General Chemistry
General Chemistry
4th Edition
ISBN: 9781891389603
Author: Donald A. McQuarrie, Peter A. Rock, Ethan B. Gallogly
Publisher: University Science Books
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Chapter 1, Problem 1.10P

(a)

Interpretation Introduction

Interpretation:

Multiplier that correspond to SI prefix pico has to be given.

Concept Introduction:

SI system of units use prefix in order to indicate the factors-of-10 multiples.  Symbols are also given specifically for each and every prefix.  Some of them are centi-, milli-, micro-, etc.

(b)

Interpretation Introduction

Interpretation:

Multiplier that correspond to SI prefix giga has to be given.

Concept Introduction:

Refer part (a).

(c)

Interpretation Introduction

Interpretation:

Multiplier that correspond to SI prefix nano has to be given.

Concept Introduction:

Refer part (a).

(d)

Interpretation Introduction

Interpretation:

Multiplier that correspond to SI prefix kilo has to be given.

Concept Introduction:

Refer part (a).

(e)

Interpretation Introduction

Interpretation:

Multiplier that correspond to SI prefix atto has to be given.

Concept Introduction:

Refer part (a).

(f)

Interpretation Introduction

Interpretation:

Multiplier that correspond to SI prefix femto has to be given.

Concept Introduction:

Refer part (a).

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(a 4 shows scanning electron microscope (SEM) images of extruded actions of packing bed for two capillary columns of different diameters, al 750 (bottom image) and b) 30-μm-i.d. Both columns are packed with the same stationary phase, spherical particles with 1-um diameter. A) When the columns were prepared, the figure shows that the column with the larger diameter has more packing irregularities. Explain this observation. B) Predict what affect this should have on band broadening and discuss your prediction using the van Deemter terms. C) Does this figure support your explanations in application question 33? Explain why or why not and make any changes in your answers in light of this figure. Figure 4 SEM images of sections of packed columns for a) 750 and b) 30-um-i.d. capillary columns.³
fcrip = ↓ bandwidth Il temp 32. What impact (increase, decrease, or no change) does each of the following conditions have on the individual components of the van Deemter equation and consequently, band broadening? Increase temperature Longer column Using a gas mobile phase instead of liquid Smaller particle stationary phase Multiple Paths Diffusion Mass Transfer
34. Figure 3 shows Van Deemter plots for a solute molecule using different column inner diameters (i.d.). A) Predict whether decreasing the column inner diameters increase or decrease bandwidth. B) Predict which van Deemter equation coefficient (A, B, or C) has the greatest effect on increasing or decreasing bandwidth as a function of i.d. and justify your answer. Figure 3 Van Deemter plots for hydroquinone using different column inner diameters (i.d. in μm). The data was obtained from liquid chromatography experiments using fused-silica capillary columns packed with 1.0-μm particles. 35 20 H(um) 큰 20 15 90 0+ 1500 100 75 550 01 02 594 05 μ(cm/sec) 30 15 10

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