20 20 0

Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter6: An Introduction To Spectrometric Methods
Section: Chapter Questions
Problem 6.19QAP
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THANSHITTANCETST
Relative Intensity
LOD
5D
Unknown #2
Elemental Analysis:
55.81% Carbon, 7.03% Hydrogen, 37.17% Oxygen
Exchanges
100
MS-NW-4945
80-
60
40
40
20
0
10
20
30
40
40
4000
Mass Spec
Mass of
Molecular lon=
86 m/z
550
50
60
70
80
-
90
100
110 120
m/z
IR
3000
2000
AVENUMBER 1500
1000
500
1H NMR
with
D₂O
5.32 ppm
5.25 ppm
6.07 ppm
Chemical Formula:
Proposed Structure:
12
15
13C NMR
6
PPM
200
180
160
140
120
100
CDS-03-015
ppm
HDI Calculation:
88
80
60
60
40
40
2.90 ppm
20
20
0
Transcribed Image Text:THANSHITTANCETST Relative Intensity LOD 5D Unknown #2 Elemental Analysis: 55.81% Carbon, 7.03% Hydrogen, 37.17% Oxygen Exchanges 100 MS-NW-4945 80- 60 40 40 20 0 10 20 30 40 40 4000 Mass Spec Mass of Molecular lon= 86 m/z 550 50 60 70 80 - 90 100 110 120 m/z IR 3000 2000 AVENUMBER 1500 1000 500 1H NMR with D₂O 5.32 ppm 5.25 ppm 6.07 ppm Chemical Formula: Proposed Structure: 12 15 13C NMR 6 PPM 200 180 160 140 120 100 CDS-03-015 ppm HDI Calculation: 88 80 60 60 40 40 2.90 ppm 20 20 0
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