Prelab Introduction to Qualitative Analysis part 2

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School

Florida International University *

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Course

1045L

Subject

Chemistry

Date

Jun 3, 2024

Type

docx

Pages

6

Uploaded by guille125

Name: Guillermo Rumbos Panther ID: 6206887 Course and section number: CHM 1045L U01 TA Name: Giselle Castano Date: 05 /28/ 2024 Prelab Introduction to Qualitative Analysis part 2 Purpose This lab's objective was to use the flowchart created in the first part of this experiment to analyze an unknown sample that contained some of the ions previously investigated. After analyzing the unknown sample, the recollected data was used to identify what ions were present and explain how that conclusion was achieved.
Flowchart Deep orange precipitate was formed
Procedure When introducing SO4, add the unknown sample in a labeled test tube and add 10 drops of 3 M H2SO4 with a dropper. Record any visual changes and be sure to stir the sample if precipitate forms. Afterwards, centrifugate the sample and record the data. Safely dispose of the sample before cleaning tubes. Ag+, Pb+2, Ni+2, Ba+2, Fe+3 Add HCL Add Heat PPT Ag+ +K2CO 4 Formed white precipitate, light yellow supernatant SP N pB +2 +K2CO 4 Formed precipitate in a cloudy darker yellow supernatant. Supernatant Ni+2, Ba+2, Fe+3 +H2SO 4 PPT Ba+2 SPN Ni+2, Fe+3 PPT Fe+3 Red precipitate was formed NH3+DMG SPN Ni+2 Turned clear blue supernatant +NaO H Formed precipitate Ag+, Pb+2 White precipitate
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