(a) Interpretation: The product of the given reductive amination reaction is to be drawn. Concept introduction: Amines are the derivatives of ammonia consisting of a nitrogen atom with the lone pair of electrons. They are basic compounds. Reductive amination comprises transformation of the carbonyl group of ketone or aldehyde to an imine intermediate, which leads to the formation of an amine. The synthesis of the products relies upon the type of reactants and reagents that are used during the reactions. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

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Answer 1

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Definition Definition Organic compounds that have a carbonyl group, C=O, as their functional group. The carbonyl group in aldehydes is placed at the end of the molecular structure, which means the C=O is attached to one hydrogen atom and an alkyl group or a benzene ring. Just like all the other homologous series in organic chemistry, the naming of aldehydes uses the suffix “-al”. The general molecular formula is C n H 2n O.

Chapter 25, Problem 25.50P

Interpretation Introduction

(a)

Interpretation: The product of the given reductive amination reaction is to be drawn.

Concept introduction: Amines are the derivatives of ammonia consisting of a nitrogen atom with the lone pair of electrons. They are basic compounds. Reductive amination comprises transformation of the carbonyl group of ketone or aldehyde to an imine intermediate, which leads to the formation of an amine. The synthesis of the products relies upon the type of reactants and reagents that are used during the reactions. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

Interpretation Introduction

(b)

Interpretation: The product of the given reductive amination reaction is to be drawn.

Concept introduction: Amines are the derivatives of ammonia consisting of a nitrogen atom with the lone pair of electrons. They are basic compounds. Reductive amination comprises transformation of the carbonyl group of ketone or aldehyde to an imine intermediate, which leads to the formation of an amine. The synthesis of the products relies upon the type of reactants and reagents that are used during the reactions. The reagents perform numerous functions in reactions like proton abstraction, oxidation.

Interpretation Introduction

(c)

Interpretation: The product of the given reductive amination reaction is to be drawn.

Concept introduction: Amines are the derivatives of ammonia consisting of a nitrogen atom with the lone pair of electrons. They are basic compounds. Reductive amination comprises transformation of the carbonyl group of ketone or aldehyde to an imine intermediate, which leads to the formation of an amine. The synthesis of the products relies upon the type of reactants and reagents that are used during the reactions. The reagents perform numerous functions in reactions like proton abstraction, oxidation.

Interpretation Introduction

(d)

Interpretation: The product of the given reductive amination reaction is to be drawn.

Concept introduction: Amines are the derivatives of ammonia consisting of a nitrogen atom with the lone pair of electrons. They are basic compounds. Reductive amination comprises transformation of the carbonyl group of keto acids to an imine intermediate, which leads to the formation of an amine. The synthesis of the products relies upon the type of reactants and reagents that are used during the reactions. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

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(a 4 shows scanning electron microscope (SEM) images of extruded actions of packing bed for two capillary columns of different diameters, al 750 (bottom image) and b) 30-μm-i.d. Both columns are packed with the same stationary phase, spherical particles with 1-um diameter. A) When the columns were prepared, the figure shows that the column with the larger diameter has more packing irregularities. Explain this observation. B) Predict what affect this should have on band broadening and discuss your prediction using the van Deemter terms. C) Does this figure support your explanations in application question 33? Explain why or why not and make any changes in your answers in light of this figure. Figure 4 SEM images of sections of packed columns for a) 750 and b) 30-um-i.d. capillary columns.³

fcrip = ↓ bandwidth Il temp 32. What impact (increase, decrease, or no change) does each of the following conditions have on the individual components of the van Deemter equation and consequently, band broadening? Increase temperature Longer column Using a gas mobile phase instead of liquid Smaller particle stationary phase Multiple Paths Diffusion Mass Transfer

34. Figure 3 shows Van Deemter plots for a solute molecule using different column inner diameters (i.d.). A) Predict whether decreasing the column inner diameters increase or decrease bandwidth. B) Predict which van Deemter equation coefficient (A, B, or C) has the greatest effect on increasing or decreasing bandwidth as a function of i.d. and justify your answer. Figure 3 Van Deemter plots for hydroquinone using different column inner diameters (i.d. in μm). The data was obtained from liquid chromatography experiments using fused-silica capillary columns packed with 1.0-μm particles. 35 20 H(um) 큰 20 15 90 0+ 1500 100 75 550 01 02 594 05 μ(cm/sec) 30 15 10

Answer 2

Question

Definition Definition Organic compounds that have a carbonyl group, C=O, as their functional group. The carbonyl group in aldehydes is placed at the end of the molecular structure, which means the C=O is attached to one hydrogen atom and an alkyl group or a benzene ring. Just like all the other homologous series in organic chemistry, the naming of aldehydes uses the suffix “-al”. The general molecular formula is C n H 2n O.

Chapter 25, Problem 25.50P

Interpretation Introduction

(a)

Interpretation: The product of the given reductive amination reaction is to be drawn.

Concept introduction: Amines are the derivatives of ammonia consisting of a nitrogen atom with the lone pair of electrons. They are basic compounds. Reductive amination comprises transformation of the carbonyl group of ketone or aldehyde to an imine intermediate, which leads to the formation of an amine. The synthesis of the products relies upon the type of reactants and reagents that are used during the reactions. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

Interpretation Introduction

(b)

Interpretation: The product of the given reductive amination reaction is to be drawn.

Concept introduction: Amines are the derivatives of ammonia consisting of a nitrogen atom with the lone pair of electrons. They are basic compounds. Reductive amination comprises transformation of the carbonyl group of ketone or aldehyde to an imine intermediate, which leads to the formation of an amine. The synthesis of the products relies upon the type of reactants and reagents that are used during the reactions. The reagents perform numerous functions in reactions like proton abstraction, oxidation.

Interpretation Introduction

(c)

Interpretation: The product of the given reductive amination reaction is to be drawn.

Concept introduction: Amines are the derivatives of ammonia consisting of a nitrogen atom with the lone pair of electrons. They are basic compounds. Reductive amination comprises transformation of the carbonyl group of ketone or aldehyde to an imine intermediate, which leads to the formation of an amine. The synthesis of the products relies upon the type of reactants and reagents that are used during the reactions. The reagents perform numerous functions in reactions like proton abstraction, oxidation.

Interpretation Introduction

(d)

Interpretation: The product of the given reductive amination reaction is to be drawn.

Concept introduction: Amines are the derivatives of ammonia consisting of a nitrogen atom with the lone pair of electrons. They are basic compounds. Reductive amination comprises transformation of the carbonyl group of keto acids to an imine intermediate, which leads to the formation of an amine. The synthesis of the products relies upon the type of reactants and reagents that are used during the reactions. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

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Answer 3

Question

Definition Definition Organic compounds that have a carbonyl group, C=O, as their functional group. The carbonyl group in aldehydes is placed at the end of the molecular structure, which means the C=O is attached to one hydrogen atom and an alkyl group or a benzene ring. Just like all the other homologous series in organic chemistry, the naming of aldehydes uses the suffix “-al”. The general molecular formula is C n H 2n O.

Chapter 25, Problem 25.50P

Interpretation Introduction

(a)

Interpretation: The product of the given reductive amination reaction is to be drawn.

Concept introduction: Amines are the derivatives of ammonia consisting of a nitrogen atom with the lone pair of electrons. They are basic compounds. Reductive amination comprises transformation of the carbonyl group of ketone or aldehyde to an imine intermediate, which leads to the formation of an amine. The synthesis of the products relies upon the type of reactants and reagents that are used during the reactions. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

Interpretation Introduction

(b)

Interpretation: The product of the given reductive amination reaction is to be drawn.

Concept introduction: Amines are the derivatives of ammonia consisting of a nitrogen atom with the lone pair of electrons. They are basic compounds. Reductive amination comprises transformation of the carbonyl group of ketone or aldehyde to an imine intermediate, which leads to the formation of an amine. The synthesis of the products relies upon the type of reactants and reagents that are used during the reactions. The reagents perform numerous functions in reactions like proton abstraction, oxidation.

Interpretation Introduction

(c)

Interpretation: The product of the given reductive amination reaction is to be drawn.

Concept introduction: Amines are the derivatives of ammonia consisting of a nitrogen atom with the lone pair of electrons. They are basic compounds. Reductive amination comprises transformation of the carbonyl group of ketone or aldehyde to an imine intermediate, which leads to the formation of an amine. The synthesis of the products relies upon the type of reactants and reagents that are used during the reactions. The reagents perform numerous functions in reactions like proton abstraction, oxidation.

Interpretation Introduction

(d)

Interpretation: The product of the given reductive amination reaction is to be drawn.

Concept introduction: Amines are the derivatives of ammonia consisting of a nitrogen atom with the lone pair of electrons. They are basic compounds. Reductive amination comprises transformation of the carbonyl group of keto acids to an imine intermediate, which leads to the formation of an amine. The synthesis of the products relies upon the type of reactants and reagents that are used during the reactions. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

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Answer 4

Question

Definition Definition Organic compounds that have a carbonyl group, C=O, as their functional group. The carbonyl group in aldehydes is placed at the end of the molecular structure, which means the C=O is attached to one hydrogen atom and an alkyl group or a benzene ring. Just like all the other homologous series in organic chemistry, the naming of aldehydes uses the suffix “-al”. The general molecular formula is C n H 2n O.

Chapter 25, Problem 25.50P

Interpretation Introduction

(a)

Interpretation: The product of the given reductive amination reaction is to be drawn.

Concept introduction: Amines are the derivatives of ammonia consisting of a nitrogen atom with the lone pair of electrons. They are basic compounds. Reductive amination comprises transformation of the carbonyl group of ketone or aldehyde to an imine intermediate, which leads to the formation of an amine. The synthesis of the products relies upon the type of reactants and reagents that are used during the reactions. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

Interpretation Introduction

(b)

Interpretation: The product of the given reductive amination reaction is to be drawn.

Concept introduction: Amines are the derivatives of ammonia consisting of a nitrogen atom with the lone pair of electrons. They are basic compounds. Reductive amination comprises transformation of the carbonyl group of ketone or aldehyde to an imine intermediate, which leads to the formation of an amine. The synthesis of the products relies upon the type of reactants and reagents that are used during the reactions. The reagents perform numerous functions in reactions like proton abstraction, oxidation.

Interpretation Introduction

(c)

Interpretation: The product of the given reductive amination reaction is to be drawn.

Concept introduction: Amines are the derivatives of ammonia consisting of a nitrogen atom with the lone pair of electrons. They are basic compounds. Reductive amination comprises transformation of the carbonyl group of ketone or aldehyde to an imine intermediate, which leads to the formation of an amine. The synthesis of the products relies upon the type of reactants and reagents that are used during the reactions. The reagents perform numerous functions in reactions like proton abstraction, oxidation.

Interpretation Introduction

(d)

Interpretation: The product of the given reductive amination reaction is to be drawn.

Concept introduction: Amines are the derivatives of ammonia consisting of a nitrogen atom with the lone pair of electrons. They are basic compounds. Reductive amination comprises transformation of the carbonyl group of keto acids to an imine intermediate, which leads to the formation of an amine. The synthesis of the products relies upon the type of reactants and reagents that are used during the reactions. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

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Answer 5

Chapter 25, Problem 25.50P

Interpretation Introduction

(a)

Interpretation: The product of the given reductive amination reaction is to be drawn.

Concept introduction: Amines are the derivatives of ammonia consisting of a nitrogen atom with the lone pair of electrons. They are basic compounds. Reductive amination comprises transformation of the carbonyl group of ketone or aldehyde to an imine intermediate, which leads to the formation of an amine. The synthesis of the products relies upon the type of reactants and reagents that are used during the reactions. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

Interpretation Introduction

(b)

Interpretation: The product of the given reductive amination reaction is to be drawn.

Concept introduction: Amines are the derivatives of ammonia consisting of a nitrogen atom with the lone pair of electrons. They are basic compounds. Reductive amination comprises transformation of the carbonyl group of ketone or aldehyde to an imine intermediate, which leads to the formation of an amine. The synthesis of the products relies upon the type of reactants and reagents that are used during the reactions. The reagents perform numerous functions in reactions like proton abstraction, oxidation.

Interpretation Introduction

(c)

Interpretation: The product of the given reductive amination reaction is to be drawn.

Concept introduction: Amines are the derivatives of ammonia consisting of a nitrogen atom with the lone pair of electrons. They are basic compounds. Reductive amination comprises transformation of the carbonyl group of ketone or aldehyde to an imine intermediate, which leads to the formation of an amine. The synthesis of the products relies upon the type of reactants and reagents that are used during the reactions. The reagents perform numerous functions in reactions like proton abstraction, oxidation.

Interpretation Introduction

(d)

Interpretation: The product of the given reductive amination reaction is to be drawn.

Concept introduction: Amines are the derivatives of ammonia consisting of a nitrogen atom with the lone pair of electrons. They are basic compounds. Reductive amination comprises transformation of the carbonyl group of keto acids to an imine intermediate, which leads to the formation of an amine. The synthesis of the products relies upon the type of reactants and reagents that are used during the reactions. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

Answer 6

Chapter 25, Problem 25.50P

Interpretation Introduction

(a)

Interpretation: The product of the given reductive amination reaction is to be drawn.

Concept introduction: Amines are the derivatives of ammonia consisting of a nitrogen atom with the lone pair of electrons. They are basic compounds. Reductive amination comprises transformation of the carbonyl group of ketone or aldehyde to an imine intermediate, which leads to the formation of an amine. The synthesis of the products relies upon the type of reactants and reagents that are used during the reactions. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

Answer 7

Chapter 25, Problem 25.50P

Interpretation Introduction

(a)

Interpretation: The product of the given reductive amination reaction is to be drawn.

Concept introduction: Amines are the derivatives of ammonia consisting of a nitrogen atom with the lone pair of electrons. They are basic compounds. Reductive amination comprises transformation of the carbonyl group of ketone or aldehyde to an imine intermediate, which leads to the formation of an amine. The synthesis of the products relies upon the type of reactants and reagents that are used during the reactions. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

Answer 8

Interpretation Introduction

(b)

Interpretation: The product of the given reductive amination reaction is to be drawn.

Concept introduction: Amines are the derivatives of ammonia consisting of a nitrogen atom with the lone pair of electrons. They are basic compounds. Reductive amination comprises transformation of the carbonyl group of ketone or aldehyde to an imine intermediate, which leads to the formation of an amine. The synthesis of the products relies upon the type of reactants and reagents that are used during the reactions. The reagents perform numerous functions in reactions like proton abstraction, oxidation.

Answer 9

Interpretation Introduction

(b)

Interpretation: The product of the given reductive amination reaction is to be drawn.

Concept introduction: Amines are the derivatives of ammonia consisting of a nitrogen atom with the lone pair of electrons. They are basic compounds. Reductive amination comprises transformation of the carbonyl group of ketone or aldehyde to an imine intermediate, which leads to the formation of an amine. The synthesis of the products relies upon the type of reactants and reagents that are used during the reactions. The reagents perform numerous functions in reactions like proton abstraction, oxidation.

Answer 10

Interpretation Introduction

(c)

Interpretation: The product of the given reductive amination reaction is to be drawn.

Concept introduction: Amines are the derivatives of ammonia consisting of a nitrogen atom with the lone pair of electrons. They are basic compounds. Reductive amination comprises transformation of the carbonyl group of ketone or aldehyde to an imine intermediate, which leads to the formation of an amine. The synthesis of the products relies upon the type of reactants and reagents that are used during the reactions. The reagents perform numerous functions in reactions like proton abstraction, oxidation.

Answer 11

Interpretation Introduction

(c)

Interpretation: The product of the given reductive amination reaction is to be drawn.

Concept introduction: Amines are the derivatives of ammonia consisting of a nitrogen atom with the lone pair of electrons. They are basic compounds. Reductive amination comprises transformation of the carbonyl group of ketone or aldehyde to an imine intermediate, which leads to the formation of an amine. The synthesis of the products relies upon the type of reactants and reagents that are used during the reactions. The reagents perform numerous functions in reactions like proton abstraction, oxidation.

Answer 12

Interpretation Introduction

(d)

Interpretation: The product of the given reductive amination reaction is to be drawn.

Concept introduction: Amines are the derivatives of ammonia consisting of a nitrogen atom with the lone pair of electrons. They are basic compounds. Reductive amination comprises transformation of the carbonyl group of keto acids to an imine intermediate, which leads to the formation of an amine. The synthesis of the products relies upon the type of reactants and reagents that are used during the reactions. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

Answer 13

Interpretation Introduction

(d)

Interpretation: The product of the given reductive amination reaction is to be drawn.

Concept introduction: Amines are the derivatives of ammonia consisting of a nitrogen atom with the lone pair of electrons. They are basic compounds. Reductive amination comprises transformation of the carbonyl group of keto acids to an imine intermediate, which leads to the formation of an amine. The synthesis of the products relies upon the type of reactants and reagents that are used during the reactions. The reagents perform numerous functions in reactions like proton abstraction, oxidation, reduction, catalysis, and dehydrogenation.

Answer 14

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Answer 16

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Answer 17

Ch. 25 - Prob. 25.1P Ch. 25 - Prob. 25.2P Ch. 25 - Prob. 25.3P Ch. 25 - Prob. 25.4P Ch. 25 - Prob. 25.5P Ch. 25 - Prob. 25.6P Ch. 25 - Problem 25.7 Draw the product of each...Ch. 25 - Prob. 25.8P Ch. 25 - Prob. 25.9P Ch. 25 - Prob. 25.10P

Solution Summary: The author explains the product of the given reductive amination reaction is shown in Figure 1.

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