CHEM 2411 Exp#12 NMR Spectr 3. Compound 3 is a low boiling liquid (bp-58C) that reacts with Br. in CCI. to form a 1,1.2.2 tetra-bromide. Elemental Analysis: C-48 36%, 11-4.06% contains halogen "C Spectral Data: 80.4ppm (doublet), 68.3ppm (singlet), 34.7ppm (triplet) Mam Spectrom Absorbence Insty Infrared Spectrom 4000 3000 2500 2000 'H NMR 14 110 120 130 140 130 180 170 me Wave Number, cm 1 1500 1300 1200 11001009 nr Wavelength, microne Compound 3 Structure ppm,

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CHEM 241L. Exp#12 NMR Spectre
3. Compound 3 is a low boiling liquid (bp-58°C) that reacts with Br. in CCl. to form a 1,1,2,2 tetra-bromide.
Elemental Analysis: C-48.36%, II - 4.06%; contains halogen
"C Spectral Data: 80.4ppm (doublet), 68.3ppm (singlet), 34.7ppm (triplet)
Mass Spectrom
Absorbence
Intonally
48
'H NMR
Infrared Spectrom
4000 3000 2500 2000
74
70 80 90 100 110 120 130 140 150 160 170 100
mie
Wave Number, cm .1
1300 1200 1100 1000
mon
1600
Wavelength, microne
Compound 3 Structure
Ppin
Transcribed Image Text:CHEM 241L. Exp#12 NMR Spectre 3. Compound 3 is a low boiling liquid (bp-58°C) that reacts with Br. in CCl. to form a 1,1,2,2 tetra-bromide. Elemental Analysis: C-48.36%, II - 4.06%; contains halogen "C Spectral Data: 80.4ppm (doublet), 68.3ppm (singlet), 34.7ppm (triplet) Mass Spectrom Absorbence Intonally 48 'H NMR Infrared Spectrom 4000 3000 2500 2000 74 70 80 90 100 110 120 130 140 150 160 170 100 mie Wave Number, cm .1 1300 1200 1100 1000 mon 1600 Wavelength, microne Compound 3 Structure Ppin
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