5) C3H120 13C NMR IR ppm 100 199.61 159.85 126.86 80 36.11 34.40 60 32.83 27.71 %T 40 20 4000 3000 2000 Wavenumberlcm-1) 1500 1000 500 400 200 150 100 50 IR2010-87985TK CR201002120NS ppm 1Η NMR Assign. Shift(ppm) A 6.659 В 5.836 C 2.455 1.873 E 1.169 TMS 2 2 1 1 Impurity 7 6 2 1 Ho
5) C3H120 13C NMR IR ppm 100 199.61 159.85 126.86 80 36.11 34.40 60 32.83 27.71 %T 40 20 4000 3000 2000 Wavenumberlcm-1) 1500 1000 500 400 200 150 100 50 IR2010-87985TK CR201002120NS ppm 1Η NMR Assign. Shift(ppm) A 6.659 В 5.836 C 2.455 1.873 E 1.169 TMS 2 2 1 1 Impurity 7 6 2 1 Ho
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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Question
E. explain each step with words on how to get the structure.
Step 1: Calculate the Index of Hydrogen Deficiency (IHD).
Step 2: Use IR to determine obvious
Step 3: Use 1H-NMR to determine structural details.
Step 4: Confirm the final structure using 13C-NMR.
![5) CH,20
13C NMR
IR
ppm
100
199.61
159.85
126.86
80
36.11
34.40
60
32.83
27.71
%T
40
20
2000
3000
2000
1500
1000
500 400
200
150
100
50
IR2010-8798STK
Wavenumber[cm-1]
CR20100212ONS
ppm
1Η ΝMR
Assign. Shift(ppm)
A
6.659
В
5.836
2.455
1.873
E
1.169
TMS
2
2
1
1
Impurity
7
4
3
2](/v2/_next/image?url=https%3A%2F%2Fcontent.bartleby.com%2Fqna-images%2Fquestion%2F684fca1c-95d0-4c4b-8900-ee027b0abba4%2F4057eddd-0af7-43f4-891a-5d752e644525%2F9u6duv7_processed.png&w=3840&q=75)
Transcribed Image Text:5) CH,20
13C NMR
IR
ppm
100
199.61
159.85
126.86
80
36.11
34.40
60
32.83
27.71
%T
40
20
2000
3000
2000
1500
1000
500 400
200
150
100
50
IR2010-8798STK
Wavenumber[cm-1]
CR20100212ONS
ppm
1Η ΝMR
Assign. Shift(ppm)
A
6.659
В
5.836
2.455
1.873
E
1.169
TMS
2
2
1
1
Impurity
7
4
3
2
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