DMTO glass bead NH NMe2 1) in%CHCA 2Cl2 2) Ph HN- N reagent structures 'N Cl3C OH & names -Ń DMTO -Ń TCA tetrazole 2,6-lutidine NC i-Pr `N- (dABZ) CH3CN -Pr 4) 1% TCA in CH2Cl2 5) dCBz, tetrazole 6) 12, H2O, 2,6-lutidine 7) 1% TCA in CH2Cl2 8) dT, tetrazole 9) 12, H2O, 2,6-lutidine 10) 1% TCA in CH2Cl₂ 11) dABz, tetrazole 12) 12, H2O, 2,6-lutidine 13) 1% TCA in CH2Cl2 14) Conc. NH3 3) 12, H₂O, 2,6-lutidine
DMTO glass bead NH NMe2 1) in%CHCA 2Cl2 2) Ph HN- N reagent structures 'N Cl3C OH & names -Ń DMTO -Ń TCA tetrazole 2,6-lutidine NC i-Pr `N- (dABZ) CH3CN -Pr 4) 1% TCA in CH2Cl2 5) dCBz, tetrazole 6) 12, H2O, 2,6-lutidine 7) 1% TCA in CH2Cl2 8) dT, tetrazole 9) 12, H2O, 2,6-lutidine 10) 1% TCA in CH2Cl₂ 11) dABz, tetrazole 12) 12, H2O, 2,6-lutidine 13) 1% TCA in CH2Cl2 14) Conc. NH3 3) 12, H₂O, 2,6-lutidine
Chapter10: Reconstitution Of Powdered Drugs
Section: Chapter Questions
Problem 11SST
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Transcribed Image Text:DMTO
glass
bead
NH
NMe2
1) in%CHCA
2Cl2
2)
Ph
HN-
N
reagent
structures
'N
Cl3C OH
& names
-Ń
DMTO
-Ń
TCA
tetrazole
2,6-lutidine
NC
i-Pr
`N-
(dABZ)
CH3CN
-Pr
4) 1% TCA in CH2Cl2
5) dCBz, tetrazole
6) 12, H2O, 2,6-lutidine
7) 1% TCA in CH2Cl2
8) dT, tetrazole
9) 12, H2O, 2,6-lutidine
10) 1% TCA in CH2Cl₂
11) dABz, tetrazole
12) 12, H2O, 2,6-lutidine
13) 1% TCA in CH2Cl2
14) Conc. NH3
3) 12, H₂O,
2,6-lutidine
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