Principles of Instrumental Analysis
Principles of Instrumental Analysis
7th Edition
ISBN: 9781305577213
Author: Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher: Cengage Learning
Question
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Chapter 3, Problem 3.25QAP
Interpretation Introduction

(a)

Interpretation:

The function of the operational amplifier 1 should be determined.

Concept introduction:

The operational amplifier is a high gain device and it amplifies the voltage. Generally, a voltage amplifier has a single output and differential input. So, basically, an operational amplifier produces an output much higher than the input voltage. The output voltage could be thousands of times higher than the input voltage.

Here, the given electronic circuit is as below:

Principles of Instrumental Analysis, Chapter 3, Problem 3.25QAP , additional homework tip  1

Expert Solution
Check Mark

Explanation of Solution

Given information:

Principles of Instrumental Analysis, Chapter 3, Problem 3.25QAP , additional homework tip  2

The operational amplifier is a high gain device and it amplifies the voltage. Generally, a voltage amplifier has a single output and differential input. So basically, an operational amplifier produces an output much higher than the input voltage. The output voltage could be thousands of times higher than the input voltage.

Here the given electronic circuit is as below:

Principles of Instrumental Analysis, Chapter 3, Problem 3.25QAP , additional homework tip  3

It can be seen that the operational amplifier 1 here performing the function of inverting voltage amplifier.

Interpretation Introduction

(b)

Interpretation:

The function of the operational amplifier 2 should be determined.

Concept introduction:

The operational amplifier is a high gain device and it amplifies the voltage. Generally, a voltage amplifier has a single output and differential input. So, basically, an operational amplifier produces an output much higher than the input voltage. The output voltage could be thousands of times higher than the input voltage.

Here the given electronic circuit is as below

Principles of Instrumental Analysis, Chapter 3, Problem 3.25QAP , additional homework tip  4

Expert Solution
Check Mark

Explanation of Solution

The operational amplifier is a high gain device and it amplifies the voltage. Generally, a voltage amplifier has a single output and differential input. So basically, an operational amplifier produces an output much higher than the input voltage. The output voltage could be thousands of times higher than the input voltage.

Here the given electronic circuit is as below:

Principles of Instrumental Analysis, Chapter 3, Problem 3.25QAP , additional homework tip  5

It can be seen that the operational amplifier 2 here performing the function of integrating circuit and hence the integration.

Interpretation Introduction

(c)

Interpretation:

The output voltage during the interval Δt1 should be described and plotted. Where Δt1 is the first period when switches S1 and S2 are closed and switch S4 opens. The function of the operational amplifier 2.

Concept introduction:

The operational amplifier is a high gain device and it amplifies the voltage. Generally, a voltage amplifier has a single output and differential input. So, basically, an operational amplifier produces an output much higher than the input voltage. The output voltage could be thousands of times higher than the input voltage.

Here the given electronic circuit is as below

Principles of Instrumental Analysis, Chapter 3, Problem 3.25QAP , additional homework tip  6

Expert Solution
Check Mark

Explanation of Solution

The operational amplifier is a high gain device and it amplifies the voltage. Generally, a voltage amplifier has a single output and differential input. So basically, an operational amplifier produces an output much higher than the input voltage. The output voltage could be thousands of times higher than the input voltage.

Here the given electronic circuit is as below:

Principles of Instrumental Analysis, Chapter 3, Problem 3.25QAP , additional homework tip  7

Here the input voltage v1 is linearly increasing voltage. This is given by the equation

v1=at+c

Where a and c are constants and t is time.

As per the problem switches S1 and S2 are closed and switch S4 opens hence the circuit acts as an integrating circuit which amplifies the output.

Here, the output signal can be given by the formula as below

vo=1RC0tv1dt=1RC0t(at+c)dt=1RC×(at+c)22a

Now assume RC=12,a=1,c=0.

Substitute the values in the above equation and simplify, the result obtained is

vo=t2

The integrating voltage at different time intervals is given as:

Time(s) Output Voltage (V)
1 1
4 16
6 36
8 64
11 121
20 40

The plot can be obtained as shown below:

Principles of Instrumental Analysis, Chapter 3, Problem 3.25QAP , additional homework tip  8

Interpretation Introduction

(d)

Interpretation:

The output voltage during the second interval Δt should be described and plotted. Where Δt is the second period when switches S2 opens and S3 closes.

Concept introduction:

The operational amplifier is a high gain device and it amplifies the voltage. Generally, a voltage amplifier has a single output and differential input. So, basically, an operational amplifier produces an output much higher than the input voltage. The output voltage could be thousands of times higher than the input voltage.

Here the given electronic circuit is as below

Principles of Instrumental Analysis, Chapter 3, Problem 3.25QAP , additional homework tip  9

Expert Solution
Check Mark

Explanation of Solution

The operational amplifier is a high gain device and it amplifies the voltage. Generally, a voltage amplifier has a single output and differential input. So basically, an operational amplifier produces an output much higher than the input voltage. The output voltage could be thousands of times higher than the input voltage.

Here the given electronic circuit is as below

Principles of Instrumental Analysis, Chapter 3, Problem 3.25QAP , additional homework tip  10

Here the input voltage v1 is linearly increasing voltage. This is given by the equation

v1=at+c

Where a and c are constants and t is time.

As per the problem switches S2 opens and S3 closes hence the circuit acts as an combination of the inverting voltage amplifier and integrating circuit.

Here the output signal can be given by the formula as below

vo=RfRivi

Where Rf and Ri are resistance. Also assume that Rf=Ri.

Therefore, it can be said that

vo=vi

The output of the second operational amplifier which is actually the final output can be given by the equation as below:

vo=1RC×(at+c)22a

Where a and c are constants.

Now assume RC=12,a=1,c=0.

Substitute the values in the above equation and simplify, the result obtained is

vo=t2

The integrating voltage at different time intervals is given as:

Time(s) Output Voltage (V)
1 -1
4 -16
6 -36
8 -64
11 -121
20 -40

The plot can be obtained as shown below:

Principles of Instrumental Analysis, Chapter 3, Problem 3.25QAP , additional homework tip  11

Interpretation Introduction

(e)

Interpretation:

The output voltage Vo at the end of the measurement cycle is given by vo=k× input rate should be shown.

Concept introduction:

The operational amplifier is a high gain device and it amplifies the voltage. Generally, a voltage amplifier has a single output and differential input. So, basically, an operational amplifier produces an output much higher than the input voltage. The output voltage could be thousands of times higher than the input voltage.

Here the given electronic circuit is as below

Principles of Instrumental Analysis, Chapter 3, Problem 3.25QAP , additional homework tip  12

Expert Solution
Check Mark

Explanation of Solution

The operational amplifier is a high gain device and it amplifies the voltage. Generally, a voltage amplifier has a single output and differential input. So basically, an operational amplifier produces an output much higher than the input voltage. The output voltage could be thousands of times higher than the input voltage.

Here the given electronic circuit is as below

Principles of Instrumental Analysis, Chapter 3, Problem 3.25QAP , additional homework tip  13

Since there is no current so capacitor will discharge. And circuit will act as differentiator.

voRf=C×dvidt

Further, it can be re-written as

vo=RfC×dvidt

The output can be given as

vo=k×dvidt

Interpretation Introduction

(f)

Interpretation:

The advantages and disadvantages of the given circuit over the normal amplifier should be described.

Concept introduction:

The operational amplifier is a high gain device and it amplifies the voltage. Generally, a voltage amplifier has a single output and differential input. So, basically, an operational amplifier produces an output much higher than the input voltage. The output voltage could be thousands of times higher than the input voltage.

Here the given electronic circuit is as below

Principles of Instrumental Analysis, Chapter 3, Problem 3.25QAP , additional homework tip  14

Expert Solution
Check Mark

Explanation of Solution

The operational amplifier is a high gain device and it amplifies the voltage. Generally, a voltage amplifier has a single output and differential input. So basically, an operational amplifier produces an output much higher than the input voltage. The output voltage could be thousands of times higher than the input voltage.

Here the given electronic circuit is as below

Principles of Instrumental Analysis, Chapter 3, Problem 3.25QAP , additional homework tip  15

Since there is no current so capacitor will discharge. And circuit will act as differentiator.

In general, the normal operational amplifier circuit can be used as a differentiator circuit only. But the given integrating circuit can be used as differentiator as well as integrator. Just one disadvantage is that the given circuit has higher noise level as compared to the normal circuit.

Interpretation Introduction

(g)

Interpretation:

The scenario if the input signal gets changes with the slope during the measurement cycle should be determined.

Concept introduction:

The operational amplifier is a high gain device and it amplifies the voltage. Generally, a voltage amplifier has a single output and differential input. So, basically, an operational amplifier produces an output much higher than the input voltage. The output voltage could be thousands of times higher than the input voltage.

Here the given electronic circuit is as below

Principles of Instrumental Analysis, Chapter 3, Problem 3.25QAP , additional homework tip  16

Expert Solution
Check Mark

Explanation of Solution

The operational amplifier is a high gain device and it amplifies the voltage. Generally, a voltage amplifier has a single output and differential input. So basically, an operational amplifier produces an output much higher than the input voltage. The output voltage could be thousands of times higher than the input voltage.

Here the given electronic circuit is as below

Principles of Instrumental Analysis, Chapter 3, Problem 3.25QAP , additional homework tip  17

Since there is no current so capacitor will discharge. And circuit will act as differentiator.

The output of the second operational amplifier which is actually the final output can be given by the equation as below:

vo=1RC×(at+c)22a

Where a and c are constants.

Now assume RC=12,a=1,c=0.

Substitute the values in the above equation and simplify, the result obtained is

vo=at2

Further it can be written that

vo1vo2=a1a2t2

Interpretation Introduction

(h)

Interpretation:

The result obtained if the two-time intervals are separated by a time delay Δt3 should be determined.

Concept introduction:

The operational amplifier is a high gain device and it amplifies the voltage. Generally, a voltage amplifier has a single output and differential input. So, basically, an operational amplifier produces an output much higher than the input voltage. The output voltage could be thousands of times higher than the input voltage.

Here the given electronic circuit is as below

Principles of Instrumental Analysis, Chapter 3, Problem 3.25QAP , additional homework tip  18

Expert Solution
Check Mark

Explanation of Solution

The operational amplifier is a high gain device and it amplifies the voltage. Generally, a voltage amplifier has a single output and differential input. So basically, an operational amplifier produces an output much higher than the input voltage. The output voltage could be thousands of times higher than the input voltage.

Here the given electronic circuit is as below

Principles of Instrumental Analysis, Chapter 3, Problem 3.25QAP , additional homework tip  19

For the given circuit the during the first time interval Δt1, the output voltage is an integration voltage over a period of Δt1. Also, in the same way the output voltage is integrating voltage during the second interval Δt2 but in this case the phase is opposite of the previous phase.

Now if the two-time intervals are separated by a time delay Δt3 then there will be a sudden change in the output voltage. The change is output voltage can be from 225v to 1.

Interpretation Introduction

(i)

Interpretation:

The result if the two-time intervals were of different duration should be determined.

Concept introduction:

The operational amplifier is a high gain device and it amplifies the voltage. Generally, a voltage amplifier has a single output and differential input. So, basically, an operational amplifier produces an output much higher than the input voltage. The output voltage could be thousands of times higher than the input voltage.

Here the given electronic circuit is as below

Principles of Instrumental Analysis, Chapter 3, Problem 3.25QAP , additional homework tip  20

Expert Solution
Check Mark

Explanation of Solution

The operational amplifier is a high gain device and it amplifies the voltage. Generally, a voltage amplifier has a single output and differential input. So basically, an operational amplifier produces an output much higher than the input voltage. The output voltage could be thousands of times higher than the input voltage.

Here the given electronic circuit is as below

Principles of Instrumental Analysis, Chapter 3, Problem 3.25QAP , additional homework tip  21

As its known that, if the two-time intervals are same then the plot of the output voltage is same in magnitude and opposite in sign for both the interval. But if the two-time intervals are of different duration then the magnitude of output signal will be different for both the time periods.

Interpretation Introduction

(j)

Interpretation:

The reason should be discussed for why the time interval is desirable to be as large as possible in measuring enzyme kinematics.

Concept introduction:

The operational amplifier is a high gain device and it amplifies the voltage. Generally, a voltage amplifier has a single output and differential input. So, basically, an operational amplifier produces an output much higher than the input voltage. The output voltage could be thousands of times higher than the input voltage.

Here the given electronic circuit is as below:

Principles of Instrumental Analysis, Chapter 3, Problem 3.25QAP , additional homework tip  22

Expert Solution
Check Mark

Explanation of Solution

The operational amplifier is a high gain device and it amplifies the voltage. Generally, a voltage amplifier has a single output and differential input. So basically, an operational amplifier produces an output much higher than the input voltage. The output voltage could be thousands of times higher than the input voltage.

Here the given electronic circuit is as below

Principles of Instrumental Analysis, Chapter 3, Problem 3.25QAP , additional homework tip  23

Since there is no current so capacitor will discharge. And circuit will act as differentiator.

The output of the second operational amplifier which is actually the final output can be given by the equation as below:

vo=1RC×(at+c)22a

Where a and c are constants.

Now, assume RC=12,a=1,c=0.

Substitute the values in the above equation and simplify, the result obtained is

vo=at2

If the time gets larger then the output voltage also gets larger.

Enzyme kinematics are generally time-consuming process. So, its desirable to have larger time.

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