Absorbance Compound #21 is a liquid (boiling point 60 °C) that has Z stereochemistry. Utilizing the Mass, IR, and 'H NMR spectra, along with "C NMR data, determine the structure of this compound. Elemental Analysis: C, 25.04; H, 1.05; contains two moles of a halogen. 100-25-04-105=13917 61 18/02504) Intensity $0 40 50 80 70 80 96 98 90 100 110 120 130 140 150 160 170 180 190 200 m/e Wave Number, cm-1 4000 3000 2500 2000 1500 1300 1200 1100 1000 900 800 700 "C NMR Spectral Data: doublet, 116.3 ppm 10 11 12 14 15 Wavelength, microns ppm, 5
Absorbance Compound #21 is a liquid (boiling point 60 °C) that has Z stereochemistry. Utilizing the Mass, IR, and 'H NMR spectra, along with "C NMR data, determine the structure of this compound. Elemental Analysis: C, 25.04; H, 1.05; contains two moles of a halogen. 100-25-04-105=13917 61 18/02504) Intensity $0 40 50 80 70 80 96 98 90 100 110 120 130 140 150 160 170 180 190 200 m/e Wave Number, cm-1 4000 3000 2500 2000 1500 1300 1200 1100 1000 900 800 700 "C NMR Spectral Data: doublet, 116.3 ppm 10 11 12 14 15 Wavelength, microns ppm, 5
Macroscale and Microscale Organic Experiments
7th Edition
ISBN:9781305577190
Author:Kenneth L. Williamson, Katherine M. Masters
Publisher:Kenneth L. Williamson, Katherine M. Masters
Chapter13: Mass Spectrometry
Section: Chapter Questions
Problem 3Q
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