Problem 13 119 IR Spectrum d fam 4000 3000 2000 1600 1200 v (cm) B00 100 63 80 Mass Spectrum 60 No significant Uv 40 65 absorption above 220 nm 63 20 M 98/100/102 C2H4CI2 40 80 120 160 200 240 280 m/e 13C NMR Spectrum (50 0 MHz CDCI, solution) proton coupled solvent proton decoupled 8 (ppm) 80 40 200 160 120 'H NMR Spectrum (200 MHz, CDCI, solution) expansions 2.2 2.0 ppm 6.0 58 ppm TMS 3 2 6. 8 (ppm 10 9. 8. 4. ead aseg o s

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Problem 13
2980
119
IR Spectrum
d fam
4000
3000
2000
v (cm')
1600
1200
B00
100
63
80
Mass Spectrum
60
No significant UV
65
absorption above 220 nm
M
98/100 102
63
C2H4CI2
40
80
120
160
280
200
240
m/e
13C NMR Spectrum
(50 0 MHz. CDCI, solution)
proton coupled
solvent
proton decoupled
8 (ppm)
80
40
200
160
120
H NMR Spectrum
(200 MHz, CDCI, solution)
expansions
2.2 2.0
ppm
6.0
5.8 ppm
TMS
6.
8 (ppm)
9.
8
7.
10
2.
4.
Transcribed Image Text:Problem 13 2980 119 IR Spectrum d fam 4000 3000 2000 v (cm') 1600 1200 B00 100 63 80 Mass Spectrum 60 No significant UV 65 absorption above 220 nm M 98/100 102 63 C2H4CI2 40 80 120 160 280 200 240 m/e 13C NMR Spectrum (50 0 MHz. CDCI, solution) proton coupled solvent proton decoupled 8 (ppm) 80 40 200 160 120 H NMR Spectrum (200 MHz, CDCI, solution) expansions 2.2 2.0 ppm 6.0 5.8 ppm TMS 6. 8 (ppm) 9. 8 7. 10 2. 4.
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