EBK EXPERIMENTAL ORGANIC CHEMISTRY: A M
6th Edition
ISBN: 9781305687875
Author: Gilbert
Publisher: CENGAGE LEARNING - CONSIGNMENT
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Chapter 3.2, Problem 15E
Interpretation Introduction
Interpretation:Five criteria that are used to select solvent for recrystallization should be determined.
Concept introduction:Recrystallization is technique that is used for purification of organic compounds. This process includes dissolution of solid in specific solvent at high temperature and then crystals are made again by process of cooling. Temperature of crystals is decreased to allow impurities to remain in solution only.
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Describe the steps involved in recrystallization.
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Chapter 3 Solutions
EBK EXPERIMENTAL ORGANIC CHEMISTRY: A M
Ch. 3.2 - Prob. 1ECh. 3.2 - Prob. 2ECh. 3.2 - Prob. 3ECh. 3.2 - Prob. 4ECh. 3.2 - Prob. 5ECh. 3.2 - Prob. 6ECh. 3.2 - Prob. 7ECh. 3.2 - Prob. 8ECh. 3.2 - Prob. 9ECh. 3.2 - Prob. 10E
Ch. 3.2 - Prob. 11ECh. 3.2 - Prob. 12ECh. 3.2 - Prob. 13ECh. 3.2 - Prob. 14ECh. 3.2 - Prob. 15ECh. 3.2 - Prob. 16ECh. 3.2 - Prob. 17ECh. 3.2 - Prob. 18ECh. 3.2 - Prob. 19ECh. 3.2 - Prob. 20ECh. 3.2 - Prob. 21ECh. 3.2 - Prob. 22ECh. 3.2 - Prob. 23ECh. 3.2 - Prob. 24ECh. 3.2 - Prob. 25ECh. 3.2 - Prob. 26ECh. 3.2 - Prob. 27ECh. 3.2 - Prob. 28ECh. 3.2 - Prob. 29ECh. 3.2 - Prob. 30ECh. 3.2 - Prob. 31ECh. 3.2 - Prob. 32ECh. 3.2 - Prob. 34ECh. 3.3 - Prob. 1ECh. 3.3 - Prob. 2ECh. 3.3 - Prob. 3ECh. 3.3 - Prob. 4ECh. 3.3 - Prob. 5ECh. 3.3 - Prob. 6ECh. 3.3 - Prob. 7ECh. 3.3 - Prob. 8ECh. 3.3 - Prob. 10ECh. 3.3 - Prob. 11ECh. 3.3 - Prob. 12ECh. 3.3 - Prob. 13ECh. 3.3 - Prob. 14ECh. 3.3 - Prob. 15ECh. 3.3 - Prob. 16ECh. 3.3 - Prob. 17ECh. 3.3 - Prob. 18ECh. 3.3 - Prob. 19ECh. 3.3 - Prob. 21ECh. 3.3 - Prob. 22ECh. 3.3 - Prob. 23ECh. 3.3 - Prob. 24ECh. 3.3 - Prob. 25ECh. 3.3 - Prob. 26E
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- Which of these is NOT true of a good recrystallization solvent? Which of these is NOT true of a good recrystallization solvent? a) The compound is insoluble in the solvent when it is cold. b) The solvent boiling temperature is at least 40 °C. c) The solvent has many impurities. d) The compound is soluble in the solvent when it is hot.arrow_forwardCompare the three main purification methods (recrystallization, distillation, and extraction) by stating whateach one is best for.arrow_forwardWhat is the theory behind recrystallization purifying a solid?arrow_forward
- Draw an outline of the recrystallization process- Assume all types of Impurities(Soluble, Insoluble and colored) are present.arrow_forwardWhy is recrystallization not applicable to samples which contain large amount of impurities?arrow_forwardWhat properties should ideally be possessed by a recrystallization solvent?arrow_forward
- Which one answer does NOT represent a characteristic of a good recrystallizing solvent? O 1) Should not react with sample. O 2) Should do a poor job of dissolving impurities when hot. O 3) Should have a moderate boiling point. O 4) Should do a good job dissolving a sample when cold.arrow_forwardUse the dropdown menus to indicate whether a solvent pair could be used successfully in a mixed-solvent recrystallization. a-hexanes and water [ Select successful or unsuccessful ] b-chloroform and diethyl ether [ Select successful or unsuccessful ] c-acetone and methanol [ Select successful or unsuccessful ]arrow_forwardExplain the difference between saturated and unsaturatedsolutions.arrow_forward
- You are tasked with performing a recrystallization. You have 3 potential solvents to use, but you don't know which one will work. How will you go about deciding which solvent to use?arrow_forwardWhy is water not used as a solvent in extraction of nutsarrow_forwardChemistry Which lab technique(s) can be performed on solid, somewhat soluble samples? Melting Range Determination or Recrystallization. Melting Range Determination. Not Recrystallization. Neither Recrystallization nor Melting Range Determination. Recrystallization. Not Melting Range Determination.arrow_forward
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