Elucidate the structure for compound Busing spectroscopic data provided. B. Spectral analysis of a pure compound gave the following MS, IR data and H-NMR data (after D2O shake). i) Provide the Molecular formula, (ii) Identify the correct structure (iii) Identify the most important (diagnostic) IR signal(s) and match each proton NMR absorption with the proton that is causing that absorbance? MS: m/z: 86 (10%) ; 87 (0.5); 68.07 (100.0%), 69.08 (5.4%) 1H NMR (d): 5.67 (1H, doublet, J = 18), 5.63 (1H, quartet, J= 17), 4.38 (1H, quartet), 1.63 (3H, doublet), 1.07 (3H, doublet). IR (see below) LOD 4000 3000 2000 HAVENUMBERI-1 1500 1000 500
Elucidate the structure for compound Busing spectroscopic data provided. B. Spectral analysis of a pure compound gave the following MS, IR data and H-NMR data (after D2O shake). i) Provide the Molecular formula, (ii) Identify the correct structure (iii) Identify the most important (diagnostic) IR signal(s) and match each proton NMR absorption with the proton that is causing that absorbance? MS: m/z: 86 (10%) ; 87 (0.5); 68.07 (100.0%), 69.08 (5.4%) 1H NMR (d): 5.67 (1H, doublet, J = 18), 5.63 (1H, quartet, J= 17), 4.38 (1H, quartet), 1.63 (3H, doublet), 1.07 (3H, doublet). IR (see below) LOD 4000 3000 2000 HAVENUMBERI-1 1500 1000 500
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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Transcribed Image Text:Elucidate the structure for compound Busing spectroscopic data provided.
B. Spectral analysis of a pure compound gave the following MS, IR data and H-NMR data (after D2O shake). i) Provide the Molecular formula, (ii) Identify the correct structure (iii) Identify
the most important (diagnostic) IR signal(s) and match each proton NMR absorption with the proton that is causing that absorbance?
MS: m/z: 86 (10%) ; 87 (0.5); 68.07 (100.0%), 69.08 (5.4%)
1H NMR (d): 5.67 (1H, doublet, J = 18), 5.63 (1H, quartet, J= 17), 4.38 (1H, quartet), 1.63 (3H, doublet), 1.07 (3H, doublet).
IR (see below)
LOD
4000
3000
2000
HAVENUMBERI
1500
1000
500
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