1. Circle the structure that corresponds to the given IR spectrum, mass spectrum, coupled 3C NMR spectrum, and H NMR spectrum. a. Assign the relevant peaks in the IR spectrum for the circled structure. b. Assign the molecular ion and base peaks in the mass spectrum for the circled structure and draw the structure of the fragment ion corresponding to the base peak. c. Assign the peak clusters in the coupled 13C NMR spectrum for the circled structure. d. Assign the peak clusters in the 'H NMR spectrum for the circled structure. OH "OH 0.8 0.6- 0.4 0.2 3000 2000 1000 Wavenumber (cm-1) 100 80 60 40- 20 0.0 0.0 20 40 60 80 100 120 m/z Rel. Intensity Transmitance

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Chapter1: Chemical Foundations
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1. Circle the structure that corresponds to the given IR spectrum, mass spectrum, coupled 13c
NMR spectrum, and H NMR spectrum.
a. Assign the relevant peaks in the IR spectrum for the circled structure.
b. Assign the molecular ion and base peaks in the mass spectrum for the circled structure
and draw the structure of the fragment ion corresponding to the base peak.
c. Assign the peak clusters in the coupled 13C NMR spectrum for the circled structure.
d. Assign the peak clusters in the H NMR spectrum for the circled structure.
OH
HO.
0.8
0.6
0.4
0.2
3000
2000
1000
Wavenumber (cm-1)
100
80
60
40-
20
0.0-
0.0
20
40
60
80
100
120
m/z
Rel. Intensity
Transmitance
Transcribed Image Text:1. Circle the structure that corresponds to the given IR spectrum, mass spectrum, coupled 13c NMR spectrum, and H NMR spectrum. a. Assign the relevant peaks in the IR spectrum for the circled structure. b. Assign the molecular ion and base peaks in the mass spectrum for the circled structure and draw the structure of the fragment ion corresponding to the base peak. c. Assign the peak clusters in the coupled 13C NMR spectrum for the circled structure. d. Assign the peak clusters in the H NMR spectrum for the circled structure. OH HO. 0.8 0.6 0.4 0.2 3000 2000 1000 Wavenumber (cm-1) 100 80 60 40- 20 0.0- 0.0 20 40 60 80 100 120 m/z Rel. Intensity Transmitance
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