Prelab Introduction to Qualitative Analysis part 2
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Name: Guillermo Rumbos Panther ID: 6206887 Course and section number: CHM 1045L U01 TA Name: Giselle Castano Date: 05 /28/ 2024 Prelab Introduction to Qualitative Analysis part 2
Purpose
This lab's objective was to use the flowchart created in the first part of this experiment to
analyze an unknown sample that contained some of the ions previously investigated. After
analyzing the unknown sample, the recollected data was used to identify what ions were present
and explain how that conclusion was achieved.
Flowchart
Deep orange precipitate was formed
Procedure When introducing SO4, add the unknown sample in a labeled test tube and add 10 drops
of 3 M H2SO4 with a dropper. Record any visual changes and be sure to stir the sample if
precipitate forms. Afterwards, centrifugate the sample and record the data. Safely dispose of the
sample before cleaning tubes. Ag+, Pb+2, Ni+2, Ba+2, Fe+3
Add HCL
Add Heat
PPT
Ag+
+K2CO
4
Formed white precipitate, light yellow supernatant
SP
N
pB
+2
+K2CO
4
Formed precipitate in a cloudy darker yellow supernatant.
Supernatant
Ni+2, Ba+2, Fe+3
+H2SO
4
PPT
Ba+2
SPN
Ni+2, Fe+3
PPT
Fe+3
Red precipitate was formed
NH3+DMG
SPN
Ni+2
Turned clear blue supernatant
+NaO
H
Formed precipitate
Ag+, Pb+2
White precipitate
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Related Questions
Do not give handwriting solution.
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IN QUALITATIVE ANALYSIS OF GROUP 3 CATIONS , COMPLETE THIS TABLE AND WRITE THE CHEMICAL REACTIONS FOR THE IONS THAT OCCURED.
COMPLETE THIS TABLE:
Group IIICations
ConfirmatoryReagent
Result/Observation
SubstanceFormed
Inference
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PLEASE Answer within 20-30 minutes. Thank you!
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#23 and 6
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PART ONE: Preparation of FECNS* Solution
Prepare the two solutions in table 1 by accurately measuring the required volumes of distilled
water and CNS into two labeled test tubes. The absorbance of the solutions must be measured
soon after adding the Fe" solution from a buret.
TABLE 1
Fe
5 ml
5S mL
Solution
Distilled Water
CNS
2 mL
Total Volume
3 ml
2 ml
10 ml
3 mL
10 ml
In this part of the experiment you are to explore what the above quote means. As a
PRELIMINARY Exercise, formulate a hypothesis as to what would happen under each of the
following circumstances:
1. 1ml of 0.0020 M CNS' solution is added to the unused portion of
solution 1 in the test tube
2. One drop of 0.20 M CNS solution is added to the unused portion of
solution 2 in the test tube.
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The spectroscopic data in the table is generated with five solutions of known concentration.
Concentration (M)
0.0133
m=
0.0266
0.0532
0.106
0.213
Absorbance
0.1271
What is the intercept of the linear regression line?
0.08531
0.5388
1.069
Use a spreadsheet program, such as Microsoft Excel, to graph the data points and determine the equation of the best-fit line.
1.954
What is the slope of the linear regression line formed by these points?
M-1
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A chemist received a radioactive sample that is suspected to contain U, 23U and other elements. The authority wants to know the distribution, qualitative and quantitative composition of the sample. Propose with justifications, ONE Surface analysis technique that can be performed on this sample.
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Read the following short piece titled "The
Status of Qualitative Research in
Criminology." by Jody Miller, read pages 69-
72.
Discuss the validity and reliability issues in
relation to qualitative studies.
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CHEMISTRY
RATE WILL BE GIVEN! NO LONG EXPLANATION NEEDED.
PLEASE ANSWER 43-45
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Absorbance
1.40
Beer's Law Plot
1.20
1.00
0.80
0.60
0.40
0.20
0.00
0
10
20
30
40
50
Concentration (M x 105)
D
The slope for the line is 80.23. Use the Beer's Law plot provided to determine the
concentration for a solution with absorbance = 0.5786.
M
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You determine the Mg concentration of a water sample using atomic absorption spectroscopy (AAS). The sample is first diluted: 4.00 mL of the water sample is diluted to a final volume of 25.0 mL. The AAS reading for the diluted sample is 1.755 ppm. What was the Mg concentration of the original water sample, in ppm? (Enter the numerical value without units.)
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Document1 - Word
Search (Alt+Q)
References
Mailings
Review
View
Help
Write the corresponding letters to the following descriptions. Each proposal can be associated with 0 or
1 match and each letter is not necessarily associated with a proposal.
a. [Ar] 4s?
b. 1s 2s2p63s23p3
c. 1s2s2p2
d. [Ne] 3s23ps
e. [Ar] 4s23d10
f. 1s22s!
g. None of those answers
1. I am a halogen
2. I am a transition metal
3. I am alkaline
4. I have exactly 2 single electrons
5. I am the smallest of the atoms presented here
6. I have exactly 3 valence electrons
7.I am the most paramagnetic of the atoms presented here
8. I am the copper
9.I am isoelectronic with Ti2+
IF
cessibility: Good to go
IA
16
SIS
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If Jotaro Kujo measured the amount of current that passes through a sample to measure the amount of analyte in the sample, what kind of method did he use?
Volumetric method
Spectroscopic method
Gravimetric method
Electroanalytical method
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Dangerous Paint Stripper Jessica has a summer job working for the
city parks program. She has been using a cleaner called “Graffiti Gone” to
remove graffiti from the bathrooms. She has to take a lot of breaks, because
the chemical makes her throat burn. It also makes her feel dizzy sometimes,
especially when the bathrooms don’t have very many windows. On the label, she
sees that the cleaner has methylene chloride in it. She feels like she’s
managing to get the work done, but she is worried about feeling dizzy. She
wants to find out more about this chemical, what harm it can cause, and
whether there are safer ways to do this work.
Questions for following story.
1. What went right in this situation?
2. What went wrong in this situation?
3. What steps should be taken in this workplace to make sure employees are
better protected and prepared the next time?
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[References]
Use the References to access important values if needed for this question.
Taking logarithms and antilogarithms is necessary to solve many chemistry problems. For practice, complete the following table, where
N is a number.
In N
log N
26.7
--0.261
0.246
Submit Answer
Retry Entire Group
No more group attempts remain
Visited
eq
req
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A water sample was analyzed for iron content using the iron-phenanthroline method. Using the set of data from Question 15 (as
presented below),
Reagent Blank Absorbance
Absorbance (au)
Reagent Blank Absorbance
0.003
Concentration of Stock Solution: 10 ppm
Volume of Stock
Solution (mL)
Total Volume of
Standard Solution
(mL)
0.50
10.00
1.00
10.00
2.00
10.00
3.00
10.00
4.00
10.00
5.00
10.00
Volume of
Trial
Unknown Solution
(mL)
1
5.00
2
5.00
3
5.00
find the true concentration of Fe2+ of the original sample.
A) 5.12 ppm
B) 2.56 ppm
2.52 ppm
D) 5.05 ppm
Concentration of
Standard Solution
(ppm)
Total Volume of
Unknown Solution
(mL)
10.00
10.00
10.00
Absorbance (au)
0.012
0.132
0.267
0.349
0.428
0.560
Absorbance (au)
0.289
0.296
0.281
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7. Chemical Formula: C3H7NO₂
1H, broad
12
10
2H, broad
Final Answer
8
PPM
6
1H q
A-
3H d
2
0
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If an analytical method relies on a measurable property of an analyte that can be correlated with the amount of the said analyte, what type of analytical method is it?
Oxidative methods
Instrumental methods
Blank Correction methods
Classical methods
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What is the importance of the following analytical methods in chemical analysis?
i. UV-vis spectrophotometry
ii. HPLC
iii. GC
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Give a detailed description of how these both analytical separation protocol will be employed to recover river bodies from heavy metals and particulate matter.
I. Centrifugation
II. Chemical precipitation
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M
Apple Google Disney ESPN Yahoo! Biomedical Careers Program Apple iCloud Yahoo Images Bing Google Wikipedia
COWLv2 |... b D2L
☆
&
G
For the reaction
r
r
Submit Answer
prod03-cnow-owl.cengagenow.com
Fe(s) + 2HCI(aq)→→→FeCl₂(s) + H₂(g)
AH° = -7.4 kJ and AS° = 107.9 J/K
D2L
D2L
D2L
Facebook Twitter LinkedIn
Use the References to access important values if needed for this question.
The Weather Channel Yelp TripAdvisor
b
D2L M G C
The maximum amount of work that could be done when 2.08 moles of Fe(s) react at 286 K, 1 atm is
Assume that AH° and ASº are independent of temperature.
Retry Entire Group 4 more group attempts remaining
kj.
+88
M
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V2
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The spectroscopic data in the table is generated with five solutions of known concentration.
Concentration (M)
0.0179
0.0358
0.0716
0.143
0.286
Absorbance
0.1425
0.1896
0.5722
1.126
2.110
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Why is strict implementation of LQMS (Laboratory Quality Management System) or GLP is necessary ? What are the elements ?
arrow_forward
NO
85
At
RI
Astatin
209967
222.018
117
118
Uus Uuo
Chunoctium
unknown
84
Bi
Po
Pulonium
[2002)
3
116
up Lv
Livermorum nuncium
own [298]
unknown
69
70
Tm
Thulum
168934
Yb
Yicerbium
123055
102
101
Md
No
Mendelevium Nobellum
258.1
259.101
71
Lu
Lutecium
174.967
103
Lr
Lawrencium
[262]
DELL
2015
He
org
Stoichiometry (On Your Own)
Solve the following stoichiometry grams-grams problems:
1)
Using the following equation:
2 NaOH + H₂SO4 → 2 H₂O + Na₂SO4
How many grams of sodium sulfate will be formed if you start with 200 grams of sodium hydroxide and
you have an excess of sulfuric acid?
2)
Using the following equation:
Pb(SO4)2 + 4 LINO3 → Pb(NO3)4 + 2 Li₂SO4
How many grams of lithium nitrate will be needed to make 250 grams of lithium sulfate, assuming that
you have an adequate amount of lead (IV) sulfate to do the reaction?
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Explain Qualitative Chemistry and Quantitative Chemistry .
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The best fit curve line to an absorbance vs. concentration plot for standard solutions of a dye
has a slope of 0.1815 mL/mg and intercept of 0.0477. A sample solution prepared of the same
dye has an absorbance of 0.464 at the wavelength used to establish the Beer's law plot. What
is the concentration of dye in the prepared solution?
Select one:
O a. 0.132 mg/mL
b. 2.29 mg/mL
O c. 0.464 mg/mL
O d. 2.82 mg/mL
e. 0.0365 mg/mL
Next page
Law Tutorial Part 2
Jump to...
Exp #9 - Laboratory Practical►
Worksheet
étv A
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The following Absorbance vs concentration of nitrite graph is obtained for a set of data:
Absorbance Vs Concentration y = 1.6628x+0.0373
R? = 0.9893
1.8
1.6
1.4
1.2
1
0.8
0.6
0.4
0.2
0.2
0.4
0.6
0.8
1
Concentration of nitrite (mg/L)
Determine the concentration of unknown solution for which the absorbance is determined
as 0.69
A. More data is required
В. 0.69
С. 0.65
D. 0.39
Absorbance
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A direct ELISA experiment was done to determine the amount of protein present in a sample. A standard curve was prepared by plotting log Absorbance versus log concentration of protein in (ng/mL). The equation of the line is Y= 0.895 X -1.25. If an unknown protein shows an absorbance of 1.23. Calculate the concentration of this protein in the sample in (ng/mL).
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how do i find x?
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CHEMISTRY
RATE WILL BE GIVEN! NO LONG EXPLANATION NEEDED.
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Explain the importance of analytical chemistry in medicine. As well as:
1. Chemical chemistry
2. Medicinal chemistry
3. Pharmacology
4. Toxicology
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Which of the hypothetic equations below is incorrectly balanced:
a.
2 X + 3 Y2Z4 → 1 X2 (Z4)3 + 6 Y2
b.
2 D2F4G + 5 G2 → 4 DG2 + 4 F2G
c.
2 KLMN3 → 1 K2MN3 + 1 MN2 + 1 L2N
d.
1 J12B22C11 → 12 J + 11 B2C
e.
1 ABC4 → 1 AB + 2 C
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The concentration of methylene blue in the sample is estimated through (select the correct)
options:
refractive index measurement (refractometry).
turbidity measurement (turbidimetry).
absorbance measurement (spectrophotometry).
titration with 2% HCl solution.
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