EBK EXPERIMENTAL ORGANIC CHEMISTRY: A M
6th Edition
ISBN: 9781305687875
Author: Gilbert
Publisher: CENGAGE LEARNING - CONSIGNMENT
expand_more
expand_more
format_list_bulleted
Question
Chapter 3.2, Problem 27E
Interpretation Introduction
Interpretation:Purpose to scratch inside of flask with glass rod should be determined. Also, other methods to induce crystallization should be determined.
Concept introduction:Recrystallization is technique that is used for purification of organic compounds. This process includes dissolution of solid in specific solvent at high temperature and then crystals are made again by process of cooling. Temperature of crystals is decreased to allow impurities to remain in solution only.
Expert Solution & Answer
Trending nowThis is a popular solution!
Students have asked these similar questions
Briefly explain how slow cooling contributes to the formation of pure crystals during recrystallization.
In an experiment, is a 100% yield possible in recrystallization? Please explain.
In recrystallization, is it always good to have a high % recovery? Explain. What are the advantages and disadvantages of recrystallization?
Chapter 3 Solutions
EBK EXPERIMENTAL ORGANIC CHEMISTRY: A M
Ch. 3.2 - Prob. 1ECh. 3.2 - Prob. 2ECh. 3.2 - Prob. 3ECh. 3.2 - Prob. 4ECh. 3.2 - Prob. 5ECh. 3.2 - Prob. 6ECh. 3.2 - Prob. 7ECh. 3.2 - Prob. 8ECh. 3.2 - Prob. 9ECh. 3.2 - Prob. 10E
Ch. 3.2 - Prob. 11ECh. 3.2 - Prob. 12ECh. 3.2 - Prob. 13ECh. 3.2 - Prob. 14ECh. 3.2 - Prob. 15ECh. 3.2 - Prob. 16ECh. 3.2 - Prob. 17ECh. 3.2 - Prob. 18ECh. 3.2 - Prob. 19ECh. 3.2 - Prob. 20ECh. 3.2 - Prob. 21ECh. 3.2 - Prob. 22ECh. 3.2 - Prob. 23ECh. 3.2 - Prob. 24ECh. 3.2 - Prob. 25ECh. 3.2 - Prob. 26ECh. 3.2 - Prob. 27ECh. 3.2 - Prob. 28ECh. 3.2 - Prob. 29ECh. 3.2 - Prob. 30ECh. 3.2 - Prob. 31ECh. 3.2 - Prob. 32ECh. 3.2 - Prob. 34ECh. 3.3 - Prob. 1ECh. 3.3 - Prob. 2ECh. 3.3 - Prob. 3ECh. 3.3 - Prob. 4ECh. 3.3 - Prob. 5ECh. 3.3 - Prob. 6ECh. 3.3 - Prob. 7ECh. 3.3 - Prob. 8ECh. 3.3 - Prob. 10ECh. 3.3 - Prob. 11ECh. 3.3 - Prob. 12ECh. 3.3 - Prob. 13ECh. 3.3 - Prob. 14ECh. 3.3 - Prob. 15ECh. 3.3 - Prob. 16ECh. 3.3 - Prob. 17ECh. 3.3 - Prob. 18ECh. 3.3 - Prob. 19ECh. 3.3 - Prob. 21ECh. 3.3 - Prob. 22ECh. 3.3 - Prob. 23ECh. 3.3 - Prob. 24ECh. 3.3 - Prob. 25ECh. 3.3 - Prob. 26E
Knowledge Booster
Similar questions
- Vapor-pressure lowering is a colligative property, as are freezing-point depression and boiling-point elevation. What is a colligative property? Why is the freezing point depressed for a solution as compared to the pure solvent? Why is the boiling point elevated for a solution as compared to the pure solvent? Explain how to calculate T for a freezing-point depression problem or a boiling-point elevation problem. Of the solvents listed in Table 10-5, which would have the largest freezing-point depression for a 0.50 molal solution? Which would have the smallest boiling-point elevation for a 0.50 molal solution? A common application of freezing-point depression and boiling-point elevation experiments is to provide a means to calculate the molar mass of a nonvolatile solute. What data are needed to calculate the molar mass of a nonvolatile solute? Explain how you would manipulate these data to calculate the molar mass of the nonvolatile solute.arrow_forwardI need the answer as soon as possiblearrow_forwardIn the technique of recrystallization, one step involves heating the solvent containing the solute to its boiling point and, after the solution is cooled to room temperature, cooling it further in an ice-water bath. Why is it important to operate at these temperature extremes during a recrystallization?arrow_forward
- Draw an outline of the recrystallization process- Assume all types of Impurities(Soluble, Insoluble and colored) are present.arrow_forwardExplain how acidification or neutralization can impact the solubility of a compound (for example, compare the solubility of sodium salicylate in water to the solubility of salicylic acid.) How can this be used to purify a mixture using liquid/liquid extraction?arrow_forwardIn the Isolation of Caffeine from Tea experiment, the tea bags were first boiled in water followed by performing an extraction using the organic solvent, methylene chloride. Which physical property was essential in selectively extracting caffeine from the aqueous layer into the methylene chloride layer? Solubility Boiling point Freezing point Densityarrow_forward
- (Concentration) A solid mixture made up of 75% of solid A and 25% of solid B by mass is to be dissolved in 250.0 ± 0.5 mL of water. Assuming that the solid mixture is completely soluble in water, how many grams of the solid mixture must be used to obtain a 0.500 ± 2% molal solution of solid A. Note that the formula mass of solid A is 101.11 g/mol while the formula mass of solid B is 174.2592 g/mol. The density of water at the temperature of the experiment is 0.9972995 g/mL. What absolute uncertainty will be associated with your mass measurement? (absolute error)arrow_forwardDraw a phase diagram showing how the phase boundaries differ for a pure solvent compared with a solution. Give an explanation for the phase diagram.arrow_forward5- A chemist is given a nonelectrolyte white powder for analysis. 38.7 g of this substance is dissolved in 100.0 g of water. It is determined that the resulting solution freezes at -4.0°C. Additionally, the elemental composition of the substance is identified and found to be 40.0% C, 6.7% H and 53.3 % O by mass. Find the molecular formula of this unknown white powder using these experimental evidences (Kş of water: 1.86°C/m, C: 12 g/mol, H: 1 g/mol, O: 16 g/mol).arrow_forward
- synthetic ion exchange resins. These resins are organic polymeric networks that contain functional groups that are permanently attached to the resin. One such functional group is sulfonic acid, -SO3H. When placed in water, the resin (being a large organic molecule) will not dissolve. However, the ionic functional groups become hydrated and the resin will swell as it takes up waters of hydration. The resin may then be thought of as a solid solution mixture with the functional groups being "dissolved" but the polymer remaining as a solid. The hydronium ion (H3O+) associated with acidic functional groups like sulfonic acid will dissociate just as it would if the acid were free of the resin. If other cations such as Cu2+ or Na+ are added to the resin, an ion-exchange reaction can occur: . Note that one H+ is released for each positive charge bound to the resin. Since the resin exchanges a hydrogen ion for a sodium ion in this reaction, sulfonic acid resins are called cation-exchange…arrow_forwardWhy is flameless heating used for heating a solution in hexane or diethyl ether during a recrystallization? Why should the size of crystals obtained in a recrystallization be neither too large nor too small?arrow_forward2. You have a solution that contains 4.0g of oxalic acid dissolved in 100 mL of water. This solution is placed in a separatory funnel, and then 100 mL of diethyl ether is added to the separatory funnel and an extraction is performed. (Diethyl ether and water are immiscible solvents.) Use the following constants to calculate how much oxalic acid is in each solvent after the extraction. Solubility of oxalic acid in water = 9.5 g / 100 mL Solubility of oxalic acid in ether = 16.9 g/100 mLarrow_forward
arrow_back_ios
SEE MORE QUESTIONS
arrow_forward_ios
Recommended textbooks for you
- Macroscale and Microscale Organic ExperimentsChemistryISBN:9781305577190Author:Kenneth L. Williamson, Katherine M. MastersPublisher:Brooks ColePrinciples of Modern ChemistryChemistryISBN:9781305079113Author:David W. Oxtoby, H. Pat Gillis, Laurie J. ButlerPublisher:Cengage LearningIntroductory Chemistry: An Active Learning Approa...ChemistryISBN:9781305079250Author:Mark S. Cracolice, Ed PetersPublisher:Cengage Learning
- Physical ChemistryChemistryISBN:9781133958437Author:Ball, David W. (david Warren), BAER, TomasPublisher:Wadsworth Cengage Learning,Chemistry: The Molecular ScienceChemistryISBN:9781285199047Author:John W. Moore, Conrad L. StanitskiPublisher:Cengage Learning
Macroscale and Microscale Organic Experiments
Chemistry
ISBN:9781305577190
Author:Kenneth L. Williamson, Katherine M. Masters
Publisher:Brooks Cole
Principles of Modern Chemistry
Chemistry
ISBN:9781305079113
Author:David W. Oxtoby, H. Pat Gillis, Laurie J. Butler
Publisher:Cengage Learning
Introductory Chemistry: An Active Learning Approa...
Chemistry
ISBN:9781305079250
Author:Mark S. Cracolice, Ed Peters
Publisher:Cengage Learning
Physical Chemistry
Chemistry
ISBN:9781133958437
Author:Ball, David W. (david Warren), BAER, Tomas
Publisher:Wadsworth Cengage Learning,
Chemistry: The Molecular Science
Chemistry
ISBN:9781285199047
Author:John W. Moore, Conrad L. Stanitski
Publisher:Cengage Learning