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Mass Spectrum - Carboxylic Acid Solid Unknown Relative Intensity 100 80 60 40 20 20 ... M+= 200 20 40 60 80 100 120 140 160 180 200 m/z IR Spectrum - Carboxylic Acid Solid Unknown LOD D 4000 3000 2000 1500 1000 500 HAVENUMBERI -11 CHE231L AQ22 These tables MUST be included in the report for each of your unknowns in the Results Section (4 tables in total): Chemical Name: Percent Recovery Solids Melting Point Data (°C) Crude Pure Physical Appearance MS Data Molecular Formula IHD M+ (m/z) Base Peak (m/z) Lost Fragments / Other Peaks (m/z) Unknown Code: Crude: Pure: Trial 1 Trial 2 Average IR Data Absorption Band Wavenumber (cm) Intensity Shape 1 2 3 4 (etc.) 'H NMR Data Proton(s) A B C D (etc.) 13C NMR Carbon(s) 1 2 3 4 (etc.) Structure: 8 (ppm) Splitting Integration 8 (ppm) 6

Mass Spectrum - Carboxylic Acid Solid Unknown Relative Intensity 100 80 60 40 20 20 ... M+= 200 20 40 60 80 100 120 140 160 180 200 m/z IR Spectrum - Carboxylic Acid Solid Unknown LOD D 4000 3000 2000 1500 1000 500 HAVENUMBERI -11 CHE231L AQ22 These tables MUST be included in the report for each of your unknowns in the Results Section (4 tables in total): Chemical Name: Percent Recovery Solids Melting Point Data (°C) Crude Pure Physical Appearance MS Data Molecular Formula IHD M+ (m/z) Base Peak (m/z) Lost Fragments / Other Peaks (m/z) Unknown Code: Crude: Pure: Trial 1 Trial 2 Average IR Data Absorption Band Wavenumber (cm) Intensity Shape 1 2 3 4 (etc.) 'H NMR Data Proton(s) A B C D (etc.) 13C NMR Carbon(s) 1 2 3 4 (etc.) Structure: 8 (ppm) Splitting Integration 8 (ppm) 6

Fundamentals Of Analytical Chemistry
Fundamentals Of Analytical Chemistry
9th Edition
ISBN:9781285640686
Author:Skoog
Publisher:Skoog
Chapter16: Applications Of Neutralization Titrations
Section: Chapter Questions
Problem 16.17QAP
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Mass Spectrum - Carboxylic Acid Solid Unknown Relative Intensity 100 80 60 40 20 20 ... M+= 200 20 40 60 80 100 120 140 160 180 200 m/z IR Spectrum - Carboxylic Acid Solid Unknown LOD D 4000 3000 2000 1500 1000 500 HAVENUMBERI -11
Transcribed Image Text:Mass Spectrum - Carboxylic Acid Solid Unknown Relative Intensity 100 80 60 40 20 20 ... M+= 200 20 40 60 80 100 120 140 160 180 200 m/z IR Spectrum - Carboxylic Acid Solid Unknown LOD D 4000 3000 2000 1500 1000 500 HAVENUMBERI -11
CHE231L AQ22 These tables MUST be included in the report for each of your unknowns in the Results Section (4 tables in total): Chemical Name: Percent Recovery Solids Melting Point Data (°C) Crude Pure Physical Appearance MS Data Molecular Formula IHD M+ (m/z) Base Peak (m/z) Lost Fragments / Other Peaks (m/z) Unknown Code: Crude: Pure: Trial 1 Trial 2 Average IR Data Absorption Band Wavenumber (cm) Intensity Shape 1 2 3 4 (etc.) 'H NMR Data Proton(s) A B C D (etc.) 13C NMR Carbon(s) 1 2 3 4 (etc.) Structure: 8 (ppm) Splitting Integration 8 (ppm) 6
Transcribed Image Text:CHE231L AQ22 These tables MUST be included in the report for each of your unknowns in the Results Section (4 tables in total): Chemical Name: Percent Recovery Solids Melting Point Data (°C) Crude Pure Physical Appearance MS Data Molecular Formula IHD M+ (m/z) Base Peak (m/z) Lost Fragments / Other Peaks (m/z) Unknown Code: Crude: Pure: Trial 1 Trial 2 Average IR Data Absorption Band Wavenumber (cm) Intensity Shape 1 2 3 4 (etc.) 'H NMR Data Proton(s) A B C D (etc.) 13C NMR Carbon(s) 1 2 3 4 (etc.) Structure: 8 (ppm) Splitting Integration 8 (ppm) 6
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