3420 IR Spectrum (liquid film) 1742 4000 3000 2000 1600 1200 800 v (cm") 100F Mass Spectrum 80 6아 No significant UV absorption above 220 nm M- 104 ( 1%) 2야 76 40 80 120 160 200 240 280 m/e 13C NMR Spectrum (50.0 MHtz. CDCI, sokuton) DEPT CH CHt CHt solvent proton decoupled 200 160 120 80 40 O 8 (ppm) 'H NMR Spectrum (200 MHz. CDCI, solution) % of base peak

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Identify the IR and analyze the mass spec and find the working structure and NMR

3420
IR Spectrum
(liquid film)
1742
4000
3000
2000
1600
1200
800
V (cm")
100
Mass Spectrum
80
60
No significant UV
absorption above 220 nm
40
M*= 104 ( 1%)
20
61
76
40
80
120
160
200
240
280
m/e
13C NMR Spectrum
(50.0 MHtz. CDCI, sokution)
DEPT CH. CHB сн!
solvent
proton decoupled
200
160
120
80
40
8 (ppm)
'H NMR Spectrum
(200 Mitz, CDCI, sokution)
expansions
exchanges
with D20
4.4
4.0
3.6
ppm
14
1.2 ppm
TMS
6
4 3
1
8 (ppm)
10
8
7
% of base peak
2.
Transcribed Image Text:3420 IR Spectrum (liquid film) 1742 4000 3000 2000 1600 1200 800 V (cm") 100 Mass Spectrum 80 60 No significant UV absorption above 220 nm 40 M*= 104 ( 1%) 20 61 76 40 80 120 160 200 240 280 m/e 13C NMR Spectrum (50.0 MHtz. CDCI, sokution) DEPT CH. CHB сн! solvent proton decoupled 200 160 120 80 40 8 (ppm) 'H NMR Spectrum (200 Mitz, CDCI, sokution) expansions exchanges with D20 4.4 4.0 3.6 ppm 14 1.2 ppm TMS 6 4 3 1 8 (ppm) 10 8 7 % of base peak 2.
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