Which of the following is incorrect: General steps in qualitative analysis include: Method selection, sampling, sample processing, calibration & measurement. b. Quantitative analytical methods include: gravimetric, volumetric, spectroscopic and electroanalytical methods. c. The first step in sample processing is sample preparation. d. Replication improves the quality of results and their reliability. e. In quantitative analysis there should be a direct proportionality between a measured property and the concentration or amount of substance. Please fill in the spa ces one of the following characters (a or b or c or d or e)

Which of the following is incorrect: General steps in qualitative analysis include: Method selection, sampling, sample processing, calibration & measurement. b. Quantitative analytical methods include: gravimetric, volumetric, spectroscopic and electroanalytical methods. c. The first step in sample processing is sample preparation. d. Replication improves the quality of results and their reliability. e. In quantitative analysis there should be a direct proportionality between a measured property and the concentration or amount of substance. Please fill in the spa ces one of the following characters (a or b or c or d or e)

Chemistry

10th Edition

ISBN:9781305957404

Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Chapter1: Chemical Foundations

Section: Chapter Questions

Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...

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You were tasked to separate the components of a mixture containing silica, sodium chloride and charcoal. TNāCI dissolves in water while silica and charcoal are not water-soluble. Only charcoal dissolves in carbon disulfide. a. Write a short experimental procedure to carry out the separation of the mixture. b. Given the following data, determine the percentage of charcoal, sodium chloride and silica. Mass (g) Mass of beaker 100.000 Mass of beaker + mixture 110.000 mass of evaporating dish 62.000 mass of evaporating dish + solid after evaporation of water 65.000 Mass of beaker + charcoal + silica after evaporation of excess water 117.000 mass of beaker + silica after decanting dissolved charcoal and drying 113.545
What is an analytical balance?
12. This type of analysis means that the amount of some constituents were determined. Complete analysis a. b. Ultimate analysis с. Partial analysis d. Single-component analysis 13. This process is one way of reducing occluded particles and mechanical entrapment impurities. a. Washing b. Heating c. Stirring d. Digestion
What kind of mixture of substance has Distillation and Chromatography has?
Laboratory Questions (edited) Put answers on a separate piece of paper and provide enough room for instructor comments. 1. Based on the procedure of this experiment, explain the effect of the following actions on the assessed masses of the components indicated. Where indicated, also address the effect on the percent recovery (Part D of the experiment). The choices include: lower, higher, no effect or could be higher or lower. If the answer could be higher or lower, provide a detailed explanation. a) Sublimation of NH4CI was not complete. How does this situation affect the calculated mass of NH4CI and the percent recovery? b) While decanting, some of the salty water was spilled onto the lab bench. How does this situation affect the calculated mass of NaCl and the percent recovery? c) While decanting, some of the sand was inadvertently transferred to the second evaporating dish. How does this situation affect the masses of NaCl and sand (SiO2) and the percent recovery? d) While weighing…
2. In your experiment today will the percent yeild of calcium carbonate be higher, lower, or unchanged if: a. The torn-off-corner of the filter paper is discarded instead of placing it in the cone. Explain. b. The graduated cylinder is not rinsed after transferring the sodium carbonate to the beaker. Explain. c. The calcium carbonate precipitate is weighed today instead of the next lab period? Explain.
alculate the approximate volume of the vinegar sample needed for the analyses (Part A.1). Brand of vinegar or unknown no. Colauita tof White Wine Trial 1 1122809 Trial 2 Trial 1 Trial 2 e Guia 112.280g (12.822g 112.796 115 565 lis.9 1. Mass of flask (g) l15.603 2. Mass of flask + vinegar (g) 2.496 3.323 2,743 2,749 3. Mass of vinegar (g) B. Analysis of Vinegar Sample 2mL 7.5 23mL 32.コ 1. Buret reading of NaOH, initial (mL) 5.25mL 13ML amL 2. Buret reading of NaOH, final (mL) 33,3 31.2 1. Volume of NaOH used (mL) 2! mL a7.45 me 20.3 32.2 o i135 • 004 1 Molar concentration of NaOH (mol/L) Oi135 • 00 3 1003 , 063 5. Moles of NaOH added (mol) 6. Moles of CH,COOH in vinegar (mol) 7. Mass of CH,COOH in vinegar (g) 8. Percent by mass of CH,COOH in vinegar (%) 9. Average percent by mass of CH,COOH in vinegar (%) Calculations for Trial 1 of the first vinegar sample on next page. Experiment 10 137
When we need sample preparation for analysis? use your own words to explain
correct statement is? a. Safety glasses should be worn in a laboratory at all times to decrease the likelihood of eye injury. b. Safety shower would immediately be used if your clothing caught fire or if a large chemical spill had occurred on your clothing. O c. It is not allowed to smoke in the lab. o d. If you have accidentally broken a test tube and spilled a chemical on the table, Caution your lab partners to avoid the area while you inform the teacher of the small accident. e. Use the eye-wash fountain ,then notify the instructor if a chemical gets in the eye.
I don't know how to calculate parts a, b &c of question 9.
The following volumes of 0.000300 M SCN are diluted to 15.00 mL. Determine the concentration of SCN in each sample after dilution. These values will be used during the experiment. To enter exponential values, use the format 1.0e-5. Sample 0.000300 M SCN (mL) [SCN'] (M) 1 1.50 3.50 7.00 4 10.00 3.