2. Determine the structures of the compounds that give rise to the following spectral data. Draw the structure, label the hydrogens and carbons, assign each peak in the ¹H and ¹³C NMR spectra, and identify major functional group stretches in the IR. a. C4H8O₂ IR 25 26 27 28 29 3 ¹H NMR Offset: 2.0 ppm 3.5 8 TERBAIE B 7 BLENDE FRENTAR 1800 3600 3400 3200 3000 2800 2600 2400 2200 H V TAN 4.5 6 ISL 2000 Wavelength (m) 5 5.5 1800 1600 Wavenumber(cm) 1400 1200 3 10 2 1000 4 8 (ppm) Peak Summary: 9.8 (broad s, 1H), 2.35 (t, 2H), 1.68 (sextet, 2H), 0.99, (t, 3H) 13C NMR: 177, 38, 18, 13 11 15 PPM 12 800 14 15 16 0

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Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
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Chapter1: Chemical Foundations
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Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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2. Determine the structures of the compounds that give rise to the following spectral data. Draw
the structure, label the hydrogens and carbons, assign each peak in the ¹H and ¹³C NMR
spectra, and identify major functional group stretches in the IR.
a. C4H8O2
IR
25 26 27 28 29 3
¹H NMR
Offset: 2.0 ppm
3.5
N
3800 3600 3400 3200 3000 2800 2600 2400 2200
8
BRI
4.5
6
2000
Wavelength (um)
5
5.5
1800
1600
Wavenumber (cm)
1400
1200
3
1000
4
8 (ppm)
Peak Summary: 9.8 (broad s, 1H), 2.35 (t, 2H), 1.68 (sextet, 2H), 0.99, (t, 3H)
13C NMR: 177, 38, 18, 13
2
1.5 PPM
800
13
14 15 16
0
600
Transcribed Image Text:2. Determine the structures of the compounds that give rise to the following spectral data. Draw the structure, label the hydrogens and carbons, assign each peak in the ¹H and ¹³C NMR spectra, and identify major functional group stretches in the IR. a. C4H8O2 IR 25 26 27 28 29 3 ¹H NMR Offset: 2.0 ppm 3.5 N 3800 3600 3400 3200 3000 2800 2600 2400 2200 8 BRI 4.5 6 2000 Wavelength (um) 5 5.5 1800 1600 Wavenumber (cm) 1400 1200 3 1000 4 8 (ppm) Peak Summary: 9.8 (broad s, 1H), 2.35 (t, 2H), 1.68 (sextet, 2H), 0.99, (t, 3H) 13C NMR: 177, 38, 18, 13 2 1.5 PPM 800 13 14 15 16 0 600
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