Principles of Instrumental Analysis
7th Edition
ISBN: 9781305577213
Author: Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher: Cengage Learning
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Chapter 26, Problem 26.22QAP
Interpretation Introduction
Interpretation:
The percentage of each component in the given mixture is to be stated.
Concept introduction:
The retention factor is the ratio of the number of moles of the solutes in the mobile phase and the number of moles of the solutes in the stationary phase.
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Chapter 26 Solutions
Principles of Instrumental Analysis
Ch. 26 - Prob. 26.1QAPCh. 26 - Prob. 26.2QAPCh. 26 - Prob. 26.3QAPCh. 26 - Prob. 26.4QAPCh. 26 - Prob. 26.5QAPCh. 26 - Prob. 26.6QAPCh. 26 - Prob. 26.7QAPCh. 26 - Prob. 26.8QAPCh. 26 - Prob. 26.9QAPCh. 26 - Prob. 26.10QAP
Ch. 26 - Prob. 26.11QAPCh. 26 - Prob. 26.12QAPCh. 26 - Prob. 26.13QAPCh. 26 - Prob. 26.14QAPCh. 26 - Prob. 26.15QAPCh. 26 - Prob. 26.16QAPCh. 26 - From the data in Problem 26-14, calculate for...Ch. 26 - Prob. 26.18QAPCh. 26 - Prob. 26.19QAPCh. 26 - Prob. 26.20QAPCh. 26 - Prob. 26.21QAPCh. 26 - Prob. 26.22QAPCh. 26 - Prob. 26.23QAP
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- You have obtained a gas chromatogram of a two component mixture of compounds A and B. The height of peak A is 3.84 cm. and the width at half height is 1 cm. The height of peak B is 3.49 cm. and the width at half height is 1.36 cm. The percentage of a component in the mixture is proportional to peak area. Estimate peak areas by multiplying height by width at half height. What was the percentage of compound B in the mixture? (Enter your answer as a number without any percent symbol or the word percent.)arrow_forwardChromatography is a separation technique. What is the physical or chemical basis for separation of compounds during thin layer chromatography?arrow_forwardFor quantitative analysis with gas chromatography: O the area of a peak reported by the instrument for a compound is proportional to the quantity of that compound. O the calculated response factor value for a compound is proportional to the quantity of that compound. O the retention time reported by the instrument for a compound is proportional to the quantity of that compound. O the peak height reported by the instrument for a compound is inversely proportional to the quantity of that compound. O the peak shape reported by the instrument for a compound is proportional to the quantity of that compound.arrow_forward
- 1) Study the chromatograph (below) of a mixture of Compounds A and B, run on the GCs in the teaching labs at CU Boulder. Compound A has the shorter retention time. STAAT 61 1.11 227 RT TYPE AREA XXXX XXXX XXXX AREAS 0.009 55874 44.117 ARIHT 0.61 XX XX XX 1.11 2.27 XX XX XX TOTAL AREA=XX MUL FACTOR=XX 1. What is the retention time of compound A? Compound B? 2. Which compound is present in a larger amount? 3. Which compound has the lower boiling point? 4. What would happen to the retention times of compounds A and B if the column temperature were raised? 5. You suspect that compound B is octane. What can you do to provide supporting evidence for this hypothesis?arrow_forwardA student places an unknown sample on a thin-layer chromatography plate and develops it in dichloromethane as a solvent. Only one spot whose Rf is 0.98 is observed. Does this result indicate that the unknown material is a pure compound? If not a pure compound, suggest an alternate procedure to verify the purity of the sample.arrow_forwardA chromatographic column is eluted with a solution containing a mixture of two components, X and Y. The chemical affinity of X for the stationary phase is less than that of Y and the chemical affinity for X for the mobile is greater than that of Y. Which substance will be eluted first? Explain your answer.arrow_forward
- Which statement(s) are correct for gas chromatography? A) the components in a mixture can be identified from their retention time. B) the relative peak areas give the proportions of components in a mixture. C) Calibration curves are used to confirms the concentrations of components in a mixture.arrow_forwardThe height of three peaks; A, B, and C obtained in a gas chromatogram are 20.6 mm, 17.5 mm and 40.6 mm. The width of the peaks, at half height, are 4.4 mm, 4.0 mm and 3.9 mm, respectively. Calculate the percentage composition of A in the sample.arrow_forwardHow does paper chromatography allow you to separate substances?arrow_forward
- Which of the following changes would work to improve chromatographic separations? Explain briefly why each option would or would not help. 1) Decreasing the length of the column. 2) Increasing the diameter of the column 3) Decreasing the diameter of the column 4) Increasing the length of the columnarrow_forwardHow do I answer this question?arrow_forwardSketch a chromatogram for a compound with a stronger interaction with the stationary phase than the one shown below (draw on top of the shown chromatogram). Briefly explain how and why it is different.arrow_forward
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