Step 1: Calculate the Index of Hydrogen Deficiency (IHD). Step 2: Use IR to determine obvious functional groups. Step 3: Use 1H-NMR to determine structural details.  Step 4: Confirm the final structure using 13C-NMR.   Find and draw the structure and give supporting data.

Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
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Step 1: Calculate the Index of Hydrogen Deficiency (IHD).

Step 2: Use IR to determine obvious functional groups.

Step 3: Use 1H-NMR to determine structural details. 

Step 4: Confirm the final structure using 13C-NMR.

 

Find and draw the structure and give supporting data.

4) C„H,,0
13C NMR
IR
ppm
LOD
200.39
137.19
132.83
128.56
128.06
38.30
26.51
22.51
13.95
4800
3000
2000
1000
MAVENUMBERI -l
200
180
160
140
120
100
80
60
40
20
CDS-04-808
pom
1Η NMR
Assign. Shift(ppm)
IT
A
7.95
7.51
C
7.47
2.95
E
1.72
F
1.41
G
0.96
TMS
2
2
3
CHCI,
2
Impurity
2
7
6
5
4
3
1
Transcribed Image Text:4) C„H,,0 13C NMR IR ppm LOD 200.39 137.19 132.83 128.56 128.06 38.30 26.51 22.51 13.95 4800 3000 2000 1000 MAVENUMBERI -l 200 180 160 140 120 100 80 60 40 20 CDS-04-808 pom 1Η NMR Assign. Shift(ppm) IT A 7.95 7.51 C 7.47 2.95 E 1.72 F 1.41 G 0.96 TMS 2 2 3 CHCI, 2 Impurity 2 7 6 5 4 3 1
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