EBK CHEMISTRY: THE MOLECULAR NATURE OF
7th Edition
ISBN: 9781119513216
Author: HYSLOP
Publisher: JOHN WILEY+SONS INC.
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Chapter 10, Problem 55RQ
A sample of argon with a volume of 6.18 L, a pressure of 761 torr, and a temperature of
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You have now performed a liquid-liquid extraction protocol in Experiment 4. In doing so, you
manipulated and exploited the acid-base chemistry of one or more of the compounds in your
mixture to facilitate their separation into different phases. The key to understanding how liquid-
liquid extractions work is by knowing which layer a compound is in, and in what protonation state.
The following liquid-liquid extraction is different from the one you performed in Experiment
4, but it uses the same type of logic. Your task is to show how to separate apart Compound
A and Compound B.
. Complete the following flowchart of a liquid-liquid extraction. Handwritten work is
encouraged.
•
Draw by hand (neatly) only the appropriate organic compound(s) in the boxes.
.
Specify the reagent(s)/chemicals (name is fine) and concentration as required in Boxes 4
and 5.
•
Box 7a requires the solvent (name is fine).
•
Box 7b requires one inorganic compound.
• You can neatly complete this assignment by hand and…
b) Elucidate compound D w) mt at 170 nd shows c-1 stretch at 550cm;'
The compound has the ff electronic transitions: 0%o* and no a*
1H NMR Spectrum
(CDCl3, 400 MHz)
3.5
3.0
2.5
2.0
1.5
1.0
0.5 ppm
13C{H} NMR Spectrum
(CDCl3, 100 MHz)
Solvent
80
70
60
50
40
30
20
10
0 ppm
ppm
¹H-13C me-HSQC Spectrum
ppm
(CDCl3, 400 MHz)
5
¹H-¹H COSY Spectrum
(CDCl3, 400 MHz)
0.5
10
3.5
3.0
2.5
2.0
1.5 1.0
10
15
20
20
25
30
30
-35
-1.0
1.5
-2.0
-2.5
3.0
-3.5
0.5
ppm
3.5
3.0
2.5
2.0
1.5
1.0
0.5
ppm
Show work with explanation. don't give Ai generated solution
Chapter 10 Solutions
EBK CHEMISTRY: THE MOLECULAR NATURE OF
Ch. 10 - Prob. 1PECh. 10 - Prob. 2PECh. 10 - Prob. 3PECh. 10 - Prob. 4PECh. 10 - Prob. 5PECh. 10 - Prob. 6PECh. 10 - Prob. 7PECh. 10 - Prob. 8PECh. 10 - Prob. 9PECh. 10 - Prob. 10PE
Ch. 10 - Practice Exercise 10.11 How many grams of argon...Ch. 10 - Prob. 12PECh. 10 - Practice Exercise 10.13
The label on a cylinder of...Ch. 10 - A glass bulb is found to have a volume of 544.23...Ch. 10 - Sulfur dioxide is a gas that has been used in...Ch. 10 - Radon, a radioactive gas, is formed in one step of...Ch. 10 - Practice Exercise 10.17
A gaseous compound of...Ch. 10 - A compound composed of only carbon and hydrogen...Ch. 10 - Carbon disulfide is an extremely flammable liquid....Ch. 10 - In one lab, thegas-collecting apparatus used a gas...Ch. 10 - The explosive PETN, pentaerythritoltetranitrate,...Ch. 10 - Prob. 22PECh. 10 - Suppose you prepared a sample of nitrogen and...Ch. 10 - A 2.50 L sample of methane was collected over...Ch. 10 - Suppose a mixture containing 2.15 g H2 and 34.0 g...Ch. 10 - Sulfur dioxide and oxygen react according to the...Ch. 10 - Bromine has two isotopes with masses of 78.9 and...Ch. 10 - The hydrogen halide gases all have the same...Ch. 10 - Prob. 1RQCh. 10 - Prob. 2RQCh. 10 - Prob. 3RQCh. 10 - Prob. 4RQCh. 10 - Prob. 5RQCh. 10 - Prob. 6RQCh. 10 - Prob. 7RQCh. 10 - What is meant by an ideal gas? Under what...Ch. 10 - Prob. 9RQCh. 10 - Prob. 10RQCh. 10 - Prob. 11RQCh. 10 - Prob. 12RQCh. 10 - Prob. 13RQCh. 10 - Prob. 14RQCh. 10 - Prob. 15RQCh. 10 - Prob. 16RQCh. 10 - Prob. 17RQCh. 10 - Prob. 18RQCh. 10 - Prob. 19RQCh. 10 - Prob. 20RQCh. 10 - Prob. 21RQCh. 10 - Prob. 22RQCh. 10 - Prob. 23RQCh. 10 - Prob. 24RQCh. 10 - Prob. 25RQCh. 10 - Prob. 26RQCh. 10 - Prob. 27RQCh. 10 - Prob. 28RQCh. 10 - Prob. 29RQCh. 10 - Prob. 30RQCh. 10 - What does a small value for the van der Waals...Ch. 10 - Which of the molecules below has the larger value...Ch. 10 - Under the same conditions of T and V, why is the...Ch. 10 - Prob. 34RQCh. 10 - Carry out the following unit conversions: (a) 1.26...Ch. 10 - Prob. 36RQCh. 10 - Prob. 37RQCh. 10 - 10.38 What is the pressure in atm of each of the...Ch. 10 - 10.39 An open-end manometer containing mercury was...Ch. 10 - Prob. 40RQCh. 10 - Prob. 41RQCh. 10 - An open-end mercury manometer was connected to a...Ch. 10 - Prob. 43RQCh. 10 - 10.44 Suppose a gas is in a vessel connected to...Ch. 10 - Prob. 45RQCh. 10 - Prob. 46RQCh. 10 - Prob. 47RQCh. 10 - Prob. 48RQCh. 10 - Prob. 49RQCh. 10 - Prob. 50RQCh. 10 - A sample of helium at a pressure of 74$ torr and...Ch. 10 - When a sample of neon with a volume of 648 mL and...Ch. 10 - What must be the new volume of a sample of...Ch. 10 - When 286 mL of oxygen at 741 torr and 18.0C was...Ch. 10 - A sample of argon with a volume of 6.18 L, a...Ch. 10 - Prob. 56RQCh. 10 - How many milliliters of O2 are consumed in the...Ch. 10 - How many milliliters of oxygen are required to...Ch. 10 - *10.59 How many milliliters of measured at and...Ch. 10 - How many milliliters of H2O vapor, measured at...Ch. 10 - Prob. 61RQCh. 10 - Prob. 62RQCh. 10 - Prob. 63RQCh. 10 - Prob. 64RQCh. 10 - Prob. 65RQCh. 10 - Prob. 66RQCh. 10 - Prob. 67RQCh. 10 - Prob. 68RQCh. 10 - Prob. 69RQCh. 10 - 10.70 Methane is formed in landfills by the action...Ch. 10 - A chemist isolated a gas in a glass bulb with a...Ch. 10 - Prob. 72RQCh. 10 - 10.73 To three significant figures, calculate the...Ch. 10 - To three significant figures, calculate the...Ch. 10 - 10.75 What density does oxygen have at and 742...Ch. 10 - At 748.0 torr and 20.65C, what is the density of...Ch. 10 - The explosive PETN, pentaerythritol tetranitrate,...Ch. 10 - TNT, trinitrotoluene, is an explosive that can...Ch. 10 - Propylene, C3H6, reacts with hydrogen under...Ch. 10 - Nitric acid is formed when NO2 is dissolved in...Ch. 10 - A mixture of gases contains 315 torr N2, 275 torr...Ch. 10 - Prob. 82RQCh. 10 - A 1.00 L container was filled by pumping into it...Ch. 10 - A special gas mixture, BAR 97 High without NO, is...Ch. 10 - Prob. 85RQCh. 10 - Prob. 86RQCh. 10 - A 22.4 L container at 0C contains 0.300 mol N2,...Ch. 10 - A mixture of N2,O2,andCO2 Has a total pressure of...Ch. 10 - A 0.200 mol sample of a mixture of N2 and CO2 with...Ch. 10 - A sample of carbon monoxide was prepared and...Ch. 10 - Prob. 91RQCh. 10 - What volume of wet oxygen would you have to...Ch. 10 - Prob. 93RQCh. 10 - Prob. 94RQCh. 10 - Prob. 95RQCh. 10 - 10.96 For the gases which gas will effuse the...Ch. 10 - Prob. 97RQCh. 10 - Prob. 98RQCh. 10 - Uranium hexafluoride is a white solid that readily...Ch. 10 - Prob. 100RQCh. 10 - Prob. 101RQCh. 10 - A typical automobile has a weight of approximately...Ch. 10 - *10.103 Suppose you were planning to move a house...Ch. 10 - Prob. 104RQCh. 10 - Two flasks (which we will refer to as flask 1 and...Ch. 10 - *10.106 A bubble of air escaping from a divers...Ch. 10 - *10.107 In a diesel engine, the fuel is ignited...Ch. 10 - *10.108 Early one cool (60.0F) morning you start...Ch. 10 - Prob. 109RQCh. 10 - *10.110 A mixture was prepared in a 0.500 L...Ch. 10 - *10.111 A student collected 18.45 mL of H2 over...Ch. 10 - *10.112 A mixture of gases is prepared from 87.5 g...Ch. 10 - 10.113 A gas was found to have a density of...Ch. 10 - *10.114 In one analytical procedure for...Ch. 10 - Prob. 115RQCh. 10 - Prob. 116RQCh. 10 - Prob. 117RQCh. 10 - The odor of a rotten egg is caused by hydrogen...Ch. 10 - Chlorine reacts with sulfite ion to give sulfate...Ch. 10 - *10.120 In an experiment designed to prepare a...Ch. 10 - Carbon dioxide can be made in the lab by the...Ch. 10 - 10.122 Boron forms a variety of unusual compounds...Ch. 10 - Prob. 123RQCh. 10 - Carbon dioxide is implicated in global warming....Ch. 10 - Prob. 125RQCh. 10 - One of the that is implicated in decreasing the...
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- Redraw the flowchartarrow_forwardredraw the flowchart with boxes and molecules written in themarrow_forwardPart I. a) Elucidate the structure of compound A using the following information. • mass spectrum: m+ = 102, m/2=57 312=29 • IR spectrum: 1002.5 % TRANSMITTANCE Ngg 50 40 30 20 90 80 70 60 MICRONS 5 8 9 10 12 13 14 15 16 19 1740 cm M 10 0 4000 3600 3200 2800 2400 2000 1800 1600 13 • CNMR 'H -NMR Peak 8 ppm (H) Integration multiplicity a 1.5 (3H) triplet b 1.3 1.5 (3H) triplet C 2.3 1 (2H) quartet d 4.1 1 (2H) quartet & ppm (c) 10 15 28 60 177 (C=0) b) Elucidate the structure of compound B using the following information 13C/DEPT NMR 150.9 MHz IIL 1400 WAVENUMBERS (CM-1) DEPT-90 DEPT-135 85 80 75 70 65 60 55 50 45 40 35 30 25 20 ppm 1200 1000 800 600 400arrow_forward
- • Part II. a) Elucidate The structure of compound c w/ molecular formula C10 11202 and the following data below: • IR spectra % TRANSMITTANCE 1002.5 90 80 70 60 50 40 30 20 10 0 4000 3600 3200 2800 2400 2000 1800 1600 • Information from 'HAMR MICRONS 8 9 10 11 14 15 16 19 25 1400 WAVENUMBERS (CM-1) 1200 1000 800 600 400 peak 8 ppm Integration multiplicity a 2.1 1.5 (3H) Singlet b 3.6 1 (2H) singlet с 3.8 1.5 (3H) Singlet d 6.8 1(2H) doublet 7.1 1(2H) doublet Information from 13C-nmR Normal carbon 29ppm Dept 135 Dept -90 + NO peak NO peak 50 ppm 55 ppm + NO peak 114 ppm t 126 ppm No peak NO peak 130 ppm t + 159 ppm No peak NO peak 207 ppm по реак NO peakarrow_forwardCould you redraw these and also explain how to solve them for me pleasarrow_forwardNonearrow_forward
- Draw the curved-arrow mechanism with the drawings of the molecules, not just abbreviations. -NO₂ Sn, HCl (aq) E D H (CH3CO)₂O -NH2 CH3arrow_forwardWhat is/are the product(s) of the following reaction? Select all that apply. * HI A B C OD OH A B OH D Carrow_forwardIn the image, the light blue sphere represents a mole of hydrogen atoms, the purple or teal spheres represent a mole of a conjugate base. A light blue sphere by itself is H+. Assuming there is 2.00 L of solution, answer the following: The Ka of the left & right solution is? The pH of the left & right solution is? The acid on the left & right is what kind of acid?arrow_forward
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