Please complete these blanks need that asap Acid Catalyzed Aromatization of Carvonecalculations. Show your calculations (except the calculation of formula weights) in the spaceComplete the following table. Include density only where needed for carrying out thebelow the table. Each calculation should be done in a neat and easy-to-follow manner. Allunits should be included and significant figures should be given close attention.H2SO4(aq)HF.W.amount1.00 mLmg Theoretical10.0 mL 6.0 MmmolesTheoreticaldensityMass of rb flask 30.79_ gMass of rb flask plus product 32.65gMass of productmg% Yield of product_

Step 1: Volume of carvone = 1.00 mLdensity of carvone = 0.959 g/mLMass of carvone = density×volume…

Answered: Acid Catalyzed Aromatization of Carvone…

Macroscale and Microscale Organic Experiments

7th Edition

ISBN:9781305577190

Author:Kenneth L. Williamson, Katherine M. Masters

Publisher:Kenneth L. Williamson, Katherine M. Masters

Chapter43: Amines

Section: Chapter Questions

Problem 5Q

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Can you please provide steps for how to answer the following? This is not a graded question, it's just for practice and will give me no credit. The concentration of the glucose stock solution in bottle is 50 uM. If you take 25 ml out of the above stock solution and add it to a test tube containing the following reagents 5 ml of water, 10 ml of cofactor and 10 ml of buffer. What will be the final concentration of glucose in the test tube? a. 0.015 mM b. 0.020 mM c. 0.025 mM d. 0.035 mM e. none.
. Given the following drugs in a urine specimen: Cocaine alkaloid Secobarbital (a derivative of barbituric acid) Carisoprodol (a neutral drug) Devise an analytical flow chart that will be used to separate these substances from a urine specimen. The separation will be liquid extraction methods. Choose appropriate solvents and reagents based on the properties of the materials to be separated.
3. The melting point of salicylic acid is higher than that of acetylsalicylic acid. Explain why this is with reference to their functional groups. bibs pilvolle to-ces icon 4. Tylenol also is an analgesic often taken by people allergic to aspirin. The active ingredient is acetaminophen. sulsV HO- 10 ONE NH H3C bis blas pily Would acetaminophen give a positive phenol test? (Y/N). bbs selyde A\8 Does this compound contain the ester functional group? If not, what functional group(s) is/are present? Benzer
Assuming that cyclohexanone is the limiting reagent for the synthesis of cyclohexanone oxime and that cyclohexanone oxime is the limiting reagent for the synthesis of caprolactam; what is the overall % yield of caprolactam from cyclohexanone given the percentage yield of each step of the reaction sequence as follows? Give only two significant digits. If the answer is a whole number with two digits, do not include the decimal. 57% 27% cyclohexanone → cyclohexanone oxime → caprolactam Answer:
Name Melting point (°C) Unknown 121-122 Mandelic acid 120 Benzoic acid 123 Unknown + Benzoic acid 117-123 Unknown + Mandelic acid 120-121 Please refer to the table above. Without using the mixed melting points method, can we determine the identity of the unknown sample using only the melting points of mandelic and benzoic acid? Explain
4 Complete the figure below G H NaOH / A (CH3CO) 20 (acetic anhydride) E / AICI 3 H₂O/H* -CH3COOH F J SO3 H₂SO4 1. NaOH 2. CH31 HNO3 H₂SO4 OCH3 A E / AICI 3 Zn/HCI B 1. NaNO₂/HCI 2. H₂O, A 1. NaOH 2. CH31 C
1. A vial containing an unknown sample is suspected to be one of the following compounds (mp.): urea (~133 °C), 2,4-dimethylacetanilide (~133 °C), phenacetin (~134°C) or 3-chlorobenzamide (~134 °C). A list of melting points taken on a machine when the 50% of the unknown by volume has been mixed with 50% each of the possibilities is shown in the following table: Melting point (°C) of mixture Substance mixed with unknown (50% each) urea 133.5-134.0 2,4-dimethylacetanilide phenacetin 3-chlorobenzamide 108.6-128.1 105.7-120.4 120.3-130.5 Identify the unknown and explain your reasoning, using the notes you have taken in the lab.
Hw.16.
To 20 drops of 10%NaOH, add 20 drops of dilute acetic acid. Add 5 drops of ferric chloride solution. Observe. Only the highlighted part
You are employed as a coop student at the Drug and Alcohol Testing Association of Canada (DATAC) developing analytical tests for sports doping agents. You are asked to prepare a procedure for the extraction of methylphenidate, the active compound in Ritalin, from urine samples (consider them as simple aqueous layers, you do not need to consider other components!). The goal of the procedure is to extract the methylphenidate into an organic layer which will then be evaporated, and the residue will be tested for the drug.Your colleague is helping you develop the urine test. They suggest that the urine should be adjusted to a pH above 7 before extracting with the organic solvent. Why is this necessary? Support your explanation with a full arrow-pushing mechanism for the reaction that would occur if the pH was below 7. Include all formal charges, intermediates (if applicable) and products.
You are employed as a coop student at the Drug and Alcohol Testing Association of Canada (DATAC) developing analytical tests for sports doping agents. You are asked to prepare a procedure for the extraction of methylphenidate, the active compound in Ritalin, from urine samples (consider them as simple aqueous layers, you do not need to consider other components!). The goal of the procedure is to extract the methylphenidate into an organic layer which will then be evaporated, and the residue will be tested for the drug.You find that methylphenidate is highly soluble in 2-methyltetrahydrofuran, a bio-renewable solvent. Draw the structure of 2-methyltetrahydrofuran and give two reasons why it is a good solvent choice for liquid-liquid extraction.
A mixed melting point was determined mixing unknown with benzilic acid (p 144-152), and unknown with adipic acid (mp 150-152), and unknown with salicylic acid (m 145-155). The actual, literature reported melting point of benzilic acid (mp was 149-151), adipic acid (mp 151-3), and salicylic acid (mp 158-161). The students unknown was? How do you know you are right?

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