IR Spectrum (KBr disc) 1693 4000 3000 800 2000 1600 V (cm') 1200 10아 Mass Spectrum 56 80 M*112 60 40 20 CeH8O2 40 80 120 160 200 240 280 % of base peak

Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter9: Atomic Absorption And Atomic Fluorescence Spectrometry
Section: Chapter Questions
Problem 9.16QAP
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Question
116
Problem 10
IR Spectrum
(KBr disc)
14=12+2
1693
4000
(02F14-8 2
CH2
3000
2000
1600
1200
B00
V (cm')
100
C=02
56
Mass Spectrum
80
M* 112
60
No significant UV
absorption above 220 nm
40
20
CeHgO2
12+2-06/44
40
120
m/e
80
160
200
240
280
13C NMR Spectrum
(100 O MHz. CDCI, solution)
DEPT CH, CH,t CHt
proton decoupled
solvent
200
160
120
80
40
8 (ppm)
H NMR Spectrum
(400 MHz, CDCI, solution)
TMS
1
8 (ppm
7
6.
4
3
2
10
9.
Transcribed Image Text:116 Problem 10 IR Spectrum (KBr disc) 14=12+2 1693 4000 (02F14-8 2 CH2 3000 2000 1600 1200 B00 V (cm') 100 C=02 56 Mass Spectrum 80 M* 112 60 No significant UV absorption above 220 nm 40 20 CeHgO2 12+2-06/44 40 120 m/e 80 160 200 240 280 13C NMR Spectrum (100 O MHz. CDCI, solution) DEPT CH, CH,t CHt proton decoupled solvent 200 160 120 80 40 8 (ppm) H NMR Spectrum (400 MHz, CDCI, solution) TMS 1 8 (ppm 7 6. 4 3 2 10 9.
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