Macroscale and Microscale Organic Experiments
7th Edition
ISBN: 9781305577190
Author: Kenneth L. Williamson, Katherine M. Masters
Publisher: Brooks Cole
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Chapter 5, Problem 13Q
Interpretation Introduction
Interpretation:
The explanation for the arrangement of water inlet and outlet position in the water-cooled condensers should be given.
Concept introduction:
The process to separate the component from a liquid mixture by boiling of selective liquid followed by condensation of the mixture is called distillation. The distillation depends upon the boiling point difference of the components. The distillation is used in various industries to get the pure component
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A student obtained a solid product in a laboratory synthesis. To verify the identity of the solid, she measured its melting point and found that the material melted over a 12 degrees Celsius range. After it had cooled, she measured the melting point of the same sample again and found that this time the solid had a sharp melting point at the temperature that is characteristic of the desired product. Why were the two melting points different? What was responsible for the change in the melting point?
A solution of acetic acid
CH3COOH
and water is boiling at
100.4°C
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10.%
acetic acid by mass.
Calculate the percent by mass of acetic acid in the boiling solution. Here's some data you may need:
normal boiling point
density
vapor pressure at
100.4°C
acetic acid
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538.torr
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sample is analyzed, and turns out to be 90.% methyl acetate by mass.
Calculate the percent by mass of methyl acetate in the boiling solution. Here's some data you may need:
methyl acetate
water
[]%
normal
boiling point
57. °C
100. °C
density
0.93
1.00
g
mL
X
g
mL
vapor pressure
at 79.8 °C
Be sure your answer has 2 significant digits.
Note for advanced students: you may assume the solution and vapor above it are ideal.
S
1551. torr
359. torr
Chapter 5 Solutions
Macroscale and Microscale Organic Experiments
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