Problem 118 IR Spectrum (liquid film) 1698 4000 3000 2000 1600 1200 800 v (cm") 100 Mass Spectrum UV Spectrum 80 M*. 136 A max 277 nm (log10€ 4.2) solvent : methanol 92 107 22 20 C3HBO2 160 m/e 40 80 120 200 240 280 13C NMR Spectrum (100.0 MHz, CDCI, solution) DEPT CH сH снt solvent proton decoupled 200 160 120 80 40 O 8 (ppm) expansion 'H NMR Spectrum (400 MHz, CDCI, solution) 7.65 7.45 6.85 6.65 ppm TMS 10 8 7 6 4 3 2 8 (ppm) % of base peak
Problem 118 IR Spectrum (liquid film) 1698 4000 3000 2000 1600 1200 800 v (cm") 100 Mass Spectrum UV Spectrum 80 M*. 136 A max 277 nm (log10€ 4.2) solvent : methanol 92 107 22 20 C3HBO2 160 m/e 40 80 120 200 240 280 13C NMR Spectrum (100.0 MHz, CDCI, solution) DEPT CH сH снt solvent proton decoupled 200 160 120 80 40 O 8 (ppm) expansion 'H NMR Spectrum (400 MHz, CDCI, solution) 7.65 7.45 6.85 6.65 ppm TMS 10 8 7 6 4 3 2 8 (ppm) % of base peak
Chapter93: Refractometry
Section: Chapter Questions
Problem 2P
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