PACTICAL SrECTROSCOPY ed 14is a low-melting solid (melting point 48-49 C). The Mass, IR. and 'H NMP smectra, along with C NMK da given helow Elemental Analysis: C, 85.69, H, 5 53; 0, 8 78 Mass Spectrum 105 77 I82 30 40 s0 60 70 00 roo 110 120 130 140 150 160 170 180 190 200 me Infrared Spectrum Wave Number, om 1 4000 000 2500 0 100e 700 2000 1300 1200 E00 900 12 13 14 15 'H NMR Wavelength, microns ppm. "C Spectral Data: Structure: singlet, 187.0 ppm singlet, 137.8 ppm doublet, 132.2 ppm doublet, 130.I ppm doublet, 128.2 ppm 02000 Brooks/Cole Publishing Company

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PACTICAL SPECTROSCOPY
72
Compound 14 is a low-melting solid (melling point 48-49 "C). The Mass, IR. and 'H NMP nectra along with DC NMR data, ae
given below Elemental Analysis: C, 85.69, H, 5.53; 0, 8 78
Mass Spectrum
77
170 180 190 200
30
ro0 110 12o 130 140 150 160
mve
Infrared Spectrum
Wave Number, cm 1
700
4000 3000 2500
2000
1500
'Η ΝMR
Wavelength, microns
"C Spectral Data:
singlet, 187.0 ppm
singlet, 137 8 pprm
doublet, 132.2 ppm
doublet, 130.I ppm
doublet, 128.2 ppm
Structurel
02000 Brooks/Cole Publishing Company
Transcribed Image Text:PACTICAL SPECTROSCOPY 72 Compound 14 is a low-melting solid (melling point 48-49 "C). The Mass, IR. and 'H NMP nectra along with DC NMR data, ae given below Elemental Analysis: C, 85.69, H, 5.53; 0, 8 78 Mass Spectrum 77 170 180 190 200 30 ro0 110 12o 130 140 150 160 mve Infrared Spectrum Wave Number, cm 1 700 4000 3000 2500 2000 1500 'Η ΝMR Wavelength, microns "C Spectral Data: singlet, 187.0 ppm singlet, 137 8 pprm doublet, 132.2 ppm doublet, 130.I ppm doublet, 128.2 ppm Structurel 02000 Brooks/Cole Publishing Company
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