Problem 11117 IR Spectrum uit em 4000 1738 3000 2000 1600 v (em') 100 1200 B00 COO 80 Mass Spectrum M 84 No significant uv absorption above 220 nm Cuclo Penanon CHO 40 80 120 160 200 240 280 m/e 13C NMR Spectrum (100 O MHZ. CDC, sokution) DEPT CH CH,t CHt ICH CH proton decoupled solvent 40 8 (ppm) 200 160 120 80 'H NMR Spectrum (400 MHz, CDCI, solution) expansion tripler TMS 2.2 1.8 PPM 3 2 4 8 (ppm 6. 9. 8. 10
Problem 11117 IR Spectrum uit em 4000 1738 3000 2000 1600 v (em') 100 1200 B00 COO 80 Mass Spectrum M 84 No significant uv absorption above 220 nm Cuclo Penanon CHO 40 80 120 160 200 240 280 m/e 13C NMR Spectrum (100 O MHZ. CDC, sokution) DEPT CH CH,t CHt ICH CH proton decoupled solvent 40 8 (ppm) 200 160 120 80 'H NMR Spectrum (400 MHz, CDCI, solution) expansion tripler TMS 2.2 1.8 PPM 3 2 4 8 (ppm 6. 9. 8. 10
Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter19: Nuclear Magnetic Resonance Spectroscopy
Section: Chapter Questions
Problem 19.33QAP
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Question
![Problem 11117
IR Spectrum
quid e
4000
S730
3000
2000
100
1600
v (cm')
1200
B00
B0
Mass Spectrum
60
No significant Uv
absorption above 220 nm
CHO
40
80
120
160
200
240
280
m/e
13C NMR Spectrum
(100 O MHZ. CDCI, solution)
DEPT CH CHt CHt
ICH
proton decoupled
solvent
40
8 (ppm)
200
160
120
80
'H NMR Spectrum
expansion
(400 MHz, CDCI, solution)
tripler
TMS
22
1.8 PPM
4
3
2
8 (ppm)
7.
6.
9.
8
100
iof base peak
10](/v2/_next/image?url=https%3A%2F%2Fcontent.bartleby.com%2Fqna-images%2Fquestion%2F6ee05c2a-a5fe-4634-b66b-ff7772f4d5a9%2F3fd03935-9917-42a9-b3ac-15c92ee840e4%2F92l5efr_processed.jpeg&w=3840&q=75)
Transcribed Image Text:Problem 11117
IR Spectrum
quid e
4000
S730
3000
2000
100
1600
v (cm')
1200
B00
B0
Mass Spectrum
60
No significant Uv
absorption above 220 nm
CHO
40
80
120
160
200
240
280
m/e
13C NMR Spectrum
(100 O MHZ. CDCI, solution)
DEPT CH CHt CHt
ICH
proton decoupled
solvent
40
8 (ppm)
200
160
120
80
'H NMR Spectrum
expansion
(400 MHz, CDCI, solution)
tripler
TMS
22
1.8 PPM
4
3
2
8 (ppm)
7.
6.
9.
8
100
iof base peak
10
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