(a) Interpretation: The mole percent of the each given compound in the mixture is to be stated. Concept introduction: NMR spectroscopy is a technique used to determine a unique structure of the compounds. It identifies the carbon-hydrogen bonding of an organic compound. A hydrogen atom is known as a proton in the NMR spectroscopy. The number of NMR signal in a compound is equal to the number of chemically non-equivalent protons present in that compound. The more the shielded proton lesser will be its chemical shift value and the corresponding signal will be produced at the right-hand side or lower frequency region or vice versa.

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Answer 1

Question

Chapter 13, Problem 13.12P

Interpretation Introduction

(a)

Interpretation:

The mole percent of the each given compound in the mixture is to be stated.

Concept introduction:

NMR spectroscopy is a technique used to determine a unique structure of the compounds. It identifies the carbon-hydrogen bonding of an organic compound. A hydrogen atom is known as a proton in the NMR spectroscopy.

The number of NMR signal in a compound is equal to the number of chemically non-equivalent protons present in that compound. The more the shielded proton lesser will be its chemical shift value and the corresponding signal will be produced at the right-hand side or lower frequency region or vice versa.

Interpretation Introduction

(b)

Interpretation:

Among 1 mole percent CH3I impurity in (CH3)3C−Br, and 1 mole percent (CH3)3C−Br impurity in CH3I, the one which is more easily detected by NMR is to be stated with an explanation.

Concept introduction:

NMR spectroscopy is a technique used to determine a unique structure of the compounds. It identifies the carbon-hydrogen bonding of an organic compound. A hydrogen atom is known as a proton in the NMR spectroscopy.

The number of NMR signal in a compound is equal to the number of chemically non-equivalent protons present in that compound. The more the shielded proton lesser will be its chemical shift value and the corresponding signal will be produced at the right-hand side or lower frequency region or vice versa.

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Answer 2

Question

Chapter 13, Problem 13.12P

Interpretation Introduction

(a)

Interpretation:

The mole percent of the each given compound in the mixture is to be stated.

Concept introduction:

NMR spectroscopy is a technique used to determine a unique structure of the compounds. It identifies the carbon-hydrogen bonding of an organic compound. A hydrogen atom is known as a proton in the NMR spectroscopy.

The number of NMR signal in a compound is equal to the number of chemically non-equivalent protons present in that compound. The more the shielded proton lesser will be its chemical shift value and the corresponding signal will be produced at the right-hand side or lower frequency region or vice versa.

Interpretation Introduction

(b)

Interpretation:

Among 1 mole percent CH3I impurity in (CH3)3C−Br, and 1 mole percent (CH3)3C−Br impurity in CH3I, the one which is more easily detected by NMR is to be stated with an explanation.

Concept introduction:

NMR spectroscopy is a technique used to determine a unique structure of the compounds. It identifies the carbon-hydrogen bonding of an organic compound. A hydrogen atom is known as a proton in the NMR spectroscopy.

The number of NMR signal in a compound is equal to the number of chemically non-equivalent protons present in that compound. The more the shielded proton lesser will be its chemical shift value and the corresponding signal will be produced at the right-hand side or lower frequency region or vice versa.

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Answer 3

Question

Chapter 13, Problem 13.12P

Interpretation Introduction

(a)

Interpretation:

The mole percent of the each given compound in the mixture is to be stated.

Concept introduction:

NMR spectroscopy is a technique used to determine a unique structure of the compounds. It identifies the carbon-hydrogen bonding of an organic compound. A hydrogen atom is known as a proton in the NMR spectroscopy.

The number of NMR signal in a compound is equal to the number of chemically non-equivalent protons present in that compound. The more the shielded proton lesser will be its chemical shift value and the corresponding signal will be produced at the right-hand side or lower frequency region or vice versa.

Interpretation Introduction

(b)

Interpretation:

Among 1 mole percent CH3I impurity in (CH3)3C−Br, and 1 mole percent (CH3)3C−Br impurity in CH3I, the one which is more easily detected by NMR is to be stated with an explanation.

Concept introduction:

NMR spectroscopy is a technique used to determine a unique structure of the compounds. It identifies the carbon-hydrogen bonding of an organic compound. A hydrogen atom is known as a proton in the NMR spectroscopy.

The number of NMR signal in a compound is equal to the number of chemically non-equivalent protons present in that compound. The more the shielded proton lesser will be its chemical shift value and the corresponding signal will be produced at the right-hand side or lower frequency region or vice versa.

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Answer 4

Question

Chapter 13, Problem 13.12P

Interpretation Introduction

(a)

Interpretation:

The mole percent of the each given compound in the mixture is to be stated.

Concept introduction:

NMR spectroscopy is a technique used to determine a unique structure of the compounds. It identifies the carbon-hydrogen bonding of an organic compound. A hydrogen atom is known as a proton in the NMR spectroscopy.

The number of NMR signal in a compound is equal to the number of chemically non-equivalent protons present in that compound. The more the shielded proton lesser will be its chemical shift value and the corresponding signal will be produced at the right-hand side or lower frequency region or vice versa.

Interpretation Introduction

(b)

Interpretation:

Among 1 mole percent CH3I impurity in (CH3)3C−Br, and 1 mole percent (CH3)3C−Br impurity in CH3I, the one which is more easily detected by NMR is to be stated with an explanation.

Concept introduction:

NMR spectroscopy is a technique used to determine a unique structure of the compounds. It identifies the carbon-hydrogen bonding of an organic compound. A hydrogen atom is known as a proton in the NMR spectroscopy.

The number of NMR signal in a compound is equal to the number of chemically non-equivalent protons present in that compound. The more the shielded proton lesser will be its chemical shift value and the corresponding signal will be produced at the right-hand side or lower frequency region or vice versa.

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Answer 5

Chapter 13, Problem 13.12P

Interpretation Introduction

(a)

Interpretation:

The mole percent of the each given compound in the mixture is to be stated.

Concept introduction:

NMR spectroscopy is a technique used to determine a unique structure of the compounds. It identifies the carbon-hydrogen bonding of an organic compound. A hydrogen atom is known as a proton in the NMR spectroscopy.

The number of NMR signal in a compound is equal to the number of chemically non-equivalent protons present in that compound. The more the shielded proton lesser will be its chemical shift value and the corresponding signal will be produced at the right-hand side or lower frequency region or vice versa.

Interpretation Introduction

(b)

Interpretation:

Among 1 mole percent CH3I impurity in (CH3)3C−Br, and 1 mole percent (CH3)3C−Br impurity in CH3I, the one which is more easily detected by NMR is to be stated with an explanation.

Concept introduction:

NMR spectroscopy is a technique used to determine a unique structure of the compounds. It identifies the carbon-hydrogen bonding of an organic compound. A hydrogen atom is known as a proton in the NMR spectroscopy.

The number of NMR signal in a compound is equal to the number of chemically non-equivalent protons present in that compound. The more the shielded proton lesser will be its chemical shift value and the corresponding signal will be produced at the right-hand side or lower frequency region or vice versa.

Answer 6

Chapter 13, Problem 13.12P

Interpretation Introduction

(a)

Interpretation:

The mole percent of the each given compound in the mixture is to be stated.

Concept introduction:

NMR spectroscopy is a technique used to determine a unique structure of the compounds. It identifies the carbon-hydrogen bonding of an organic compound. A hydrogen atom is known as a proton in the NMR spectroscopy.

The number of NMR signal in a compound is equal to the number of chemically non-equivalent protons present in that compound. The more the shielded proton lesser will be its chemical shift value and the corresponding signal will be produced at the right-hand side or lower frequency region or vice versa.

Answer 7

Chapter 13, Problem 13.12P

Interpretation Introduction

(a)

Interpretation:

The mole percent of the each given compound in the mixture is to be stated.

Concept introduction:

NMR spectroscopy is a technique used to determine a unique structure of the compounds. It identifies the carbon-hydrogen bonding of an organic compound. A hydrogen atom is known as a proton in the NMR spectroscopy.

The number of NMR signal in a compound is equal to the number of chemically non-equivalent protons present in that compound. The more the shielded proton lesser will be its chemical shift value and the corresponding signal will be produced at the right-hand side or lower frequency region or vice versa.

Answer 8

Interpretation Introduction

(b)

Interpretation:

Among 1 mole percent CH3I impurity in (CH3)3C−Br, and 1 mole percent (CH3)3C−Br impurity in CH3I, the one which is more easily detected by NMR is to be stated with an explanation.

Concept introduction:

NMR spectroscopy is a technique used to determine a unique structure of the compounds. It identifies the carbon-hydrogen bonding of an organic compound. A hydrogen atom is known as a proton in the NMR spectroscopy.

The number of NMR signal in a compound is equal to the number of chemically non-equivalent protons present in that compound. The more the shielded proton lesser will be its chemical shift value and the corresponding signal will be produced at the right-hand side or lower frequency region or vice versa.

Answer 9

Interpretation Introduction

(b)

Interpretation:

Among 1 mole percent CH3I impurity in (CH3)3C−Br, and 1 mole percent (CH3)3C−Br impurity in CH3I, the one which is more easily detected by NMR is to be stated with an explanation.

Concept introduction:

NMR spectroscopy is a technique used to determine a unique structure of the compounds. It identifies the carbon-hydrogen bonding of an organic compound. A hydrogen atom is known as a proton in the NMR spectroscopy.

The number of NMR signal in a compound is equal to the number of chemically non-equivalent protons present in that compound. The more the shielded proton lesser will be its chemical shift value and the corresponding signal will be produced at the right-hand side or lower frequency region or vice versa.

Answer 10

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Answer 11

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Answer 12

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Answer 13

Ch. 13 - Prob. 13.1P Ch. 13 - Prob. 13.2P Ch. 13 - Prob. 13.3P Ch. 13 - Prob. 13.4P Ch. 13 - Prob. 13.5P Ch. 13 - Prob. 13.6P Ch. 13 - Prob. 13.7P Ch. 13 - Prob. 13.8P Ch. 13 - Prob. 13.9P Ch. 13 - Prob. 13.10P

Solution Summary: The author explains that NMR spectroscopy identifies the carbon-hydrogen bonding of an organic compound.

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Chapter 13 Solutions