3) C,H1,N2 13C NMR IR LUU ppm 62.65 45.53 39.79 4000 3000 2000 L000 NAVENUNBERl 200 180 160 140 120 100 80 60 40 20 1Η NMR Cos-03-942 ppm Assign. Shift(ppm) 3 A 1.40 В 2.228 Exchanges w/ D20 C 2.341 2.764 1 TMS 1 Impurity 1 6 4 3

Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
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Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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C. explain each step with words on how to get the structure.

Step 1: Calculate the Index of Hydrogen Deficiency (IHD).

Step 2: Use IR to determine obvious functional groups.

Step 3: Use 1H-NMR to determine structural details. 

Step 4: Confirm the final structure using 13C-NMR.

3) C,H,,N,
13C NMR
IR
LUU
ppm
62.65
45.53
39.79
4000
a000
2000
1500
1000
500
HAVENUMB ERI l
200
180
160
140
120
100
80
60
40
20
1Η NMR
CDS-03-942
ppm
Assign. Shift(ppm)
3
A
1.40
В
2.228
Exchanges
w/ D,0
C
2.341
2.764
1
TMS
1
Impurity
1
6
4
2
1
TRANSHITTANCEI%
LO
Transcribed Image Text:3) C,H,,N, 13C NMR IR LUU ppm 62.65 45.53 39.79 4000 a000 2000 1500 1000 500 HAVENUMB ERI l 200 180 160 140 120 100 80 60 40 20 1Η NMR CDS-03-942 ppm Assign. Shift(ppm) 3 A 1.40 В 2.228 Exchanges w/ D,0 C 2.341 2.764 1 TMS 1 Impurity 1 6 4 2 1 TRANSHITTANCEI% LO
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