Lab 6
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Drexel University *
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Course
151
Subject
Chemistry
Date
Feb 20, 2024
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CHEM 151 WI 2021
DATA AND RESULTS
Click or tap here to enter text.
Click or tap here to enter text. Click or tap here to enter text.
Mass of Vinegar Sample (g): 3.00 g Molarity of NaOH Solution (mol/L): 0.1142 M
Volume of added NaOH needed to reach phenolphthalein endpoint in Trial Run:
Click or tap here to enter text. mL
Trial Run Titration
Precise Run Titration
V(NaOH)(mL)
pH
Indicator Color
V(NaOH)(mL
pH
Indicator Color
0.00
2.40
Colorless
0.00
2.40
Colorless
1.00
2.00
3.00
4.00
5.00
6.00
7.00
8.00
9.00
10.00
11.00
12.00
13.00
14.00
15.00
16.00
17.00
18.00
19.00
20.00
21.00
22.00
23.00
24.00
4.30
4.20
4.10
4.00
3.90
3.70
3.40
4.40
4.50
4.60
4.60
4.70
4.80
4.90
4.90
5.00
5.10
5.2
5.3
5.40
5.50
5.70
6.00
7.10
clear
clear
clear
clear
clear
clear
clear
clear
clear
clear
clear
clear
clear
clear
clear
clear
clear
clear
clear
clear
clear
clear
clear
clear
CHEM 151 WI 2021
Trial Run Titration
Precise Run Titration
V(NaOH)(mL)
pH
Indicator Color
V(NaOH)(mL
pH
Indicator Color
25.00
26.00
27.00
28.00
29.00
30.00
pH at endpoint Click or tap here to enter text. Volume of Added NaOH at endpoint Click or tap here to enter text. mL
11.50
light purple
clear
11.80
12.00
clear
12.10
clear
12.20
12.30
clear
clear
CHEM 151 WI 2021
DATA AND RESULTS
Calculation of percentage of acetic acid in vinegar
Calculate the molar mass of acetic acid from its molecular formula. Then use the following equations to calculate the table entries. Please show your work in the space below the table
.
•
Equivalence Volume = Vol of NaOH to reach endpoint (mL) x
(1 L/1000 mL)
•
Moles of Acetic Acid = (Equivalence Volume(L))
x
(Molarity of NaOH)
•
Mass of Acetic Acid =
(Moles of acetic acid) x (Molar mass of acetic acid)
•
Mass Percent of Acetic Acid in vinegar = (Mass of Acetic Acid/Mass of Vinegar) x 100
Equivalence Volume (L)
Moles of Acetic Acid
Mass of Acetic Acid (g)
Mass Percent of Acetic Acid in Vinegar
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CHEM 151 WI 2021
Titration Curves
Attach the titration curve (pH versus volume of added NaOH in mL) for your sample. Make
your plot using Excel and be sure to include your name and student ID in the Excel
graph label. Each student should do their own graph.
Estimation of pK
a
of Acetic Acid
The pK
a of an acid is a measure of its intrinsic strength. The smaller the value, the stronger the acid. You can estimate the pK
a of acetic from your titration curve. It will
be the pH after half the equivalence volume has been added to the vinegar.
pK
a
(acetic acid) from pH at half the equivalence volume Click or tap here to enter text.
Related Documents
Related Questions
Table 1. Titration data
Trial 1
Trial 2
Trial 3
Initial burette reading (mL)
1.48
1.89
1.95
Molarity of NaOH (M)
0.100
0.100
0.100
Volume of vinegar sample (mL)
5.00
5.00
5.00
Final burette reading (mL)
49.32
49.06
49.93
Table 2. Titration data
Table view
List view
Table 2. Titration data
Trial 1
Trial 2
Trial 3
Initial burette reading (mL)
1.48
1.89
1.95
Molarity of NaOH (M)
0.100
0.100
0.100
Volume of vinegar sample (mL)
5.00
5.00
5.00
Final burette reading (mL)
49.32
49.06
49.93
Expected color at end point
Choose...
Choose...
Choose...
Volume of NaOH used (mL)
1. Average Volume of NaOH used in liters
2. Average moles of NaOH used (mol)
3. Average moles of acetic acid (mol)
4. Average molarity of acetic acid (M)
5. Average mass of acetic acid (g)…
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The molarity of HC2H3O2, M for trail 1,2,3.
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Pre Lab Questions: (Each answer is to be written as a complete sentence)
What is the reason for washing the precipitate with water in Step 9?
Define precipitate. Define filtrate.
In Step 2, what is the purpose for rinsing the stirring rod?
read the Procedure to answer the questions
Using a balance, mass between 1.50 – 2.00 grams of sodium carbonate in a pre-massed 150mL beaker.
Add 20 mL of distilled water and stir thoroughly to make sure all the crystals are dissolved. Rinse the stirring rod with a little distilled water after stirring.
Using a balance, mass between 1.50 – 2.00 grams of calcium chloride dihydrate in a pre-massed 50 mL beaker.
Repeat Step 2 for the solution in the 50 mL beaker.
Pour the calcium chloride solution into the 150mL beaker containing the sodium carbonate solution and stir.
Mass a piece of filter paper. Fold the filter paper and place it into the funnel. Wet it with a little distilled water to ensure that it is stuck to the sides of the funnel.
Slowly…
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3. Titration: Strong Acid / Weak Base. (I warned you to be ready!) Here's the cool chart!
Analyte: 20.00 mL 0.100 M Hydrazine (N₂H4)
Hd
A: initial
Vertical (Value) Axis Title
0
B: half equivalence
C: equivalence
5
10
15
20
Titrant: mL of 0.100 M HCI added
25
20.00 mL of 0.100 M hydrazine (N₂H4, pKb = 5.77) is titrated with 0.100 M HCl.
a) Find the initial pH (point A) and the pH at the equivalence point (point C).
b) Find the pH at the half equivalence point (point B).
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Please send me the question in 20 minutes it's very urgent plz
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help please answer in text form with proper working and explanation for each and every part and steps with concept and introduction no ai no copy paste remember answer must be in proper format with all working
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d) please see attached question
concentration KOH=20.8325mL
pH solution=2.9
beginning of the titration, Vbase = 0.00 mL
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Table 2. Titration data
Trial 1
Trial 2
Trial 3
Initial burette reading (mL)
1.19
2.26
2.39
Molarity of NaOH (M)
0.100
0.100
0.100
Volume of vinegar sample (mL)
5.00
5.00
5.00
Final burette reading (mL)
48.55
49.43
49.99
Expected color at end point
Volume of NaOH used (mL)
Average Volume of NaOH used in liters
Average moles of NaOH used (mol)
Average moles of acetic acid (mol)
Average molarity of acetic acid (M)
Average mass of acetic acid (g)
Average mass of vinegar (g) (assume the density of vinegar is 1.00 g/mL)
Average mass % of acetic acid in vinegar
Known mass % of acetic acid in vinegar is 5.45%
Percent Error
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based on the data tables provided, what is % CH3COOH in vinegar
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Which of the following steps MUST be done prior to titration of an analyte?
I. Prepare a standardized solution
II. Wash the burette with a standardized solution
III. Fill the burette to the 50-mL mark
IV. Prepare a contrast paper to determine burette volume and titration endpoint
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Help please!
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Label as KHTar in .01M KCl. Add approximately 100 mL of .01 M KCl and 2 grams of KHTar
Solve for [HTar] and amount used.
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Please help with explanation.
(Gpt/Ai wrong answer not allowed)
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0.2061 grams of an unknown organic acid was dissolved in about 50 mL of water in a 250 mL Erlenmeyer flask and titrated against 0.1000 M NaOH solution using bromothymol blue indicator. 15.56 mL of titrant was used to achieve end point. Calculate the Neutralization Equivalent. Write answer with two decimal places only. No units please.
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both I and III
II only
QUESTION 5
In the experiment "Preparation and Standardization of a Sodium Hydroxide Solution", why was the burette rinsed with
NAOH before filling it to "zero" for the titration?
To remove any residual liquids from the burette
To check that the burette works properly
To remove any air bubbles and fill the tip of the burette
All of the above
QUESTION 6
Sav
Click Save and Submit to save and submit. Click Save All Answers to save all answers.
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Calculate the Molarity
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Which product contains a strong base that would most likely completely dissolve in water?
O drain cleaner
ammonia
baking soda
antacid
Next
Save and Exit
Mark this and return
.com/ContentViewers/AssessmentViewer/Activit.
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1. Prepare 50-mL of a 50 mM H,PO, solution in a 50-ml conical tube. Molar mass of NaH2PO4
H2O used is 138 moles
2. Check the pH of this solution and record.
3. A5 M NAOH solution has been provided.
4. Add 45 µl of 5 M NaOH into the 50 mM H2PO, solution. Check the pH and record.
5. Add 205 µl of 5M NaOH into the 50 mM H2PO4 solution. Check the pH and record.
6. Add 205 µL more of 5M NaOH into the 50 mM H2PO, solution. Check the pH and record.
7. Add 45 µl of 5 M NaOH into the 50 mM H2PO, solution. Check the pH and record.
Complete the following table "predicted pH." Please show all work on a separate sheet of paper
and attach. Note that the pK, of H2PO, is 7.2.
What would be the predicted pH's? Would they be similar to the actual pH's from procedure?
After 45 µl of 5 | After 205 µl more
of 5M NaOH
Original
After 205 µl more
After 45 µl more
solution
M NaOH
of 5M NaOH
of 5 M NaOH
Actual pH
4.30
6.05
6.90
11.01
11.29
Predicted pH
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C. Titration of acid by a base
Standardization of NaOH
Volume of NaOH
Mass of KHP
Initial buret
Final buret
Trial
used
Molarity of NaOH
(g)
reading (mL)
reading (mL)
(mL)
(1)
(2)
(3)
(4)
(5)
1.2075
0.7
25
24.3
0.243
(6)
(7)
(8)
(9)
(10)
1.2062
16.4
40.9
24.49
0.2412
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prl 1) Please answer and explain, thank you
A diluted solution of NaOH was used to titrate three samples of KHP. Find the concentration of NaOH for each titration and the average concentration.
(attached is a photo)
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Please correct answer and don't used hand raiting
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- Table 1. Titration data Trial 1 Trial 2 Trial 3 Initial burette reading (mL) 1.48 1.89 1.95 Molarity of NaOH (M) 0.100 0.100 0.100 Volume of vinegar sample (mL) 5.00 5.00 5.00 Final burette reading (mL) 49.32 49.06 49.93 Table 2. Titration data Table view List view Table 2. Titration data Trial 1 Trial 2 Trial 3 Initial burette reading (mL) 1.48 1.89 1.95 Molarity of NaOH (M) 0.100 0.100 0.100 Volume of vinegar sample (mL) 5.00 5.00 5.00 Final burette reading (mL) 49.32 49.06 49.93 Expected color at end point Choose... Choose... Choose... Volume of NaOH used (mL) 1. Average Volume of NaOH used in liters 2. Average moles of NaOH used (mol) 3. Average moles of acetic acid (mol) 4. Average molarity of acetic acid (M) 5. Average mass of acetic acid (g)…arrow_forwardCan y'all help me finish solving my calculations pleasearrow_forwardThe molarity of HC2H3O2, M for trail 1,2,3.arrow_forward
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