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Analysis of Hydrogen Peroxide Decomposition
Introduction
Methods
List of materials
MeasureNet
Gas pressure probe kit
Thermometer
3% hydrogen peroxide, (H
2
O
2
) solution
0.5M potassium iodide, (KI) solution
Two 6’’ test tubes
Pipets
Pipet bulb
400 ml beaker
Additional beakers and glassware of assorted sizes Procedure
1.
Set up the MeasureNet going to the “Pressure v. Time,” “Calibrate,” and then set the atmospheric pressure to 760mmHg
2.
Obtain about 15ml of H
2
O
2
, 4ml of KI, and 5ml of water and collect each chemical in its own beaker. 3.
Obtain 8 test tubes
Table 14.1 sourced from (French et. all, 86).
Trial
Vol. of 3%
H
2
O
2 (mL)
Vol. of 0.500
M KI (mL)
Vol. of H
2
O
(mL)
Temperature
File Name
1
4
1
0
T
1
“001”
2
4
0.5
0.5
T
1
“002”
3
2
1
2
T
1
“003”
4
4
1
0
T
2
“004”
4.
According to the table, mix the various volumes of water and KI into 4 test tubes
5.
According to the table, add the volumes of H
2
O
2
in four test tubes
6.
Press “Display” on the MeasureNet.
7.
Mix the 4 mL H
2
O
2
solution and 1 mL KI solution together, let sit for 5 seconds
8.
Cover the solution with the gas probe and collect data for 200 seconds. 9.
Save the file as “001”
10. Repeat steps 7-9 for trials 2-3 with the appropriate volumes and save with respective file name according to Table 14.1 being sure to clean the probe and dispose of solution between each use. 11. For trial 4, fill a 400ml beaker with hot water, ensuring that the hot water temperature is at least 10C warmer than the room temperature (this may require waiting for the faucet water to heat up) which can be determined with a thermometer.
12. Place both vials for trial 4 in the hot water to rest for at least 120 seconds.
13. Mix the solutions while keeping the test tubes submerged in water.
14. Repeat steps 7-9 for trial 4.
The procedure and material list adapted from (French, et al. 70-79).
Discussion
From this experiment I learned
Conclusion
Works Cited
French, April, Allison Soult, M. Mearl Savas, Francois Botha, Carolyn Brock, Charles Griffith,
Darla Hood, Robert Kiser, Penny O’Connor, William Plucknett, Donald Sands, Diane
Vance, William Wagner. “Experiment 14 The Decomposition of Hydrogen Peroxide” General Chemistry II Laboratory Manual
. Plymouth, MI: Hayden-Mcneil, 2020. 81-86.
Web. 19 October 2021.
https://www3.chem21labs.com/labfiles/36194_48_Exp%2013_FrenchA%202187-
1%20W20..pdf?rf=6260
French, April, Allison Soult, M. Mearl Savas, Francois Botha, Carolyn Brock, Charles Griffith,
Darla Hood, Robert Kiser, Penny O’Connor, William Plucknett, Donald Sands, Diane
Vance, William Wagner. “Using MeasureNet and Probes.” General Chemistry
II Laboratory Manual
. Plymouth, MI: Hayden-Mcneil, 2020. 37-50. Web.
19 October
2021.
https://www3.chem21labs.com/labfiles/36194_48_1-4_FrenchA%202187-
1%20W20..pdf?rf=7702
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Related Questions
Please answer fast i give you upvote.
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As part of this experiment you will need to determine the concentrations of Fe* and SCN ions
present in test tubes 1-9. These values can be calculated using the volumes and concentrations
provided in Tables 1 and 2 of the Equilibrium Lab - Procedure and the dilution equation (M,V1 =
M2V2).
Note: the solutions provided in the lab, and therefore the tables in the lab document, are the
compounds used to prepare the solution. You must determine the concentration of the ions based on
how these compounds díssociate in solution
Complete the following table by filling the the calculated initial concentrations of each substance. Be
sure to:
Pay attention to significant figures
• Round appropriately
Use decimal notation (not scientific)
Do not include units
Test
Initial [Fe3*] (M)
Initial [SCN'] (M)
Tube
1
3
4.
6.
7
8.
2.
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Aktiv Chemistry
→ C
<
+
X b Success Confirmation of QX M Your Chemistry answer is rex b Answered: How many mL o x b Answered: A student combi x
app.101edu.co
Time's Up!
A 0.660 M solution of KCI needs to be prepared through dilution. A
2.00 M stock solution will be added to a 0.250 L volumetric flask and
then water will be added to the 0.250 L mark.
Determine the volume (in mL) of the 2.00 M stock solution of KCI
needed to produce this solution.
1
4
7
+/-
New Tab
2
5
8
mL
3
6
9
G
0
x +
Submit
X
C
x 100
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show full & complete procedure. Please answer parts a), b) & c). Note they are subparts of the same question
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3. Standard white vinegar you can buy in the grocery store is 5% concentration. That means 5% of the liquid vinegar is acetic acid and 95% of the solution is water. In a hardware store, you can buy industria
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Samuel does another experiment, this time with 5% vinegar and 30% vinegar. He sets up two science fair volcanoes (in no particular order), each with the same temperature, mass of baking soda and volume o
vinegar. But one volcano uses 5% vinegar and the other volcano uses 30% vinegar. He measures the volume of gas production for the'first minute of each reaction, and he records the data below.
Volcano # 1
Volume of gas produced (mL.) vs. Time (s) for Volcano #1
Time
Volume of gas
(s)
produced (ml)
60
E 50
10
20
30
25
8 40
38
46
30
20
Volume of gas
produced (ml)
40
50
50
60
52
of
10
53
20
40
60
80
Time (s)
Volcano # 2
Volume of gas
Volume of gas produced…
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How do I calculate the first table ?
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30jud to 28AM
basu mw
5. Sodium carbonate is a reagent that may be used to standardize acids in the same way that you have used
KHP in this experiment. In such a standardization it was found that a 0.498-g sample of sodium carbon-
ate required 23.5 mL of a sulfuric acid solution to reach the end point for the reaction.
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Gravimetric Analysis of Calcium Carbonate and Hard Water
Introduction
In this laboratory activity, you will develop calculating skills and facility with the techniques of
gravimetric analysis. In particular, we will practice quantitative transfer and vacuum filtration. You
will perform a precipitation reaction that involves preparing and combining solutions of sodium
carbonate, Na2CO3, and calcium chloride, CaCl2. The balanced chemical equation for this reaction
predicts the amount of precipitate that will be formed. Careful isolation, drying and weighing of the
precipitate will confirm the calculations and the percent yield.
Pre-Lab Questions
1. Define the term gravimetric analysis. Describe the procedure used in this activity, and identify two
other common examples of gravimetric analysis.
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On the graph paper plot a graph of your reaction rates vs. concentration by using
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QUESTION 24
In the experiment "Beer-Lambert's Law and Spectrophotometry", you prepared a calibration plot similar to the one
pictured below. What is the approximate concentration of a solution whose absorbance is 0.35?
Calibration Plot
0.8
0.7
0.6
0.5
0.4
0.3
0.2
0.1
0.
0.01
0.02
0.03
0.04
0.05
Save A
Click Save and Submit to save and submit. Click Save All Answers to save all wnswers.
Absorbance
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write down the correct answer to a, b,c, d
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Reactions of Na₂CO3
* Reactions with a carbonate salt and acid are gas evolving!
I
Na₂CO3(aq)
Na* CO3²-
Na2CO3(aq)
Na₂CO3 (aq)
Na₂CO3(aq)
Na₂CO3 (aq)
Na₂CO3 (aq)
Na2CO3 (aq)
Na₂CO3 (aq)
Na₂CO3 (aq)
Na₂CO3 (aq)
+
+
+
+
2
Pb(NO3)2 (aq)
H* CI
HCl (aq)
Na3PO4 (aq)
KI (aq)
CuSO4 (aq)
H₂SO4 (aq)
NaOH (aq)
AgNO3(aq)
CaCl2 (aq)
HNO3(aq)
→>>
→>
→>>>
➜>>
↑
↑
Na Cl + H* CO3²-
NaCl (aq) + [H₂CO3 (aq)] → NaCl (aq) + H₂O (1) + CO2 (s)
2 NaCl (aq) + H2₂O (1) +
PAGE 123 OF 232
(g)
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For lab 4, we combined baking soda with vinegar, according to the chemical equation
NaHCO 3 + CH 3COOH ==== NaCH 3COO + CO 2 + H 2O
Consider 3 experiments: (i) 2g baking soda + 5mL vinegar, (ii) 2g baking soda + 10mL vinegar and (iii) 2g baking soda + 20mL vinegar. The amount of CO 2 produced was highest for (iii) and lowest for (i). For these experiments, which of the following is true?
Vinegar ran out first
Baking soda ran out first
They both ran out at the same time
Neither ran out
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Can I please get all final concentrations please!
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9-
An aqueous solution at 25 C has a H,O concentration of 2. x 10 M. Calculate the OH concentration. Be sure your answer has 1 significant digits.
|| M
x10
I Don't Know
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7
Solid lead (II) nitrate is slowly added to 125 mL of a 0.190 M potassium hydroxide solution until the concentration
of lead ion is 0.0547 M. The percent of hydroxide ion remaining in solution is
%.
Submit Answer
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4
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[Review Topics)
[References
Use the References to access important values if needed for this question.
Retry Entire Group
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What reactants are used in the net ionic equation of the Chemical Kinetic reaction?
2-
103²- and SO3™
SO3²- and 103
O 103² and SO3²-
2-
OSO3 and 103
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rofiles Tab Window Help
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What volume of a 0.352 M hyd x +
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on Concentrations: This is group attempt 1 of 10
In the laboratory you dissolve 15.4 g of zinc bromide in a volumetric flask and add water to a total
volume of 250 mL.
What is the molarity of the solution?
MindTap - Cengage Learning X
Use the References to access important values if needed for this question.
What is the concentration of the zinc cation?
tv
References
What is the concentration of the bromide anion?
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Based on this student data, calculate the average molarity of the NaOH solution. Standard: KHP =
potassium hydrogen phthalate, MM 204.4 g/mol
Student Data Trial 1
E KHP
mL initial: NaOH
mL final: NaOH
2.02
0.57
19.25
Trial 2
2.05
19.25
39.80
Trial 3
1.99
1.65
20.75
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i) How many moles of hydrochloric acid were there in the volume of acid added in the titration?
ii) How many moles of calcium hydroxide were there in the 25 cm sample of solution that the student used in the titration?
iii) What was the concentration of the calcium hydroxide solution in mol/dm?
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Part A) A 10.0 mL sample of 0.250 mol/L NiF2(aq) is mixed with 20.0 mL of 0.0900 mol/L NaOH(aq) and then diluted to a final volume of 100. mL.Calculate the concentration of Ni2+ ions in the 100 mL mixture before the reaction starts. Express your answer to three significant figures.ksp: 5.48e-16
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Trial 1
Trial 2
Trial 3
Trial 4
Mass of KHC;H4O4 (KHP) 2.0158 KHP
1.9657 KHP
2.0053 KHP
|1.9801 KHP
Initial buret reading
0.00 M
|0.00 M
0.00 M
|0.00 M
Final buret reading
31.04 M
30.83 M
30.81 M
30.50 M
Volume of NaOH
0.03104 L
0.03083 L
0.03081 L
0.0305 L
Results table
Trial 1
Trial 2
Trial 3
Trial 4
Moles of KHP
0.00987
0.00962
0.00982
0.00969
Moles of NaOH
0.00987
0.00962
0.00982
0.00982
Volume of NaOH (L)
0.03104 L
0.03083 L
0.03081 L
0.0305 L
Molarity of NaOH
0.31797
3.12033
0.31883
3.2196 L
Average molarity of NaOH
Sample calculation:
In the space below show complete calculations for moles of KHP and molarity of NaOH using data from
TRIAL 1 only. Include formulas and units.
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