Exactly 5.00-mL aliquots of a methanol solution containing an unknown amount of methamphetamine were measured into 50.00-mL volumetric flasks. The following volumes of a standard methanol solution of methamphetamine containing 2.000 ug/mL of methamphetamine were then introduced into each flask and the mixture was diluted to volume with 0.000, 0.500, 1.00, 1.50 and 2.00 mL of methanol. 1 uL of these solutions was then injected into a gas chromatograph and the following respective peak areas were measured: 326, 480, 641, 802, and 956 (all peak areas were ere x 10³).| a) Plot the data b) Using the plot from (a), calculate the concentration of methamphetamine in the unknown. c) Derive a least squares equation from the data. d) Calculate the concentration of methamphetamine from the equation in (c).

Exactly 5.00-mL aliquots of a methanol solution containing an unknown amount of methamphetamine were measured into 50.00-mL volumetric flasks. The following volumes of a standard methanol solution of methamphetamine containing 2.000 ug/mL of methamphetamine were then introduced into each flask and the mixture was diluted to volume with 0.000, 0.500, 1.00, 1.50 and 2.00 mL of methanol. 1 uL of these solutions was then injected into a gas chromatograph and the following respective peak areas were measured: 326, 480, 641, 802, and 956 (all peak areas were ere x 10³).| a) Plot the data b) Using the plot from (a), calculate the concentration of methamphetamine in the unknown. c) Derive a least squares equation from the data. d) Calculate the concentration of methamphetamine from the equation in (c).

Introduction to General, Organic and Biochemistry

11th Edition

ISBN:9781285869759

Author:Frederick A. Bettelheim, William H. Brown, Mary K. Campbell, Shawn O. Farrell, Omar Torres

Publisher:Frederick A. Bettelheim, William H. Brown, Mary K. Campbell, Shawn O. Farrell, Omar Torres

Chapter6: Solutions And Colloids

Section: Chapter Questions

Problem 6.89P

See similar textbooks

Similar questions

Fluoridation of city water supplies has been practiced in the United States for several decades. It is done by continuously adding sodium fluoride to water as it comes from a reservoir. Assume you live in a medium-sized city of 150,000 people and that 660 L (170 gal) of water is used per person per day. What mass of sodium fluoride (in kilograms) must be added to the water supply each year (365 days) to have the required fluoride concentration of 1 ppm (part per million)that is, 1 kilogram of fluoride per 1 million kilograms of water? (Sodium fluoride is 45.0% fluoride, and water has a density of 1.00 g/cm3.)
6-39 Assuming that the appropriate volumetric flasks are available, describe how we would make these solutions: (a) 175 mL of a 1.14 M solution of NH4Br in water (b) 1.35 L of a 0.825 M solution of Nal in water (c) 330 mL of a 0.16 M solution of ethanol, C2H6O, in water
A solution is made by dissolving 34.0 g of NaCl in 100 g of H2O at 0C. Based on the data in Table 8-1, should this solution be characterized as a. saturated or unsaturated b. dilute or concentrated
6-38 Describe how we would prepare 250 mL of 0.10 M NaOH from solid NaOH and water.
Patients undergoing an upper gastrointestinal tract laboratory test are typically given an X-ray contrast agent that aids with the radiologic imaging of the anatomy. One such contrast agent is sodium diatrizoate, a nonvolatile water-soluble compound. A 0.378-m solution is prepared by dissolving 38.4 g sodium diatrizoate (NaDTZ) in.l.60 102 mL water at 3 1.2C (the density of water at 31.2C is 0.995 g/cm3). What is the molar mass of sodium diatrizoate? What is the vapor pressure of this solution if the vapor pressure of pure water at 31.2C is 34.1 torr?
6-35 Describe how we would prepare the following solutions: (a) 280. mL of a 27% v/v solution of ethanol C2H6O, in water (b) 435 mL of a 1.8% v/v solution of ethyl acetate, C4H8O2 in water (c) 1.65 L of an 8.00% v/v solution of benzene C6H6, in chloroform, CHCI3
Common commercial acids and bases are aqueous solutions with the following properties: Density (g/cm3) Mass Percent of Solute Hydrochloric acid 1.19 38 Nitric acid 1.42 70. Sulfuric acid 1.84 95 Acetic acid 1.05 99 Ammonia 0.95 28 Calculate the molarity, molality, and mole fraction of each of the preceding reagents.
Precipitimetry The chloride in a 4.321-g food sample was precipitated through the addition of 50.00 mL of a standard AgNO3 solution (10.00 mL AgNO3 = 11.22 mL KSCN). The precipitate was coated with nitrobenzene and the mixture was diluted to 250.0 mL. A 50.00 mL aliquot was taken from the diluted solution and required 4.56 mL back titration with a %3D standard KSCN solution (22.33 mL KSCN = 0.9758 g AgNO3). %3D Formula Masses: AgNO3 = 169.87; CI = 35.45 Calculate the following: 1. Molar concentration of KSCN solution M %3D 2. Molar concentration of AgNO3 solution M %3D 3. % (w/w) chloride in the original sample =
A 25mL volumetric pipet is used to deliver a sample of the stock solution marked “0.6000M X2SO4” into a 100mL volumetric flask. Distilled water is added to the flask until it is about 3/4thfull, the solution is mixed well, then more water is added to fill it up to the calibration mark, then it is mixed again. Calculate the concentration of X+ion in the dilute solution made above.
Oral rehydration salts are stated to contain the following components: Sodium Chloride 3.5g Potassium Chloride 1.5g Sodium Citrate 2.9g Anhydrous Glucose 20.0g 8.342 g of oral rehydration salts are dissolved in 500 ml of water. 5 ml of the solution is diluted to 100 ml and then 5 ml is taken from the diluted sample and is diluted to 100 ml. The sodium content of the sample is then determined by flame photometry. The sodium salts used to prepare the mixture were: Trisodium citrate hydrate (C6H5Na3O7, 2H2O) MW 294.1 and sodium chloride (NaCl) NW 58.5. Atomic weight of Na = 23. The content of Na in the diluted sample was determined to be 0.3210 mg/100 ml. Determine the % of stated content of Na in the sample.
Oral rehydration salts are stated to contain the following components: Sodium Chloride 3.5g Potassium Chloride 1.5g Sodium Citrate 2.9g Anhydrous Glucose 20.0g 8.342 g of oral rehydration salts are dissolved in 500 ml of water. 5 ml of the solution is diluted to 100 ml and then 5 ml is taken from the diluted sample and is diluted to 100 ml. The sodium content of the sample is then determined by flame photometry. The sodium salts used to prepare the mixture were: Trisodium citrate hydrate (C6H5Na3O7, 2H2O) MW 294.1 and sodium chloride (NaCl) NW 58.5. Atomic weight of Na = 23. The content of Na in the diluted sample was determined to be 0.3210 mg/100 ml. Determine the % of stated content of Na in the sample. The stated should be 104.5, how??
Based on the selected correct unit, what is the value of x?