3. (a) Schlenk techniques are frequently used to perform air-sensitive reactions. Outline a general experimental procedure to set up a reaction which involve the generation of a highly air-sensitive intermediate using Schlenk line and Schlenk flask. (Remark: no need to include the workup procedures) (b) If you see a pale blue liquid in the cold trap of a Schlenk line, what should you do? And why?

3. (a) Schlenk techniques are frequently used to perform air-sensitive reactions. Outline a general experimental procedure to set up a reaction which involve the generation of a highly air-sensitive intermediate using Schlenk line and Schlenk flask. (Remark: no need to include the workup procedures) (b) If you see a pale blue liquid in the cold trap of a Schlenk line, what should you do? And why?

Chemistry

10th Edition

ISBN:9781305957404

Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Chapter1: Chemical Foundations

Section: Chapter Questions

Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...

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Question

3. (a) Schlenk techniques are frequently used to perform air-sensitive reactions. Outline a
general experimental procedure to set up a reaction which involve the generation of a
highly air-sensitive intermediate using Schlenk line and Schlenk flask. (Remark: no need
to include the workup procedures)
(b) If you see a pale blue liquid in the cold trap of a Schlenk line, what should you do?
And why?

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