14_Lab_113

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University of Kentucky *

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113

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Chemistry

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Apr 3, 2024

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4

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Analysis of Hydrogen Peroxide Decomposition Introduction Methods List of materials MeasureNet Gas pressure probe kit Thermometer 3% hydrogen peroxide, (H 2 O 2 ) solution 0.5M potassium iodide, (KI) solution Two 6’’ test tubes Pipets Pipet bulb 400 ml beaker Additional beakers and glassware of assorted sizes Procedure 1. Set up the MeasureNet going to the “Pressure v. Time,” “Calibrate,” and then set the atmospheric pressure to 760mmHg 2. Obtain about 15ml of H 2 O 2 , 4ml of KI, and 5ml of water and collect each chemical in its own beaker. 3. Obtain 8 test tubes
Table 14.1 sourced from (French et. all, 86). Trial Vol. of 3% H 2 O 2 (mL) Vol. of 0.500 M KI (mL) Vol. of H 2 O (mL) Temperature File Name 1 4 1 0 T 1 “001” 2 4 0.5 0.5 T 1 “002” 3 2 1 2 T 1 “003” 4 4 1 0 T 2 “004” 4. According to the table, mix the various volumes of water and KI into 4 test tubes 5. According to the table, add the volumes of H 2 O 2 in four test tubes 6. Press “Display” on the MeasureNet. 7. Mix the 4 mL H 2 O 2 solution and 1 mL KI solution together, let sit for 5 seconds 8. Cover the solution with the gas probe and collect data for 200 seconds. 9. Save the file as “001” 10. Repeat steps 7-9 for trials 2-3 with the appropriate volumes and save with respective file name according to Table 14.1 being sure to clean the probe and dispose of solution between each use. 11. For trial 4, fill a 400ml beaker with hot water, ensuring that the hot water temperature is at least 10C warmer than the room temperature (this may require waiting for the faucet water to heat up) which can be determined with a thermometer. 12. Place both vials for trial 4 in the hot water to rest for at least 120 seconds. 13. Mix the solutions while keeping the test tubes submerged in water. 14. Repeat steps 7-9 for trial 4.
The procedure and material list adapted from (French, et al. 70-79). Discussion From this experiment I learned Conclusion Works Cited French, April, Allison Soult, M. Mearl Savas, Francois Botha, Carolyn Brock, Charles Griffith, Darla Hood, Robert Kiser, Penny O’Connor, William Plucknett, Donald Sands, Diane Vance, William Wagner. “Experiment 14 The Decomposition of Hydrogen Peroxide” General Chemistry II Laboratory Manual . Plymouth, MI: Hayden-Mcneil, 2020. 81-86. Web. 19 October 2021. https://www3.chem21labs.com/labfiles/36194_48_Exp%2013_FrenchA%202187- 1%20W20..pdf?rf=6260 French, April, Allison Soult, M. Mearl Savas, Francois Botha, Carolyn Brock, Charles Griffith, Darla Hood, Robert Kiser, Penny O’Connor, William Plucknett, Donald Sands, Diane Vance, William Wagner. “Using MeasureNet and Probes.” General Chemistry II Laboratory Manual . Plymouth, MI: Hayden-Mcneil, 2020. 37-50. Web. 19 October 2021. https://www3.chem21labs.com/labfiles/36194_48_1-4_FrenchA%202187- 1%20W20..pdf?rf=7702
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