a)
Interpretation:Use of filter flask during recrystallization at miniscale level should be determined.
Concept introduction:Recrystallization is technique that is used for purification of organic compounds. This process includes dissolution of solid in specific solvent at high temperature and then crystals are made again by process of cooling. Temperature of crystals is decreased to allow impurities to remain in solution only.
b)
Interpretation: Use of filter trap during recrystallization at miniscale level should be determined.
Concept introduction: Recrystallization is technique that is used for purification of organic compounds. This process includes dissolution of solid in specific solvent at high temperature and then crystals are made again by process of cooling. Temperature of crystals is decreased to allow impurities to remain in solution only.
c)
Interpretation: Use of Buchner funnel during recrystallization at miniscale level should be determined.
Concept introduction: Recrystallization is technique that is used for purification of organic compounds. This process includes dissolution of solid in specific solvent at high temperature and then crystals are made again by process of cooling. Temperature of crystals is decreased to allow impurities to remain in solution only.
Want to see the full answer?
Check out a sample textbook solutionChapter 3 Solutions
EBK EXPERIMENTAL ORGANIC CHEMISTRY: A M
- Volumetric pipettes are designed to deliver a precise amount of liquid, but only if you a. submerge the end of the pipette into a solution you are delivering. b. allow the pipette to drain freely, and leave any residual solution in the pipette. c. hold the pipette at a 45 degree angle and ensure that all the liquid is delivered.arrow_forwarda. What are the qualities of a perfect solvent for recrystallization? b. How much solvent must be used in the recrystallization and why?arrow_forward1. Discuss the appearance and use of each pipette. a. Ostwald folin pipette b. Volumetric pipette c. Mohr pipettearrow_forward
- Indicate which of the two filtration techniques, gravity or vacuum, is the suitable for each of the following operations. a. Hot filtration B. Removal of decolorising carbon C. Isolation of recrystallized solute from solution 2. What is the process of seedling as it applies to recrystallisation? What purpose does it serve?arrow_forwardBriefly explain why crystals form as the solvent cools during recrystallization.arrow_forwardwhich of the following statements regarding purification by recrystallization is false? i. activated charcoal removes insoluble impurities. ii. water is the best recrystallization solvent for organic compounds. iii. slow cooling permits the exclusion of the solvent from the recrystallized solid. a. i, ii, and iii b. i and ii c. i only d. ii and iiiarrow_forward
- What is brewing tea in water an example of? A. solid-liquid extraction B. liquid-liquid extraction C. none of the above D. recrystallization E. all of the abovearrow_forwardFilter paper Saturated KNO; solution 259 Figure 1. Experimental apparatus. Experimental Procedure Part 1. Copper and Zinc Metal 1) Select a piece of copper and a piece of zinc metal wire from the containers in the hood. 2) Clean the surface of the metal wires with the steel wool. Wipe clean with a dry paper towel. 3) Obtain a plastic well plate. Fill one well with 10 drops of the Copper ion solution from the dropper bottle. Label this well with a Sharpie marker so that you remember which solution you filled it with, 4) Repeat step 3 with Zinc ion solution. Select a well right next to the well in step 3 so that the two wells with Copper and Zinc ion solution are right next to each other. 5) Obtain a small dry strip of filter paper. You may have to cut a large piece of filter paper down to the appropriate size. It should be exactly this big C It's OK to tear the filter paper with your hands. Using the drop bottle, saturate the filter paper strip with KNO; solution. Gently place one end…arrow_forwardPparrow_forward
- Select all of the options below that are used to increase the purity in the purification of crystals. Stirring the solution after mixing. Filtering the crystals Recrystallization at least once. Slow cooling during crystallization. Heating the pure crystals Fast cooling during crystallization.arrow_forwardWhich statement is valid when the multiple extraction and single extraction is compared. The effciency of multiple extraction and single extraction is incomparable. Single extraction and multiple extraction have the same effciency Multiple extraction is more efficent than single extraction Single extraction is more efficient than multiple extractionarrow_forward1. Explain the importance of using a thermometer in the simple distillation setup. 2. Enumerate the characteristics of a substance for it to be separated from the heterogeneous mixture by steam distillation. 3. How does steam facilitate the distillation of essential oils? 4. Discuss some applications of simple distillation and steam distillation. Explain why you can use each method for the chosen application.arrow_forward
- Macroscale and Microscale Organic ExperimentsChemistryISBN:9781305577190Author:Kenneth L. Williamson, Katherine M. MastersPublisher:Brooks ColeChemistry: The Molecular ScienceChemistryISBN:9781285199047Author:John W. Moore, Conrad L. StanitskiPublisher:Cengage LearningEBK A SMALL SCALE APPROACH TO ORGANIC LChemistryISBN:9781305446021Author:LampmanPublisher:CENGAGE LEARNING - CONSIGNMENT